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Linear impedance of 2Si3N4–98(40Na2O-20CaO-40P2O5) glass measured with impedance spectroscopy method at low temperature region
Description
The linear electrical properties of 2Si3N4–98(40Na2O-20CaO-40P2O5) glass was measured by impedance spectroscopy method.
The composition of 2Si3N4–98(40Na2O-20CaO-40P2O5) (in mol%) was prepared by the conventional melt quenching technique. Appropriate amounts of reagents: NaH2PO4 (≥99.5% SIGMA ALDRICH), Na2CO3 (99.9+% ChemPur GmbH) and CaCO3 (99.9+% ChemPur GmbH), Si3N4 (99.9+% ChemPur GmbH) were thoroughly mixed. Batches were melted in porcelain crucibles at temperatures of 850–950 degC for 30–60 min, in air atmosphere. Melt was poured on a brass plate. The exact composition of samples was checked with the use of SEM-EDS and wa sfound to be Na17.3Ca4.6P16.6Si1.3O58N2.1 in at%.
For the electrical measurements gold electrodes were evaporated at the preheated samples. Impedance measurements were carried out in the temperature range from 153 K to 423 K, in the frequency range from 10mHz to 1 MHz and with the ac voltage of 1 Vrms with Concept 40 broadband dielectric spectrometer.
Dataset file
hexmd5(md5(part1)+md5(part2)+...)-{parts_count} where a single part of the file is 512 MB in size.Example script for calculation:
https://github.com/antespi/s3md5
File details
- License:
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CC BYAttribution - Raw data:
- Data contained in dataset was not processed.
Details
- Year of publication:
- 2018
- Verification date:
- 2021-07-19
- Dataset language:
- English
- Fields of science:
-
- materials engineering (Engineering and Technology)
- DOI:
- DOI ID 10.34808/vj5t-t870 open in new tab
- Verified by:
- Gdańsk University of Technology
Keywords
References
- publication Electrical properties of Na2O-CaO-P2O5 glasses doped with SiO2 and Si3N4
- publication Influence of synthesis conditions on glass formation, structure and thermal properties in the Na 2 O-CaO-P 2 O 5 system doped with Si 3 N 4 and Mg
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