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Search results for: Chemistry of wine
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Remarks on use of the term “deep eutectic solvent” in analytical chemistry
PublicationAbout 20 years ago, Abbott and co-workers researched new solvents that were based on mixtures of choline chloride with urea and carboxylic acids and that were liquid at ambient temperature. The term “deep eutectic solvent” (DES) was later adopted for similar mixtures. As DESs have a number of interesting features, they quickly attracted the attention of researchers and found application in various branches of chemical and materials...
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Green Analytical Chemistry: Summary of Existing Knowledge and Future Trends
PublicationAnalysis of recent publications in green analytical chemistry shows the current trends and future needs in this area. The main issues are related with search for cheaper, more efficient, more accurate, greener and miniaturized alternatives. Miniaturization is perhaps, the most notable current trend in analytical chemistry. Rapid developments and improvements in instrumentation have led to impressive range of benchtop technology...
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Influence of drying mode and feed per tooth rate on the fine dust creation in pine and beech sawing on a mini sash gang saw
PublicationThe experimental results of the study focused on the effect of drying processes of modified air drying and warm air steam mixture drying of pine and beech wood on the size of sawdust particles created in cutting using PRW-15M sash gang saw, are presented in the paper. Particle size analysis of dry sawdust was performed using two methods—sieving method and laser diffraction analysis. The results showed that the drying process did...
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The effect of full-cell impregnation of pine wood (Pinus Sylvestris L.) on the fine dust content during sawing on a frame sawing machine
PublicationIn this paper the results of the analysis of the effect of the impregnation treatment of pine wood on the granularity of sawdust from the sawing process on the frame sawing machine PRW 15M are presented. Granulometric analyses of chips from impregnated and unimpregnated pine wood implies that the impregnation of pine wood does not affect the size and structure of the sawdust produced. A major ≈ 95% share of the formed chips is...
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On-Line Partitioning for On-Line Scheduling with Resource Conflicts
PublicationWithin this paper, we consider the problem of on-line partitioning the sequence of jobs which are competing for non-sharable resources. As a result of partitioning we get the subsets of jobs that form separate instances of the on-line scheduling problem. The objective is to generate a partition into the minimum number of instances such that the response time of any job in each instance is bounded by a given constant. Our research...
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The Chemistry of Mycophenolic Acid-Synthesis and Modifictions Towards Desired Biological Activity
PublicationDokonano przeglądu literatury chemicznej na temat metod syntezy kwasu mykofenolowego oraz jego pochodnych, a także zależności pomiędzy ich strukturą i aktywnością biologiczną.
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Bioassays as one of the Green Chemistry tools for assessing environmental quality: A review
PublicationFor centuries, mankind has contributed to irreversible environmental changes, but due to the modern science of recent decades, scientists are able to assess the scale of this impact. The introduction of laws and standards to ensure environmental cleanliness requires comprehensive environmental monitoring, which should also meet the requirements of Green Chemistry. The broad spectrum of Green Chemistry principle applications should...
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Book Chapter in the Prime Archives in Chemistry: 2nd Edition (dissemination of knowledge)
PublicationTo cite a chapter in a book include: Jaroslaw Spychala. The CON−H….+NH2 Blue-Shifting H-Bond Stabilizing Effect on Z Secondary Amides and Cyclic System Conformational Rearrangement through an Alkylamine-Chain Migration Pathway. In: VSR Rajasekhar Pullabhotla, editor. Prime Archives in Chemistry: 2nd Edition. Hyderabad, India: Vide Leaf. 2022. https://doi.org/10.1155/2022/1707245
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Rime and hoarfrost chemistry in Poland - an introductory analysis from meteorological perspective
PublicationPróbki szronu i sadzi pobierano odpowiednio w 6 i 3 miejscach, które reprezentują zarówno nizinne jak i górzyste części Polski. Niższe stężenia jonów stwierdzono zarówno w próbkach szronu jak i sadzi pobranych na terenie nizinnym. Wynika to ze stosunkowo wysokiej inwersji temperatury i mniej intensywnego krążenia atmosferycznego w tym regionie. Stwierdzono również różne wartości stosunku Na/Cl w próbkach sadzi i szronu zebranych...
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Design of selective substrates of proteinase 3 using combinatorial chemistry methods
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Green analytical chemistry in sample preparation for determination of trace organic pollutants
PublicationW pracy przedstawiono przyjazne środowisku techniki analityczne, stosowane w celu izolacji i wzbogacania analitów. Ilość używanych rozpuszczalników jest ograniczana przez stosowanie alternatwnych rozpuszczalników, technik bezrozpuszczalnikowych, ekstrakcji wspomaganych czynnikami zewnętrznymi oraz przez wprowadzanie mikrosystemów analitycznych.
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Introducing the concept of sustainable development into analytical practice: green analytical chemistry
PublicationW rozdziale przedstawiono innowacyjne techniki analityczne spełniające wymogi zrównoważonego rozwoju w kontekscie praktyki analitycznej. Przedstawiono bezrozpuszczalnikowe metody przygotowania próbek oraz przykłady calych procedur analitycznych spełniajacych warunek zielonej chemii analitycznej
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Hoarfrost and rime chemistry in Poland - An introductory analysis from metrological perspective
PublicationW publikacji przedstawiono wyniki badań poziomów stężeń składników śladowych obecnych w próbkach osadów atmosferycznych (szronu i sadzi) zebranych na terenach wyraźnie różniących się pod względem położenia geograficznego jak również poziomem antropopresji. Zbadano wpływ czynników meteorologicznych tj. rodzaj mas powietrza, typ pola barycznego na chemizm tych form mokrej depozycji. Porównano skład chemiczny różnych form osadów atmosferycznych...
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Chemometrics for Selection, Prediction, and Classification of Sustainable Solutions for Green Chemistry—A Review
PublicationIn this review, we present the applications of chemometric techniques for green and sustainable chemistry. The techniques, such as cluster analysis, principal component analysis, artificial neural networks, and multivariate ranking techniques, are applied for dealing with missing data, grouping or classification purposes, selection of green material, or processes. The areas of application are mainly finding sustainable solutions...
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A Comprehensive Review of Chemistry, Sources and Bioavailability of Omega-3 Fatty Acids
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Green Chemistry in Higher Education: State of the Art, Challenges, and Future Trends
PublicationNowadays, there is increasing interest in global sustainability, and thus, university students would like to know how human actions affect the health status of our planet. This is mainly due to their basic knowledge of problems such as global warming and greenhouse gases. Students would like to gain knowledge on how to safeguard the earth for future generations. This must involve changes in education programs at interested institutions...
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The 15th Workshop on Progress in Trace Metal Speciation for Environmental Analytical Chemistry
PublicationArtykuł jest sprawozdaniem z konferencji TRACESPEC - the 15th Workshop on progress in trace Metal Speciation for Environmental Analytical Chemistry, ktora odbyla sie we wrzesniu 2016 na Politechnice Gdańskiej. W artykule przedstawiono głowne cele i załozenia konferencji oraz opisano program naukowy.
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Some remarks on gas chromatographic challenges in the context of green analytical chemistry
PublicationOmówiono możliwości wprowadzenia zasad zielonej chemii analitycznej w odniesieniu do technik chromatograficznych.
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Tendencies of change in the chemistry of precipitation at three monitoring stations 1996-1999.
PublicationW pracy przedstawiono wyniki porównawczych badań składu próbek opadów deszczowych zebranych na trzech stacjach w okresie 1996-1999, (stacje te różnią się zdecydowanie ze względu na usytuowanie geograficzne). W postaci graficznej przedstawiono zaobserwowane tendencje w składzie zebranych próbek wód opadowych.
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Badania międzylaboratoryjne w chemii analitycznej. Interlaboratory tests in analytical chemistry.
PublicationW pracy dokonano podziału dostępnych badań międzylaboratoryjnych w zależności od założonego celu badań. Przedstawiono i scharakteryzowano podstawowe typy programów badań międzylaboratoryjnych oraz aspekt ich organizacji. Omówiono również wykorzystanie badań biegłości/porównań międzylaboratoryjnych w procesach akredytacji i nadzoru laboratoriów oraz możliwy sposób obróbki danych nadesłanych przez uczestników badań.
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Detection, identification and determination of resveratrol in wine. Problems and challenges
PublicationResveratrol is a compound synthesized by plants in response to unfavorable conditions of growth like mechanical injury, siege of bacteria or fungi and UV exposure. It is concentrated mostly in grapes skin and further more in the products made from grapes especially red wines. Each wine is characterized by different amount of given stilbene since its occurrence is affected by many factors like: types of grapes, environment (climate,...
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Evaluation of the influence of grapevine growing conditions on wine quality
PublicationScientists are increasingly interested in the viticulture concept of terroir, which states that unique properties of wine are strictly related to the environmental conditions under which grapes are cultivated. The aim of the research was to compare the parameters characterizing wines produced in Poland, such as pH, conductivity, total organic carbon (TOC), and concentration of anions (F−, Cl−, NO2−, NO3−, PO43−, SO42−). It was...
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Green analytical chemistry introduction to chloropropanols determination at no economic and analytical performance costs?
PublicationIn this study we perform ranking of analytical procedures for 3-monochloropopane-1,2-diol determination in soy sauces with PROMETHEE method. Multicriteria decision analysis was performed for three different scenarios – metrological, economic and environmental, by application different weights to decision making criteria. All three scenarios indicate capillary electrophoresis – based procedure as the most preferable. Apart from...
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A Green Chemistry "environmentally friendly" approach to the synthesis of chloro-intermediates of ephedrine/pseudoephedrine
PublicationMethylamphetamine is an addictive stimulant drug that strongly activates certain systems in the brain. It is closely related chemically to amphetamine, but the central nervous system effects of methamphetamine are greater. There is much interest in methylamphetamine among scientists and therefore the synthesizes of methylamphetamine and its metabolites are carried out on a large scale in chemical laboratories. Globally, ephedrine...
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Application of chemometric approach in studies of dew chemistry (on the basis of samples collected in Poland)
PublicationPrzedstawiono wyniki badań wybranych związków chemicznych (aniony, kationy, formaldehyd, nadtlenek wodoru, suma fenoli, TC, TIC, TOC) oznaczonych w próbkach rosy zebranych z różnych obszarów na terenie Polski (Gdynia, Gdańsk, Sopot, Mława, Kraków). Zastosowano analizę funkcji dyskryminacyjnej aby dokonać klasyfikacji poszczególnych próbek w zależności od miejsca pobierania oraz wykryć podstawowe zależności pomiędzy poszczególnymi...
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Development of sensitive cathepsin G fluorogenic substrate using combinatorial chemistry methods
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A simple method for selection of trypsin chromogenic substrates using combinatorial chemistry approach
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Selection of New Chromogenic Substrates of Serine Proteinases Using Combinatorial Chemistry Methods
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Retrosynthesis from transforms to predictive sustainable chemistry and nanotechnology: a brief tutorial review
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Calculation of Vibrational Resonance Raman Spectra of Molecules Using Quantum Chemistry Methods
PublicationThe understanding and interpretation of experimental resonance Raman (RR) spectra can strongly benefit from theoretical simulations. These can be achieved by combining quantum chemistry (QC) methods to calculate the electronic and vibrational molecular properties, together with appropriate models and approximations to compute the Raman intensities. This chapter presents the main and most commonly employed approaches to calculate...
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The 12 principles of green analytical chemistry and the SIGNIFICANCE mnemonic of green analytical practices
PublicationThe current rapid development of green analytical chemistry (GAC) requires clear, concise guidelines in the form of GAC principles that will be helpful in greening laboratory practices. The existing principles of green chemistry and green engineering need revision for their use in GAC because they do not fully meet the needs of analytical chemistry. In this article we propose a set of 12 principles consisting of known concepts...
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Application of multivariate statistics in assessment of green analytical chemistry parameters of analytical methodologies
PublicationThe study offers a multivariate statistical analysis of a dataset, including the major metrological, “greenness” and methodological parameters of 43 analytical methodologies applied for aldrin determination (a frequently analyzed organic compound) in water samples. The variables (parameters) chosen were as follows: metrological (LOD, recovery, RSD), describing the “greenness” (amount of the solvent used, amount of waste generated)...
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Optimization of liquid chromatographic separation of pharmaceuticals within green analytical chemistry framework
PublicationThe contribution is aimed at the development of methodology that allows to consider green analytical chemistry criteria during optimization of liquid chromatographic separation with design of experiment. The objectives of the optimization are maximization of peak areas of five non-steroid anti-inflammatory drugs, maximization of resolution between peaks, with simultaneous shortening of chromatographic separation time and minimization...
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Examination of fresh water chemistry in maritime Antarctica during austral summer 2017
PublicationDue to the fact that Antarctica is one of the least polluted places on Earth, it is a perfect place to observe the spread of global pollution. Therefore, research conducted on this continent is important due to the possibility of investigating the type of pollution and their way of transport. This work considers presence of organic contaminants in Maritime Antarctica in unexplored until now, Lions Rump headland. Qualitative and...
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Short-Term Observations of Rainfall Chemistry Composition in Bellsund (SW Spitsbergen, Svalbard)
PublicationGlobal warming results in increasingly widespread wildfires, mostly in Siberia, but also in North America and Europe, which are responsible for the uncontrollable emission of pollutants, also to the High Arctic region. This study examines 11 samples of rainfall collected in August in a coastal area of southern Bellsund (Svalbard, Norway). It covers detailed analysis of major ions (i.e., Cl−, NO3−, and SO42−) and elements (i.e.,...
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Metals and metal-binding ligands in wine: Analytical challenges in identification.
PublicationBackground Due to important role of metals in the vinification process as well as their impact on the human health, their content in this alcoholic beverage has been extensively studied by many researchers. It is already known that speciation of metals determines their toxicity and bioavailability as well as influences their activity. Understanding the chemistry and knowing the structures of metal complexes could have relevant...
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Simple smartphone-based methods for the determination of bioactive compounds in wine
PublicationA set of simple smartphone-based methods of bioactive compounds determination were developed for wine analysis. Procedures for smartphone-based determination of the total content of phenolic compounds, flavonoids, anthocyanins and biogenic amines, as well as measurement of antioxidant activity were developed and fully validated. The experimental setup is based on smartphone and 3D-printed device, though it is very simple and can...
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Determination of Biogenic Amines in Wine Using Micellar Electrokinetic Chromatography
PublicationProduction on a large-scale of fermented alcoholic drinks made from different kinds of fruits is carried out in homes. Although wine laws regulating home production exist, they do not include upper concentration limits of biogenic amines. Therefore, a quick and inexpensive way to determine BAs in wine is crucial. A new analytical method based on micellar electrokinetic chromatography has been developed for the separation of the...
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Determination and identification of organic acids in wine samples. Problems and challenges.
PublicationFor long time, organic acids were underestimated. However, during last two decades there is an increasing interest of natural compounds having antioxidant, antimicrobial and anti-inflammatory properties thus organic acids are very preferable. Wine stands as one of the sources of organic acids since they are responsible for its organoleptic and aestethic character. Nevertheless, it is important to not exceed acceptable level of...
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Development of novel smartphone-based methods of wine quality assessment
PublicationThe doctoral dissertation concerns the development of novel smartphone-based analytical methods of wine quality evaluation, which would be in line with the stipulations of green and equitable analytical chemistry. This solution is based on the analysis of biogenic amines and selected bioactive compounds. The dissertation is based on four articles containing the results of research which led to the development of smartphone-based...
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Elastic-contractile model proteins: Physical chemistry, protein function and drug design and delivery
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Chemistry induced by low-energy electrons in condensed multilayers of pure small organic acids
PublicationPrzedstawiono reakcje indukowane przez niskoenergetyczne elektrony (0.7 - 20 eV) w kondensowanych warstwach kwasu mrówkowego (HCOOH), częściowo deuterowanego kwasu octowego (CH3COOD) oraz kwasu trifluorooctowego (CF3COOD).
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The Influence of Microstructure on the Passive Layer Chemistry and Corrosion Resistance for Some Titanium-Based Alloys
PublicationThe effect of microstructure and chemistry on the kinetics of passive layer growth and passivity breakdown of some Ti-based alloys, namely Ti-6Al-4V, Ti-6Al-7Nb and TC21 alloys, was studied. The rate of pitting corrosion was evaluated using cyclic polarization measurements. Chronoamperometry was applied to assess the passive layer growth kinetics and breakdown. Microstructure influence on the uniform corrosion rate of these alloys...
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Water chemistry of tundra lakes in the periglacial zone of the Bellsund Fiord (Svalbard) in the summer of 2013
PublicationClimate changes observed in the Arctic (e.g. permafrost degradation, glacier retreat) may have significant influence on sensitive polar wetlands. The main objectives of this paper are defining chemical features of water within six small arctic lakes located in Bellsund (Svalbard) in the area of continuous permafrost occurrence. The unique environmental conditions of the study area offer an opportunity to observe phenomena influencing...
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Drivetrain of a Wind Turbine
PublicationIn a most commonly met design of a wind turbine the power is transmitted from the rotor to the generator through the system composed of the main shaft, friction connection, multiplying gearbox and a flexible coupling. The driving system comprises almost a complete set of the machine elements being described during machine design lectures and can serve as an interesting illustration...
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E-Beam Irradiation and Ozonation as an Alternative to the Sulphuric Method of Wine Preservation
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The Education of Analytical Chemists in Polish Universities
PublicationAnalytical Chemistry plays a very important role in the modern world. The main reasons are; the need of environmental monitoring, quality of food and water control, human health, quality of industrial production control, nanotechnologies and material science. Together with Inorganic Chemistry, Organic Chemistry and Physical Chemistry, Analytical Chemistry is a fundamental chemical course. The education of Analytical Chemists is...
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Validation of dimensionless method using height average wind velocity for wind forces
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Tri(mesityloxy)silanethiol - The First Structurally CharacterizedOrganoxysilanethiol (Contributions to the Chemistry of Silicon-SulfurCompounds. 77 [1])
PublicationTri(mezytyloksy)silanotiol (TMST) wyizolowano jako jedyny produkt reakcji pomiędzy disiarczkiem krzemu a 2,4,6-trimetylofenolem. TMSTkrystalizuje w układzie trójskośnym. Dobra jakość kryształów pozwoliła na udokładnienie grupy SH bez narzuconych więzów. Długość wiązania S-H określono na 1,29(4) ang., a kąt Si-S-H na 95,4(17) deg. Cząsteczki TMST nie tworzą wiązań wodorowych w kryształach.
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Recent developments and future trends in solid phase microextraction techniques towards green analytical chemistry
PublicationSolid phase microextraction find increasing applications in the sample preparation step before chromatographic determination of analytes in samples with a complex composition. These techniques allow for integrating several operations, such as sample collection, extraction, analyte enrichment above the detection limit of a given measuring instrument and the isolation of analytes from sample matrix. In this work the information about...