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Search results for: coumarone-indene resin
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Obtaining of coumarone-indene resins based on light fraction of coal tar.1. Coumarone-indene resins with carboxy groups
PublicationCoumarone-indene resins (CIR) with carboxy groups were synthesized via cooligomerization of unsaturated compounds presented in ligh fraction of coal tar and its fraction boiling out within 423-463 K with the addition of such industrial monomers as styrene, maleic anhydride, glycidyl methacrlate and methacryclic acid. 2,2-azobs 92-methylpropionitrile) in the form of 0,2 M solution in toluene was used as an initiator. The effect...
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Obtaining of coumarone-indene resins based on light fraction of coal tar 2. Coumarone-indene resins with epoxy groups
PublicationCoumarone-indene resins (CIR) with carboxy groups were synthesized via cooligomerization of unsaturated compounds presented in light fraction of coal tar and its fraction boiling out within 423–463 K with the addition of such industrial monomers as styrene, maleic anhydride, glycidyl methacrylate and methacrylic acid. 2,2`-Azobis(2-methylpropionitrile) in the form of 0.2 M solution in toluene was used as an initiator. The effect...
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OBTAINING OF COUMARONE-INDENE RESINS BASED ON LIGHT FRACTION OF COAL TAR 3. COUMARONE-INDENE RESINS WITH METHACRYLIC FRAGMENTS
PublicationThe method for obtaining coumarone-indene resins with methacrylic fragments (CIRM) was developed with the addition of methyl ethacrylate, using a light fraction of coal tar and its fraction boiling within 423–463 К. CIRM was obtained via radical cooligomerization using 2,2'-azobis (2-methyl-propionitrile) as the initiator. The effect of the initiator amount, temperature and reaction time on the yield, softening temperature and...
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Obtaining of Coumarone-Indene Resins Based on Light Fraction of Coal Tar. 4. Bitumen-Polymer Blends with Participation of Coumarone-Indene Resins with Epoxy Groups
PublicationUsing light fraction of coal tar (5.75 wt % of coumarone and 44.45 wt % of indene), glycidyl methacrylate and styrene, the coumarone-indene resin with epoxy groups (CIRE) has been synthesized. Monoperoxy derivative of diglycidyl ether Bisphenol A (PO) was used as an initiator. The possible formation of CIRE has been studied on the model systems consisting of PO, glycidyl methacrylate, indene or coumarone, or styrene, or mixture...
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Optical properties of daylight curable resin doped with nanodiamond powder
PublicationIn this paper a new material for 3D printing was elaborated on. Since diamond has very good optical properties, an idea occurred to us to apply it in 3D printing process. A mixture of nanodiamond powder and a standard 3D printing resin was created and several printouts have been completed. They have been tested for their abilities to transmit and absorb light in a wide spectrum of wavelengths. It turned out that the nanopowder...
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Investigation of MIEX® resin sedimentation in the aspect of particle sizes remaining in the supernatant
PublicationThe aim of the study was to evaluate the effectiveness of the MIEX® resin sedimentation process, both new and repeatedly used in hybrid water treatment MIEX®DOC + microfiltration (MF) or ultrafiltration (UF) processes (repeatedly regenerated). The tests consisted of performing 1 h sedimentation of the suspension resin in nonflow conditions and analysis of supernatant water at different process durations. The suspension weight analysis...
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Identification of 1H‐indene‐(1, 3, 5, 6)‐tetrol derivatives as potent pancreatic lipase inhibitors using molecular docking and molecular dynamics approach
PublicationPancreatic lipase is a potential therapeutic target to treat diet-induced obesity in humans, as obesity-related diseases continue to be a global problem. Despite intensive research on finding potential inhibitors, very few compounds have been introduced to clinical studies. In this work, new chemical scaffold 1H-indene-(1,3,5,6)-tetrol was proposed using knowledge-based approach, and 36 inhibitors were derived by modifying its...
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Production of fuel briquette from solid waste biomass using natural resin as a binder
PublicationAbstract Background: This research aimed to evaluate the use of natural resin as a binder for the production of fuel briquette from solid waste biomass. Methods: Proximate analyses were made for fuel briquette prepared from solid waste biomass using natural resin as a binder in comparison with using starch as a binder. Results: The results for density, percent content of moisture, percent content of volatile matter, percent content...
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Production of fuel briquette from solid waste biomass using natural resin as a binder
PublicationBackground: This research aimed to evaluate the use of natural resin as a binder for the production of fuel briquette from solid waste biomass.Methods: Proximate analyses were made for fuel briquette prepared from solid waste biomass using natural resin as a binder in comparison with using starch as a binder.Results: The results for density, percent content of moisture, percent content of volatile matter, percent...
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Mechanical Properties of Bio-Composites Based on Epoxy Resin and Nanocellulose Fibres
PublicationThe aim of our research was to investigate the effect of a small nanocellulose (NC) addition on an improvement of the mechanical properties of epoxy composites. A procedure of chemical extraction from pressed lignin was used to obtain nanocellulose fibers. The presence of nanoparticles in the cellulose pulp was confirmed by FTIR/ATR spectra as well as measurement of nanocellulose particle size using a Zetasizer analyzer. Epoxy...
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Paint and Resin Times
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Pigment & Resin Technology
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Slurry Surfacing Mixes on the Basis of Bitumen Modified with Phenol-Cresol-Formaldehyde Resin
PublicationSlow-breaking monophase cationic bitumen emulsions have been produced on the basis of bitumen modified with phenol-cresol-formaldehyde resin (PhCR-F). Bitumen emulsions were used as a binder for thin-layer coatings with slurry surfacing mixes (SSM). Physical and technical parameters of modified and unmodified emulsions were determined and analyzed. The optimal compositions of SSM were selected according to the breaking criterion....
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Epoxy Composites Filled with Natural Calcium Carbonate. 1. Epoxy Composites Obtained in the Presence of Monoperoxy Derivative of Epidian-6 Epoxy Resin
PublicationPhysico-mechanical properties of the products based on filled epoxy-oligomeric mixtures composed of Epidian-5 epoxy resin, oligoesteracrylate TGM-3 and monoperoxide derivative of Epidian-6 epoxy resin (PO) have been investigated. CaCO3 was used as a filler and polyethylene polyamine was a curing agent. The effect of PO and CaCO3 on the gel-fraction content and physico-mechanical properties was examined. Using a scanning electron...
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RP-HPLC WITH DETECTION BY MEANS OF ESI-MS AND UV FOR IDENTIFICATION OF CHROMATOGRAPHIC PEAKS OF SOME HYDROXY DERIVATIVES OF EPOXY RESIN
PublicationThe composition of products synthesized on the basis of ED-24 epoxy resin has been studied using a reversed phase high-performance liquid chromatography followed by an electrospray ionization mass spectrometry (RP-HPLC/ESI-MS). The synthesized products contain free hydroxy groups and such groups, as epoxy, peroxy, carboxy or acrylate.
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Volatile Compound Emissions from Stereolithography Three-Dimensional Printed Cured Resin Models for Biomedical Applications
PublicationStereolithography three-dimensional printing is used increasingly in biomedical applications to create components for use in healthcare and therapy. The exposure of patients to volatile organic compounds (VOCs) emitted from cured resins represents an element of concern in such applications. Here, we investigate the biocompatibility in relation to inhalation exposure of volatile emissions of three different cured commercial resins...
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Impact Behaviour of Glass Fribre /Epoxy Composites with Nano-Enhanced Resin after Water Exposure
PublicationImpact behaviour of glass fibre /epoxy composites with nano- SiO2 modified resin was studied in terms of low velocity impact after water exposure. Nanocomposites with 1%, 2%, 3% 5% 7% nano-SiO2 (Nanopox- Evonic) were investigated. Peak impact load and impact damage area as a function of nanoparticle contents were compared for dry specimens and for samples exposed to water (0.7 %wt. 1.7% water absorbed) at 1J, 2J 3J impact energies....
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Effect of Surface Treatment of Halloysite Nanotubes (HNTs) on the Kinetics of Epoxy Resin Cure with Amines
PublicationThe epoxy/clay nanocomposites have been extensively considered over years because of their low cost and excellent performance. Halloysite nanotubes (HNTs) are unique 1D natural nanofillers with a hollow tubular shape and high aspect ratio. To tackle poor dispersion of the pristine halloysite (P-HNT) in the epoxy matrix, alkali surface-treated HNT (A-HNT) and epoxy silane functionalized HNT (F-HNT) were developed and cured with...
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Synthesis and application of oligomer with hydroxy groups based on peroxy derivative of ED-24 epoxy resin and POLYTHF-2000 oligoether
PublicationNew oligomer with peroxy, primary and secondary hydroxy groups has been synthesized on the basis of peroxy derivative of ED-24 epoxy resin (PO) and PolyTHF-2000 oligoether according to the developed procedure. The effect of the catalysts nature and amount, temperature and process time on the reaction rate has been studied. Benzyltriethylammonium chloride, potassium hydroxide,1,4-diazobicyclooctane and the mixture composed of benzyltriethylammonium...
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Golden artefacts, resin figurines, body adhesives and tomb sediments from the pre-Columbian burial site El Caño (Gran Coclé, Panamá): tracing organic contents using molecular archaeometry
PublicationThis research aimed to determine the origin of organic residues from funerary contexts in the El Ca~no settlement (Gran Cocl�e area, Panam�a, Central America) by means of multiple molecular probing techniques (GC-MS of organic solvent extracts and pyrolysis-GC-MS, THM-GC-MS and FTIR of solid samples). The samples include particles of precious resin figurines, fillings of golden objects, tomb sediments, plant exudates from extant...
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Kinetics of Cross-Linking Reaction of Epoxy Resin with Hydroxyapatite-Functionalized Layered Double Hydroxides
PublicationThe cure kinetics analysis of thermoset polymer composites gives useful information about their properties. In this work, two types of layered double hydroxide (LDH) consisting of Mg2+ and Zn2+ as divalent metal ions and CO32− as an anion intercalating agent were synthesized and functionalized with hydroxyapatite (HA) to make a potential thermal resistant nanocomposite. The curing potential of the synthesized nanoplatelets in the...
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Adsorption of carbon dioxide on phenolic resin-based carbon spheres
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Influence of Storage Time and Temperature on the Toxicity, Endocrine Potential, and Migration of Epoxy Resin Precursors in Extracts of Food Packaging Materials
PublicationThe aim of the present study was to establish a standard methodology for the extraction of epoxy resin precursors from several types of food packages (cans, multi-layered composite material, and cups) with selected simulation media (distilled water, 5% ethanol, 3% dimethyl sulfoxide, 5% acetic acid, artificial saliva) at different extraction times and temperatures (factors). Biological analyses were conducted to determine the acute...
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Current-Voltage Characteristics of the Composites Based on Epoxy Resin and Carbon Nanotubes
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Synthesis and characterization of resorcinol–formaldehyde resin chars doped by zinc oxide
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Effect of nanosilica on characteristics of carbonizates of phenol-formaldehyde resin – Fe(acac)3
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Curing epoxy resin with anhydride in the presence of halloysite nanotubes: the contradictory effects of filler concentration
PublicationEpoxy resins can be cured with a wide variety of curing agents such as amines and anhydrides, but anhydride curing would be more favorable for research purpose because of epoxy-anhydride curing taking place slowly at room temperature. Incorporation of natural nanosized minerals into epoxy is of environmental importance. Halloysite nanotubes (HNTs) display chemical properties similar to those of silica and alumina, and hydroxyl...
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Production of fuel briquette from solid waste biomass using natural resin as a binder
Publication10.34172/EHEM.2022.xx
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The Tribological, Physico-Chemical and Rheological Properties of Lubricating Grease Produced on Epoxy Resin Base
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The Effect of Texturing of the Surface of Concrete Substrate on the Pull-Off Strength of Epoxy Resin Coating
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Engineering and Manufacturing Technology of Green Epoxy Resin Coatings Modified with Recycled Fine Aggregates
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The Effect of Recycled Fine Aggregate Sourced from Construction and Demolition Waste on the Properties of Epoxy Resin Coatings
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Rhenium Nanostructures Loaded into Amino-Functionalized Resin as a Nanocomposite Catalyst for Hydrogenation of 4-Nitrophenol and 4-Nitroaniline
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Structural, thermal and energetic characteristics of synthetic active carbons prepared on the basis of ion-exchange resin Amberlite IRC 84
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Hecheng Shuzhi Ji Suliao/China Synthetic Resin and Plastics
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Polyhydric SiO2 coating assistant to graft organophosphorus onto glass fabric for simultaneously improving flame retardancy and mechanical properties of epoxy resin composites
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Textural Characteristics of Resorcinol—Formaldehyde Resin and Temperature Behavior of Bound Water Affected by Co-Adsorbed Trifluoroacetic Acid or Pyridine in Weakly Polar Organic Media
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Retinit im mittleren Geiseltal und in Nordwestsachsen
PublicationEs werden historische fossile Harzfunde, bekannt unter dem Namen Retinit, aus ehemaligen Braunkohlenvorkommen in Nordwestsachsen und dem Geiseltal beschrieben. Die Harzproben aus dem Geiseltal wurden mittels Infrarotspektrometer untersucht. Der Vergleich der Spektren mit Referenzspektren zeigt, dass es sich bei den „historischen“ Harzproben um ein Harz vom Retinit- Typ, den oxidierten Krantzit (Oxikrantzit), handelt.
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Laser granulometer as an useful tool for selection of appropriate membranes used in the MIEX®DOC-UF/MF hybrid process
PublicationIn the study, particle size distribution of the MIEX® resin was presented. Such analyses enable to determinate whether presence of fine resin fraction may be the reason for unfavorable membrane blocking during water purification by the hybrid MIEX®DOC-microfiltration/ultrafiltration systems. Granulometric analysis of resin grains using the laser diffraction particle size analyzer (laser granulometer) was carried out as well as...
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Valorisation of bioplastics synthesised by liquefaction of celluloseusing hetero- and homogeneous catalysts
Open Research DataThe purpose of the present study was to test the effectiveness of a heterogeneous catalyst such as Nafion ion-exchange resin on the cellulose liquefaction process. The results obtained were compared with the bio-polyols obtained in a conventional way, using a homogeneous catalyst (sulfuric acid (VI)). Depending on the catalyst used and the temperature...
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Cross-linked epoxy-isocyanate blends containing Epidian-6 modified by glycols
PublicationPolymeric films of cross-linked structure may be formed using epoxy-isocyanate blends composed of Epidian-5 epoxy resin, 4,4’-diphenylmethanediisocyanate (MDI), Z-1 polyamine hardener and Epidian-6 epoxy resin modified by glycols. The effect of the component natures and ratio, process temperature and time on the gel-fraction content, as well as film hardness, was examined. The chemistry of the film forming process was determined...
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Toughness augmentation by fibrillation and yielding in nanostructured blends with recycled polyurethane as a modifier
PublicationIn the present paper, we have carefully investigated the morphology and fracture mechanism of the recycled polyurethane (RPU) /epoxy blend system. The second phase (RPU) added to the epoxy resin has a positive effect on the overall mechanical properties. Interestingly, the recycled polymer has a remarkable effect on the fracture toughness of epoxy resin. The mechanism behind the fracture toughness improvement up on the addition...
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Cross-linking of epoxy-oligomeric mixtures in the presence of modified phenol-formaldehyde resins
PublicationCross-linking of epoxy oligomeric mixtures consisting of industrial epoxy resin ED-20, oligoetheracrylate TGM-3, peroxide derivative of epoxy resin ED-24 and phenol-formaldehyde oligomer with unsaturated methacrylate fragments or peroxide groups was studied in the presence of polyethylenepolyamine at room temperature and heated to 383, 403 or 423 K for 15, 30, 45, 60 and 75 minute. The influence of mixture composition, temperature...
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Badanie odporności na poślizg posadzkowych powłok żywicznych
PublicationW artykule przedstawiono badania wskaźnika szorstkości (odporności na poślizg) posadzki wykonanej z powłok żywicznych za pomocą wahadła angielskiego. Omówiono wybrane metody określania właściwości antypoślizgowych posadzek wraz z przeglądem literatury.
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Development of nanoscale morphology and role of viscoelastic phase separation on the properties of epoxy/recycled polyurethane blends
PublicationA novel and cost-effective approach towards the modification of epoxy matrix has been developed using recycled polyurethane for the first time without sacrificing any of the intrinsic properties of the resin. Polyurethane, recycled from waste foam by glycolysis process (RPU), was found to be very effective in improving the properties of the thermosetting resin based on Diglycidyl ether of bisphenol-A (DGEBA). The effect of the...
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Environmental Degradation of Ramie Fibre Reinforced Biocomposites
PublicationThe degradation process of two kinds of biocomposites, Ramie fibre/Ecoflex R/E and ramie fibre/cellulose nanofibre reinforced corn starch resin R/CS, were studied. It was demonstrated that R/CS degraded faster in natural environments.
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Emission and properties of airborne wear particles from train brake friction materials based on novolac phenolic resins and butadiene rubbers
PublicationThe emission of airborne particulate matter from a train brake depends on the formulation of its friction material. This study investigates the emission and properties of wear particles from train brake friction materials based on straight or resorcinol-modified novolac phenolic resin and nitrile or styrene butadiene rubber used as binding ingredients. The wear particles are generated by a pin-on-disc tribomachine inside an aerodynamic...
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New Transparent Flame-Retardant (FR) Coatings Based on Epoxy-Aluminum Hypophosphite Nanocomposites
PublicationThe present study investigated the flame-retardant (FR) effect of transparent epoxy coating containing aluminum hypophosphite (AHP) nanoparticles (NPs) on polylactic acid (PLA) sheets used as a typical model of combustible polymeric material. First, AHP NPs (≤60 nm) were prepared by a specific two-stage wet milling process and deeply analyzed (morphology, thermal/mechanisms of degradation under nitrogen and air). The thermal properties...
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Design of poroelastic wearing course with the use of direct shear test
PublicationPoroelastic Road Surfaces (PERS) are characterized by porous structure with at least 20% of air void content and stiffness almost 10 times lower than typical asphalt course. Such properties enable noise reduction up to 12 dB in comparison to SMA 11 mixture. However, the main disadvantage of previously used poroelastic mixtures, based on resin type binders, was their low durability, which resulted in raveling and delamination from...
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The application of a photopolymer material for the manufacture of machine elements using rapid prototyping techniques
PublicationThe paper discusses the application of polymer resin for 3D printing. The first section focuses on rapid prototyping technique and properties of the photopolymer, used as input material in the manufacture of machine components. Second part of the article was devoted to exemplary 3-D-printed elements for incorporation in machines. The article also contains detailed description of problems encountered in implementation of the selected...