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Search results for: SIZE-EXCLUSION CHROMATOGRAPHY
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On Decision-Making Strategies for Improved-Reliability Size Reduction of Microwave Passives: Intermittent Correction of Equality Constraints and Adaptive Handling of Inequality Constraints
PublicationDesign optimization of passive microwave components is an intricate process, especially if the primary objective is a reduction of the physical size of the structure. The latter has become an important design consideration for a growing number of modern applications (mobile communications, wearable/implantable devices, internet of things), where miniaturization is imperative due to a limited space allocated for the electronic circuitry....
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Inverse modeling for fast design optimization of small-size rat-race couplers incorporating compact cells
PublicationIn the paper, a framework for computationally-efficient design optimization of compact rat-race couplers (RRCs) is discussed. A class of hybrid RRCs with variable operating conditions is investigated, whose size reduction is obtained by replacing ordinary transmission lines with compact microstrip resonant cells (CMRCs). Our approach employs a bottom-up design strategy leading to the development of compact RRCs through rapid design...
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Development of an Analytical Protocol for Determination of Cyanide in Human Biological Samples Based on Application of Ion Chromatography with Pulsed Amperometric Detection
PublicationA simple and accurate ion chromatography (IC) method with pulsed amperometric detection (PAD) was proposed for the determination of cyanide ion in urine, sweat, and saliva samples. The sample pretreatment relies on alkaline digestion and application of Dionex OnGuard II H cartridge. Under the optimized conditions, the method showed good linearity in the range of 1–100 μg/L for urine, 5–100 μg/L for saliva, and 3–100 μg/L for sweat...
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Direct solid phase microextraction combined with gas chromatography – Mass spectrometry for the determination of biogenic amines in wine
PublicationA direct method based on immersion solid phase microextraction (DI-SPME) gas chromatography mass-spectrometry (GC-MS) was optimized and validated for the determination of 16 biogenic amines in Polish wines. In the analysis two internal standards were used: 1,7-diaminoheptane and bis-3-aminopropylamine. The method allows for simultaneous extraction and derivatization, providing a simple and fast mode of extraction and enrichment....
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Specific cutting resistance while sawing of wood - the size effect
PublicationW artykule przedstawiono wyniki analiz zmian właściwego oporu skrawania, przy zastosowaniu współczesnej mechaniki pękania z uwzględnieniem wiązkości. Analizy wykonano dla procesu przecinania drewna na pilarce ramowej PRW15M drewna jesionu i jesionu modyfikowanego termicznie. Zastosowane podejście pozwala na wyjaśnienie zjawiska wzrostu właściwego powierzchniowego oporu skrawania dla niewielkich grubości warstwy skrawanej jako efektu...
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Feature type and size selection for adaboost face detection algorithm
PublicationThe article presents different sets of Haar-like features defined for adaptive boosting (AdaBoost) algorithm for face detection. Apart from a simple set of pixel intensity differences between horizontally or vertically neighboring rectangles, the features based on rotated rectangles are considered. Additional parameter that limits the area on which the features are calculated is also introduced. The experiments carried out on...
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Tighter bounds on the size of a maximum P3-matching in a cubic graph
PublicationW pracy pokazano, że największe P3-skojarzenie dla dowolnego grafu o n>16 wierzchołkach składa się z przynajmniej 117n/152 wierzchołków.
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Applications of compression techniques for reducing the size of multibeam sonar records
PublicationJednym z najczęściej używanych urządzeń służących do szeroko rozumianego telemonitoringu morskiego są sonary wielowiązkowe (ang. Multibeam systems - MBS). Ich wysoka wydajność w tworzeniu informacji o obiektach znajdujących się pod wodą skutkuje w dużych ilościach danych pozyskiwanych podczas rejsów badawczych i pomiarowych. W tym kontekście, proces przechowywania i zarządzania takim magazynem danych staje się istotnym problemem...
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The estimation of norwegian cod size distribution from acoustic data
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Potential of Mean Force of Hydrophobic Association: Dependence on Solute Size
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Risk-based explanation for the country-level size and value effects
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Body size and wing asymmetry in bees along an urbanization gradient
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Accelerometer-based Human Activity Recognition and the Impact of the Sample Size
PublicationThe presented study focused on the recognition of eight user activities (e.g. walking, lying, climbing stairs) basing on the measurements from an accelerometer embedded in a mobile device. It is assumed that the device is carried in a specific location of the user’s clothing. Three types of classifiers were tested on different sizes of the samples. The influence of the time window (the duration of a single trial) on selected activities...
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Analysis of size and shape of abrasive micrograins in lapping of assembly joints
PublicationPrzedstawiono skomputeryzowana analizę wielkości i kształtu mikroziaren ściernych. W badaniach mikroziaren węglika boru, węglika krzemu i elektrokorundu zastosowano mikroskopie optyczna oraz specjalistyczne oprogramowanie MultiScan v.6.08
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IFF/SSR rectangular patch antenna with reduced transversal size
PublicationW artykule przedstawiono antenę mikropaskową dla systemów IFF/SSR, zasilaną poprzez szczelinę typu H. Zastosowanie tego typu szczeliny pozwoliło na 36-procentową redukcję wymiaru poprzcznego anteny,co jest szczególnie istotne ze względu na potencjalne zastosowanie anteny w szykach.Pomierzone parametry eektryczne anteny to: VSWR < 1.5; stosunek polaryzacji ortogonalnej do właściwej < 30 dB w obu płaszczyznach;zysk > 7 dBi.
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FE-simulations of size effects in granular and quasi-brittle materials
PublicationW artykule przedstawiono symulacje efektów skali w materiałach granulowanych i kruchych. Obliczenia wykonano dla ściskania dwuosiowego i fundamentu w przypadku materiałów granulowanych oraz belek zginanych w przypadku materiałów kruchych. Do obliczeń wykorzystano mikropolarne prawo hipoplastyczne i sprężysto-plastyczne prawo z nielokalnym osłabieniem.
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Deterministic and statistical size effect during shearing of granular layer
PublicationArtykuł omawia deterministyczny i statystyczny efekt skali w materiałach granulowanych podczas ścinania cienkiej warstwy piasku między dwoma bardzo szorstkimi ścianami. Obliczenia wykonano metodą elementów skończonych na bazie mikropolarnego prawa hipoplastycznego. Pokazano wyniki efektu skali przy zastosowaniu różnych metod redukujących ilość realizacji pól losowych dla początkowego wskaźnika porowatości..
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Effect of particle size of aluminosilicate microspheres on the change of hydration heat of cement mortars and selected physical, chemical, and mechanical properties.
Open Research DataThis subject of the work is the study of selected properties of cement mortars containing two fractions of aluminosilicate microspheres with grain size in the range of 125 to 250 μm and from 250 to 500 μm. Mortar mixtures with ordinary Portland cement (OPC 42.5R) and three substitution rates of cement by microspheres, 1.5%, 3.5%, and 5.0%, were investigated....
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Sensitive determination of isoprostanes in exhaled breath condensate samples with use of liquid chromatography–tandem mass spectrometry
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Determination of Pesticide Residues in Honeybees using Modified QUEChERS Sample Work-Up and Liquid Chromatography-Tandem Mass Spectrometry
PublicationIncreasing emissions of chemical compounds to the environment, especially of pesticides, is one of factors that may explain present honeybee colony losses. In this work, an analytical method employing liquid chromatography-tandem mass spectrometry (LC-MS/MS) was optimized for the simultaneous screening of 19 pesticides which have not been yet determined in honeybee samples from northern Poland (Pomerania). The sample preparation,...
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Journal of Chromatography & Seperation Techniques
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Discrepancies in determination of biogenic amines in beer samples by reversed phase and hydrophilic interaction liquid chromatography coupled with tandem mass spectrometry
PublicationBiogenic amines (BAs) are nitrogenous organic bases occurring mainly in fermented food and beverages as a result of free amino acids bacterial decarboxylation. The reversed phase liquid chromatography (RPLC) and hydrophilic interaction liquid chromatography (HILIC) based methods were compared in terms of usefulness for determination of BAs in beer samples. Analysis of BAs with the use of RPLC method were carried out after their...
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Cost-Efficient EM-Driven Size Reduction of Antenna Structures by Multi-Fidelity Simulation Models
PublicationDesign of antenna systems for emerging application areas such as the Internet of Things (IoT), fifth generation wireless communications (5G), or remote sensing, is a challenging endeavor. In addition to meeting stringent performance specifications concerning electrical and field properties, the structure has to maintain small physical dimensions. The latter normally requires searching for trade-off solutions because miniaturization...
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Quantitative structure—retention relationship modeling of the retention behavior of selected antipsychotic drugs in normal-phase thin-layer chromatography
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Mechanical Properties, Microstructure and Surface Quality of Polypropylene Green Composites as a Function of Sunflower Husk Waste Filler Particle Size and Content
PublicationAgricultural waste is a still untapped source of materials that can, in case of proper utilization, significantly improve the sustainability of polymers and their composites. In this work, polymer composites based on isotactic polypropylene were produced incorporating ground sunflower husk in the amount of 10 wt% and 20 wt%. The work’s main objective is to evaluate how preliminary fractioning of this agricultural waste filler affects...
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Size and mass minimization of capacitor bank in a power converter DC line of DC drive with closed loop control system with PWM and current limitation
PublicationPaper deals with evaluation equations for power filter of AC-DC power converter which allows to provide size and mass minimization of capacitor bank in DC drive closed loop systems with PWM and current limitation. Reliability of provided equations is proved by simulation in MATLAB/Simulink
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EM-Driven Size Reduction and Multi-Criterial Optimization of Broadband Circularly-Polarized Antennas Using Pareto Front Traversing and Design Extrapolation
PublicationMaintaining small size has become an important consideration in the design of contemporary antenna structures. In the case of broadband circularly polarized (CP) antennas, miniaturization is a challenging process due to the necessity of simultaneous handling of electrical and field properties (reflection, axial ratio, gain), as well as ensuring sufficient frequency range of operation, especially at the lower edge of the antenna...
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Vibro-Electrical Behavior of a Viscoelastic Piezo-Nanowire in an Elastic Substrate Considering Stress Nonlocality and Microstructural Size-Dependent Effects
PublicationThis research deals with dynamics response of a Pol/BaTiO3 nanowire including viscosity influences. The wire is also impressed by a longitudinal electric field. Hamilton's principle and Lagrangian strains are employed in conjunction with a refined higher-order beam theory in order to derive equations of motion. By combining nonlocality and small size...
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Gradient reversed-phase high-performance chromatography of ionogenic analytes
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Chemometric analysis for optimizing derivatization in gas chromatography-based procedures
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Biopartitioning micellar electrokinetic chromatography – Concept study of cationic analytes
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Chiral gas chromatography as a tool for investigation into illicitly manufactured methamphetamine
PublicationW pracy przedstawiono zastosowanie gazowej chromatografii chiralnej do rozdzielania związków ubocznych powstających w trakcie syntezy metylamfetaminy. Opisano rozdzielanie enancjomerów efedryny, pseudoefedryny, chlorowanych związków posrednich i metylamfetaminy stosując do derywatyzacji bezwodniki fluorowanych kwasów. Jako fazę chiralną zastosowano CHIRALDEX B-DM. Do rozdzielenia enancjomerów pseudoefedryny oraz chlorowanych produktów...
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Sorption properties of asphaltene stationary phases for gas chromatography separations
PublicationW pracy przedstawiono wyniki badań nad możliwością wykorzystania faz stacjonarnych na bazie frakcji asfaltenowych do rozdzielania mieszanin związków chemicznych z wykorzystaniem chromatografii gazowej oraz porównano selektywność faz przygotowanych z frakcji asfaltenowych wyizolowanych z różnych surowców. Na podstawie uzyskanych wyników obliczono wartości liniowych indeksów retencji oraz stałych Rohrschneidera McReynoldsa, za pomocą...
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Determination of antifreeze substances in the airport runoff waters by solid-phase microextraction and gas chromatography–mass spectrometry method
PublicationA new method has been developed for the determination of antifreeze agents such as ethylene glycol (EG), propylene glycol (PG), and diethylene glycol (DEG) in the samples of airport runoff water. The method is based on headspace solid–phase microextraction (HS–SPME) of target analytes, which is coupled with gas chromatography–mass spectrometry (GC–MS). Until now, there was a lack of appropriate methodology for collecting reliable...
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Experimentally Aided Operational Virtual Prototyping to Predict Best Clamping Conditions for Face Milling of Large-Size Structures
PublicationVibrations occurring during milling operations are one of the main issues disturbing the pursuit of better efficiency of milling operations and product quality. Even in the case of a stable cutting process, vibration reduction is still an important goal. One of the possible solutions to obtain it is selection of the favorable conditions for clamping the workpiece to the machine table. In this paper, a method for predicting and...
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Monolithic capsule phase microextraction prior to gas chromatography-mass spectrometry for the determination of organochlorine pesticides in environmental water samples
PublicationIn this study, a capsule phase microextraction (CPME) protocol followed by gas chromatography-mass spectrometry is proposed for the accurate and sensitive monitoring of organochlorine pesticides (OCPs) in environmental water samples. Different monolithic sol–gel encapsulated sorbents were compared and monolithic sol–gel poly(ethylene glycol)-based sorbent incorporated into porous microextraction capsules resulted in the highest...
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Determination of Butyltin Species in Sea Water Samples Using Solid Phase Extraction Followed by Liquid Chromatography - Tandem Mass Spectrometry
PublicationReverse phase liquid chromatography (RP-HPLC)-electrospray ionization-tandem mass spectrometry (ESI-MS-MS) was evaluated for the analysis of TBT using solid phase extraction as sample preparation method. TBT was extracted from acidified water samples (spiked with tripropyltin as internal standard) using reversed phase polymeric Strata-X cartridges. Analytes were eluted from cartridges using acetonitrile-water mixture and the volume...
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Size control mechanism of ZnO nanoparticles obtained in microwave solvothermal synthesis
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Zeta potential and droplet size of n-tetradecane/ethanol (protein) emulsions
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Size-Dependent in Vitro Biocompatibility and Uptake Process of Polymeric Carbon Nitride
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Size matters everywhere: Decomposing the small country and small industry premia
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Determination of bisphenol A in size fractions of indoor dust from several microenvironments
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Evaluation of the structures size in the liquid-gas flow by gamma-ray absorption
PublicationThe rapid development of tomography methods particularly electrical, X and gamma rays allows for a wide range of the information about flow structure. However, all of such methods are quite complicated. At the same time much simpler systems as the measuring system of gamma rays absorption, allows to obtain a all key flow information which describe the two-phase flow. In the article the results of analyzes of radiometric signal...
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Size effects in problems of footings on sand within micro-polar hypoplasticity.
PublicationW artykule przedstawiono obliczenia efektów skali na nośność fundamentu na piasku. Obliczenia wykonano przy pomocy mikropolarnego prawa hipoplastycznego. W obliczeniach wykorzystano stochastyczne rozkłady początkowego wskaźnika porowatości według rozkładu Gaussa oraz różne wymiary fundamentu.
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Investigations of size effects in granular bodies during plane strain compression
PublicationArtykuł omawia deterministyczny i statystyczny efekt skali w materiałach granulowanych podczas ściskania w płaskim stanie odkształcenia. Obliczenia wykonano metodą elementów skończonych na bazie mikropolarnego prawa hipoplastycznego. Wykorzystano metodę hiperłacińskiego próbkowania w celu redukcji ilości realizacji.
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Investigations of size effect in tensile fracture of concrete using a lattice model
PublicationArtykuł przedstawia symulacje efektu skali w betonie podczas rozciągania przy zastosowaniu nowego modelu siatkowego. Zbadano wpływ rozkładu i wielkości kruszywa oraz wpływ strefy kontaktu na efekt skali.
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Experimental investigations of size effect in reinforced concrete beams failing by shear
PublicationW artykule omówiono wyniki doświadczalne efektu skali w zbrojonych betonowych belkach niszczących się przez ścinanie. Doświadczenia wykonano dla belek o różnych wymiarach ze zbrojeniem stalowym i bazaltowym. Podczas doświadczeń pomierzono siłę oraz szerokości lokalizacji i rys. Wyniki porównano z modelem skali wg Bazanta.
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Multi-objective design optimization of antennas for reflection, size, and gain variability using kriging surrogates and generalized domain segmentation
PublicationCost-efficient multi-objective design optimization of antennas is presented. The framework exploits auxiliary data-driven surrogates, a multi-objective evolutionary algorithm for initial Pareto front identification, response correction techniques for design refinement, as well as generalized domain segmentation. The purpose of this last mechanism is to reduce the volume of the design space region that needs to be sampled in order...
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An Experimentally Aided Operational Virtual Prototyping to Obtain the Best Spindle Speed during Face Milling of Large-Size Structures
PublicationAbstract: The paper presents an original method concerning the problem of vibration reduction in the general case while milling large-size and geometrically complex details with the use of an innovative approach to the selection of spindle speed. A computational model is obtained by applying the so-called operational approach to identify the parameters of the workpiece modal model. Thanks to the experimental modal analysis results,...
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Determination of flavanols by liquid chromatography with fluorescence detection. Application to the characterization of cranberry-based pharmaceuticals through profiling and fingerprinting approaches
PublicationIn this work, a new method based on reversed-phase high-performance liquid chromatography (HPLC) with fluorescence detection (FLD) was established for the determination of catechins and related oligomeric proanthocyanidins (PACs) in cranberry-based pharmaceuticals. Compounds were recovered by liquid extraction using methanol/water/hydrochloric acid (60:39:1, v:v:v) as the extraction solvent. The chromatographic separation was carried...