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Development and validation of an LC–MS/MS method for the determination of biogenic amines in wines and beers
Abstract
Biogenic amines are group of organic, basic, nitrogenous compounds that naturally occur in plant, microorganism, and animal organisms. Biogenic amines are mainly produced through decarboxylation of amino acids. They are formed during manufacturing of some kind of food and beverages such as cheese, wine, or beer. Histamine, cadaverine, agmatine, tyramine, putrescine, and b-phenylethylamine are the most common biogenic amines found in wines and beers. This group of compounds can be toxic at high concentrations; therefore, their control is very important. Analysis of biogenicamines in alcoholic drinks (beers and wines) was carried out by HPLC–MS/MS after their derivatization with p-toluenesulfonyl chloride (tosyl chloride). The developed method has been applied for analysis of seventeen biogenic amines in twentyeight samples of lager beers and in twelve samples of different homemade wines (white grape, red grape, strawberry, chokeberry, black currant, plum, apple, raspberry, and quince). The developed method is sensitive and repeatable for majority of the analytes. It is versatile and can be used for the determination of biogenic amines in various alcoholic beverages.
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- Accepted or Published Version
- DOI:
- Digital Object Identifier (open in new tab) 10.1007/s00706-017-1992-y
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- Category:
- Articles
- Type:
- artykuł w czasopiśmie wyróżnionym w JCR
- Published in:
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MONATSHEFTE FUR CHEMIE
no. 148,
pages 1685 - 1696,
ISSN: 0026-9247 - Language:
- English
- Publication year:
- 2017
- Bibliographic description:
- Nalazek-Rudnicka K., Wasik A.: Development and validation of an LC–MS/MS method for the determination of biogenic amines in wines and beers// MONATSHEFTE FUR CHEMIE. -Vol. 148, (2017), s.1685-1696
- DOI:
- Digital Object Identifier (open in new tab) 10.1007/s00706-017-1992-y
- Verified by:
- Gdańsk University of Technology
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