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Chromogenic Macrocyclic Derivatives of Azoles - Synthesis and Properties
PublicationOpisano syntezę makrocyklicznych azokoron zawierających resztę pirolu i imi-dazolu w makropierścieniu. Zbadano zdolność kompleksowania kationów metaliprzez otrzymane związki makrocykliczne przy pomocy spektrofotometrii UV-Visw acetonitrylu. Zbadano także właściwości jonoforowe związków w membranowychelektrodach jonoselektywnych. Ustalono strukturę krystalograficzną 18-czło-nowej pochodnej pirolu.
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Acylic congener of cucurbituril: synthesis and recognition properties.
PublicationZaprezentowano syntezę analogów acyklicznych cucurbiturilu oraz ich zdolności do kompleksowania wybranych 16 amin, dioli, kwasów dikarboksylowych, pochodnych guanidyny oraz pirydyny. Obserwowane tworzenie kompleksów przebiegało około 180 razy słabiej niż dla cucurbiturilu. Wyniki te świadczą o potencjalnych możliwościach zbliżonych do analogów cyklicznych pod względem tworzenia kompleksów i rozpoznawania wyżej wymienionych...
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Experimental evaluation of the PLC-controlled drives properties.
PublicationPrzedstawiono strukturę stanowiska laboratoryjnego do testów oprogramowania PLC do sterowania napędami oraz do prowadzenia eksperymentalnych prób takich napędów. Omówiono zasady prowadzenia testów oprogramowania przed i w trakcie uruchamiania napędu. Przedstawiono przykładowe rezultaty doświadczeń.
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On direct detection of entanglement properties of unknown states
PublicationPrzystępnie omówiono detekcję własności splątania kwantowych stanów. Uwzględniono zarówno detekcje o charakterze jakościowym jak i ilościowym.
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Structural and electronic properties of diamond-composed heterostructures
PublicationDiamond is a promising material for 21st century electronics due to its high thermal and electronic conductivity, biocompatibility, chemical stability, high wear resistance, and possibility of doping. However, the semiconductor properties of diamond, especially free-standing films, have not been fully explored. Nor have their integration with polymers and fragile materials and their applications as electronic components. In this...
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SYNTHESIS AND PROPERTIES OF OLIGOMERS WITH HYDROXY END-GROUPS
PublicationMethods of oligomers (polymers) with hydroxy end-groups obtaining are examined. The synthesis of hydroxy-containing oligomers based on epoxy resins is of special attention. The molecules of mentioned oligomers apart from free primary and secondary hydroxy groups contain epoxy, peroxy, carboxy or acrylic groups.
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Properties of Composite Oxide Layers on The Ti13Nb13Zr Alloy
PublicationThe development of composite oxide layers on the Ti13Nb13Zr alloy, their structure and properties have been demonstrated. Two subsequent methods were applied to prepare the composite layers. During the first stage gas oxidation produced a solid oxide layer, and subsequently oxide nanotubes were produced by using an electrochemical method. Scanning electron microscopy (SEM), chemical analysis, energy dispersive X-ray spectroscopy...
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Properties of Vacuum Sintered Duplex Stainless Steels
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Pressure effects on the luminescence properties of CaWO4:Pr3+
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Properties of vacuum sintered duplex stainless steels
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Properties of Vacuum Sintered Duplex Stainless Steels
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Sintered Duplex Stainless Steels Corrosion Properties
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Sintered Duplex Stainless Steels Corrosion Properties
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Spectroscopic properties of the Ce-doped borate glasses
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Water properties in pâtés enriched with potato juice
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Porphyrazines with peripheral isophthaloxyalkylsulfanyl substituents and their optical properties
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The chitosan – Porphyrazine hybrid materials and their photochemical properties
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Synthesis, spectroscopic and photophysical properties of novel styryldiazepinoporphyrazine
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Chromogenic macrocyclic derivatives of azoles - synthesis and properties,
PublicationNew azocrown ethers comprising imidazoles in the macrocycle have been synthesized. Imidazole, 2-methyl-, 4-methyl-, and 4-phenylimidazole were incorporated to form macrocyclic units by coupling with the appropriate bis-diazonium salts. The syntheseswere performed under high dilution conditions. The X-ray structure of a water adduct of the 21-membered crown ether derivative of 4-methylimidazole 8 has been solved. Metal...
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Test Stand for Metamaterials Dynamic Properties Examination
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Properties of corn starch subjected hydrothermal modification
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Heteropolyanions doped polyimine—Preparation and spectroscopic properties
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Selected properties of acetylated adipate of retrograded starch
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Properties of lithium aluminate for application as an OSL dosimeter
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Production and Properties of Starch Citrates—Current Research
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Preparation and characterization of biopolymeric films with magnetic properties
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Magnetic properties of the garnet and glass forms of Mn3Al2Si3O12
PublicationPrezentujemy wyniki pomiarow podatności magnetycznej i ciepła właściwego dla Mn3Al2Si3O12 w formie krystalicznej i amorficznej. W ten sposób przeprowadzamy porównania stopnia magnetycznej frustracji dla obu form tego samego związku chemicznego.
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The influence of frequency separation on imaging properties in DFEIT
PublicationW artykule przedstawiono wpływ wyboru składowych częstotliwościowych dla różnicowej tomografii impedancyjnej na wynik i własności obrazowania w dwuczęstotliwościowej różnicowej tomografii impedancyjnej.A Dual Frequency EIT is an extension of a traditional EIT that uses two sinusoidal signals for imaging. Appropriate selection of signals' frequency allows to achieve reasonable contrast of imaged structure. It has already been shown...
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Electrical properties of polymer coatings modified with nanoadditives
PublicationW pracy przedstawiono właściwości elektryczne (antystatyczne, rezystancję powierzchniową) polimerowych powłok. Pokazano wpływ różnych domieszek na czasy rozładowania się warstwy oraz na jej rezystancję powierzchniową.
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Microstructure and Dielectric Properties of Barium-vanadate Glasses
PublicationThe ac and dc conductivity in barium-vanadate glasses was investigated as a function of temperature and frequency with the use of impedance spectroscopy. The topography and microstructure of glasses were investigated by the means of X-ray diffraction (XRD) and scanning electron microscopy (SEM) methods. The XRD results show that all samples are amorphous but microscopy investigation reveals that glasses with greater amount of V2O5...
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Measurements of fundamental properties of homogeneous tissue phantoms
PublicationWe present the optical measurement techniques used in human skin phantom studies. Their accuracy and the sources of errors in microscopic parameters’ estimation of the produced phantoms are described. We have produced optical phantoms for the purpose of simulating human skin tissue at the wavelength of 930 nm. Optical coherence tomography was used to measure the thickness and surface roughness and to detect the internal inhomogeneities....
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Microstructure and electrical properties of manganese borosilicate glasses
PublicationThe structure, optical and electrical properties of manganese borosilicate glasses of the composition xMnO–(80 − x)SiO 2 –20B 2 O 3 (x = 40, 50, and 60 mol%) were investigated. The dependence of the glass structure on its composition was discussed and related to electrical properties. A separation of two amorphous phases was observed. It was suggested that one phase is MnO-rich and the other is SiO 2 -rich. It was found that...
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Optical photoluminescent, and electroluminescent properties of organic solids
PublicationThis chapter discusses optical, photoluminescence and electroluminescence properties of organic materials. First, the spectral features of individual molecules and molecular solid states are analysed. Next, the excitonic processes in organic materials are discussed. The chapter reviews experimental methods leading to the determination of basic excitonic parameters. Finally, the electroluminescence phenomena in organic materials...
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A new method for measuring the psychoacoustical properties of tinnitus
Publicationinformation, select the tinnitus treatment and quantitatively substantiate its effects, the measurement of the Tinnitus psychoacoustic parameters should be made an inherent part of the Tinnitus therapy. Methods For this purpose the multimedia-based sound synthesizer has been proposed for testing tinnitus and the results obtained this way are compared with the outcome of the audiometer-based Wilcoxon test. The method has been verified...
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Electrical and structural properties of Nb-doped SrTiO3
PublicationNiobium-doped strontium titanate synthesized via conventional solid-state reaction has been studied. Influence of niobium content on the lattice parameters and electrical conductivity has been reported. Various reduction conditions have been investigated. For samples reduced in hydrogen at 1400°C, a transition from thermally activated to metallic behavior has been observed. Maximum electrical conductivity (ca. 55 Scm−1 at 650°C)...
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Manufacture and research of TPS/PE biocomposites properties
PublicationIn this paper the process of native starch preparing for modification by extrusion and manufacture of biocomposites is presented. The first aim of this study was to determine the mixing and granulating condition of native starch to obtain granulated native starch. For mixing and granulation of native starch Intensive Mixer manufactured by Maschinenfabrik Gustav Eirich was used. Mixing and granulation in a single process is a new...
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Properties of dimension witnesses and their semidefinite programming relaxations
PublicationIn this paper we develop a method for investigating semi-device-independent randomness expansion protocols that was introduced in Li et al. [H.-W. Li, P. Mironowicz, M. Pawłowski, Z.-Q. Yin, Y.-C. Wu, S. Wang, W. Chen, H.-G. Hu, G.-C. Guo, and Z.-F. Han, Phys. Rev. A 87, 020302(R) (2013)]. This method allows us to lower bound, with semi-definite programming, the randomness obtained from random number generators based on dimension...
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Synthesis, single crystal growth and properties of Sr5Pb3ZnO12
PublicationAbstract The novel Sr5Pb3ZnO12 oxide was synthesized by the solid-state reaction method. The crystal structure was studied by means of the powder x-ray diffraction Rietveld method and was found to be similar to 3 other previously known Sr5Pb3MO12 compounds (M = Co, Ni, Cu). Crystals of several hundred microns in size of the new phase were grown in molten sodium chloride and imaged using confocal optical and scanning electron microscopy....
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A LABORATORY STAND FOR THE ANALYSIS OF DYNAMIC PROPERTIES OF THERMOCOUPLES
PublicationIn the present elaboration, problems connected with measurements of high variable temperatures of gases are introduced and the impact of dynamic properties of different construction solutions of thermoelements on the accuracy of the measurements is considered. A laboratory stand built within research under doctoral thesis, destined for analysis of dynamic properties of thermocouples is also described. Results of numerical simulation...
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Nonlinear properties of the Gotland Deep – Baltic Sea
PublicationThe properties of the nonlinear phenomenon in water, including sea water, have been well known for many decades. The feature of the non homogeneous distribution of the speed of sound along the depth of the sea is very interesting from the physical and technical point of view. It is important especially in the observation of underwater area by means of acoustical method ( Grelowska et al ., 2013; 2014). The observation of the underwater...
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Piezoresistive properties of cement composites with expanded graphite
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Synthesis, characterization and photocatalytic properties of lithium tantalate
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Effect of basalt powder addition on properties of mortar
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Electronic Properties of Multiwall Boron Nitride Nanotubes
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Elasto-viscoplastic properties of AA2017 aluminium alloy
PublicationArtykuł opisuje procedurę identyfikacji parmetrów materiałowych dla sprężysto-lepkoplastycznego modelu Bodnera-Partoma. Prezentowane są symulacje numeryczne testów jednoosiowego rozciągania z różnymi prędkościmi odkształcenia, które porównane są z wynikami eksperymantalnymi.
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Modelling of the viscoelastic properties of the technical fabric VALMEX
PublicationThe analysis of the Burgers model used for the constitutive description of the technical fabric VALMEX vis-coelastic behavior is presented. It has revealed that the correctness of the identification depends strongly on the level of the immediate strain taken for calculations. Moreover, it has been proven that the Burgers model can be used for modelling of the viscoelastic properties of the polyester reinforced PVC coated VALMEX...
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SOME CONVERGENCE PROPERTIES OF THE SUM OF GAUSSIAN FUNCTIONALS
PublicationIn the paper, some aspects of the convergence of series of dependent Gaussian sequences problem are solved. The necessary and sufficient conditions for the convergence of series of centered dependent indicators are obtained. Some strong convergence results for weighted sums of Gaussian functionals are discussed.
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Synthesis and Spectroscopic Properties of New Bis-tetrazoles
PublicationSyntheses of N,N'-phenyltetrazole podands link with aliphatic chains containing oxygen, nitrogen and sulphur atoms, are described. The complexing properties of these compounds towards metal cations (Fe2+, Cu2+, Zn2+, Co2+, Ni2+) were investigated by absorption and infrared spectroscopy. The UV-Vis titrations were performed to estimate the stability constant values of the respective complexes with Cu2+ ion. Changes in UV-Vis absorption...
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Measurements of transmission properties of Acoustic Communication Channels
PublicationTough transmission properties of shallow water acoustic channels (SWAC) highly limit the use of underwater acoustic communication (UAC) systems. An adaptive matching of modulation and signaling schemes to instantaneous channel conditions is needed for reliabledata communications. This creates, however, unique challenges for designers when compared to radio transmission systems. When communication system elements are in move, the...
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Analysis of Properties of an Active Linear Gesture Sensor
PublicationBasic gesture sensors can play a significant role as input units in mobile smart devices. However, they have to handle a wide variety of gestures while preserving the advantages of basic sensors. In this paper a user-determined approach to the design of a sparse optical gesture sensor is proposed. The statistical research on a study group of individuals includes the measurement of user-related parameters like the speed of a performed...