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Description
The DataSet contains the XRD patterns of the TeOx-BaO-BiO powder. The material was obtained by the sol-gel method. The starting solution was prepared by mixing telluric acid (precursor), barium carbonate, and bismuth carbonate with thetraetylene glycol, water, ethanol, and acetic acid. (Samples molar concentration: 73TeO2-4BaO-3Bi2O3 and 73TeO2-3BaO-4Bi2O3). The sol was obtained by vigorously stirring precursor solution at 50°C for 2h, then the temperature was raised to 75°C for the next 2h. The obtained gels were dried in two different ways. The 73TeO2-4BaO-3Bi2O3 and 73TeO2-3BaO-4Bi2O3 gels were dried at 120°C under an argon atmosphere. Next, the xerogel powders were first annealing at 340°C under an argon atmosphere, then at 450°C under oxidizing atmosphere. In the second approach, the 73TeO2-4BaO-3Bi2O3 gel was dried under 80 bar at 80°C in an autoclave.
X-ray diffraction patterns (XRD) were collected on a Philips X’PERT PLUS diffractometer with Cu Ka radiation (1.5406 Å) and ranging from 10 to 80 degrees.
Dataset file
hexmd5(md5(part1)+md5(part2)+...)-{parts_count} where a single part of the file is 512 MB in size.Example script for calculation:
https://github.com/antespi/s3md5
File details
- License:
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open in new tab
CC BYAttribution - Raw data:
- Data contained in dataset was not processed.
- Software:
- HighScore Plus
Details
- Year of publication:
- 2021
- Verification date:
- 2021-07-14
- Dataset language:
- English
- Fields of science:
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- materials engineering (Engineering and Technology)
- DOI:
- DOI ID 10.34808/25yp-7b87 open in new tab
- Series:
- Verified by:
- Gdańsk University of Technology
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