Influence of the annealing condictions on the chemical structure of LaBaGdCo ceramics - Open Research Data - Bridge of Knowledge

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Influence of the annealing condictions on the chemical structure of LaBaGdCo ceramics

Description

Ceramic samples based on Barium, Lanthanum, Gadolinium and Cobaltium were produced by solid state reaction.  After sintring in a furnance, samples were annealed at 300 Celsius degree in wet and dry atmosphere. Annealing takes 72h or 2h. Results of annealing were observed by X-Ray photoemission spectroscopy (XPS), OmicronNanotechnology.  XPS analysis were performed at room temperature under a pressure below 1.1 × 10−9 mBar. The photoelectrons were excited by an Mg-Kα X-Ray anode operated at 15 keV and 300 W. Omicron Argus hemispherical electron analyser with a round aperture of 4 mm was used for the analysis of emitted photoelectrons. Measurements were carried out in a constant analyser energy (CAE) mode with pass energy equal 50 eV. To remove contaminations and oxides, the surface was etched before the measurement. Argon ion gun with energy up to 5 keV was used for 5 min. etching. In this dataset Ba3d, Ba4d and Ba4p high resolution spectra for samples are presented.

Dataset file

Ba.zip
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License:
Creative Commons: by 4.0 open in new tab
CC BY
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Details

Year of publication:
2021
Verification date:
2021-07-19
Creation date:
2019
Dataset language:
English
Fields of science:
  • materials engineering (Engineering and Technology)
DOI:
DOI ID 10.34808/d9ba-0928 open in new tab
Verified by:
Gdańsk University of Technology

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