Year 2011

• Synthesis, spectroscopy and computational studies of some novelphosphorylated derivatives of quinoline-5,8-diones

  Publication

  • J. Nycz
  • G. Malecki
  • Ł. Ponikiewski
  • M. Leboschka
  • M. Nowak
  • J. Kusz

  - JOURNAL OF MOLECULAR STRUCTURE - Year 2011

  The neutral phosphorus nucleophiles such as R2P(=Y)M allowed the radical addition to 2-methyl-5,8-dioxo-5,8-dihydroquinoline-7-amine and N-(2-methyl-5,8-dioxo-5,8-dihydroquinolin-7-yl)acetamide giving exclusively O-phosphorylated products. All products were quantitatively prepared and characterized by microanalysis, and multinuclear NMR spectroscopy. Seven of them, have been characterized by single crystal X-ray diffraction method....

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Year 2010

• Synthesis, spectroscopy and computational studies of some biologically important hydroxyhaloquinolines and their novel derivatives

  Publication

  • G. Małecki
  • J. Nycz
  • E. Ryrych
  • Ł. Ponikiewski
  • M. Nowak
  • J. Kusz
  • J. Pikies

  - JOURNAL OF MOLECULAR STRUCTURE - Year 2010

  A series crystalline compounds of methyl and phosphinyl derivatives of 2-methylquinolin-8-ol (1a) and related 5,7-dichloro-2-methylquinolin-8-ol (1b) were quantitatively prepared and characterized by microanalysis, IR, UV-vis and multinuclear NMR spectroscopy. Five of them have been characterized by single crystal X-ray diffraction method. The known compounds, 8-methoxy-2-methylquinoline (2a) and 8-methoxyquinoline (2d), were synthesised...

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