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Abstract
In this study, a QuEChERS method and gas chromatography coupled with time-of-flight mass spectrometry (GCxGC-TOFMS) was developed for rapid extraction and simultaneous determination of 12 pesticide residues in honey. The GCxGC-TOFMS method was validated according to the SANCO guidance in terms of linearity, selectivity, reproducibility and recovery. Regarding the results, recovery rates ranged between 70-120% with relative standard deviations <20% in most cases. The method limits of quantification (LOQ) ranged between 6-26 ng/g. According to the estimated LOQ values the analytical procedure can be applied to analysis of real honey samples.
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- Category:
- Articles
- Type:
- artykuły w czasopismach recenzowanych i innych wydawnictwach ciągłych
- Published in:
-
Journal of Bioprocessing & Biotechniques
no. 4,
edition 7,
pages 1 - 5,
ISSN: 2155-9821 - Language:
- English
- Publication year:
- 2014
- Bibliographic description:
- Bargańska Ż., Olkowska E., Dymerski T., Namieśnik J.: Determination of Pesticide Residues in Honey using the GC×GC-TOFMS Technique// Journal of Bioprocessing & Biotechniques. -Vol. 4., iss. 7 (2014), s.1-5
- Verified by:
- Gdańsk University of Technology
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