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Search results for: microstructural characterisation
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Study on Microstructural Characterization, Mechanical Properties and Residual Stress of GTAW Dissimilar Joints of P91 and P22 Steels
PublicationThis article deals with the dissimilar joining of two different grade Cr-Mo steel (2.25Cr-1Mo: P22 and modified 9Cr-1Mo: P91) for power plant application. The dissimilar butt-welded joint was produced for conventional V groove design by using the gas tungsten arc welding (GTAW) process with the application of an ERNiCrMo-3 Ni-based super alloy filler. A microstructure characterization was performed to measure the inhomogeneity...
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Assessment of Corrosive Behaviour and Microstructure Characterization of Hybrid Friction Stir Welded Martensitic Stainless Steel
PublicationThis study examined the effect of induction heating on the microstructure and corrosion characteristics of hybrid friction stir welded AISI 410 stainless steel. Five joints have been produced with different friction stir welding parameters like welding speed, spindle speed, plunge depth, and induction power. Their microstructures were evaluated using a scanning electron microscope, and chemical composition was examined using...
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Mechanical and Microstructural Characterization of TIG Welded Dissimilar Joints between 304L Austenitic Stainless Steel and Incoloy 800HT Nickel Alloy
PublicationIn this article, the mechanical properties and microstructure of 304L austenitic stainless steel/Incoloy 800HT nickel alloy dissimilar welded joints are investigated. The joints were made of 21.3 mm × 7.47 mm tubes using the TIG process with the use of S Ni 6082 nickel filler metal. No welding imperfections were found and high strength properties of joints were obtained, meeting the assumed acceptance criteria of the product’s...
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Iron doped manganese cobaltite spinel coatings produced by electrophoretic co-deposition on interconnects for solid oxide cells: Microstructural and electrical characterization
PublicationWe report a systematic microstructural and electrical characterization of iron doped Mn–Co spinel coatings processed by electrophoretic co-deposition of Mn1.5Co1.5O4 and Fe2O3 powders on Crofer 22 APU and AISI 441 steel substrates. Iron addition to Mn–Co spinel coating leads to a reduction of the area specific resistance on both substrates, after 3200 h at 750 °C. The Fe doped Mn–Co coating both leads to a thinner oxide scale and...
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Microstructural Analysis of Fractured Orthopedic Implants
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Microstructural Design of Ba0.5La0.5Co0.5Fe0.5O3 Perovskite Ceramics
PublicationBa0.5La0.5Co0.5Fe0.5O3 was synthesized in the solid-state reaction route. The influence of ball milling parameters (such as milling media size, angular velocity, and time), pelletizing pressure, and annealing parameters on the microstructure was studied. The grain size distribution and density or specific surface area changes were investigated in each approach while the individual parameters were changed. The evaluation of BLCF...
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Cavitation Erosion of Nodular Cast Iron - Microstructural Effects
PublicationThe paper deals with susceptibility of nodular cast iron with ferritic-pearlitic matrix on cavitation erosion. Cavitation tests were carried out with the use of a cavitation erosion vibratory apparatus employing a vibration exciter operated at frequency of 20 kHz. The study allowed to determine the sequence of subsequent stages in which microstructure of cast iron in superficial regions is subject to degradation. The first features...
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Microstructural and electrical properties of Y0.07Sr0.93-xTiO3 perovskite ceramics
PublicationIn order to find a relationship between electrical and microstructural properties, yttrium-doped strontium titanate (7 mol%) with various values of strontium nonstoichiometry was investigated and shown in this work. It has been observed that yttrium doping can affect the electrical properties of SrTiO3 to a great extent. Moreover, the microstructural and electrical properties can be influenced by strontium nonstoichiometry. The...
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Investigation of microstructure of D36 Plate
PublicationWykonano badania metalograficzne i określono strukturę blachy gatunku D36.
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Modelling of engineering materials with microstructure
PublicationArtykuł omawia różne modele do opisu lokalizacji odkształceń w postaci rys i stref ścinania w materiałach budowlanych takich jak grunt i beton. Zastosowane modele mechaniki ośrodka ciągłego i modele dyskretne.
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Microstructural aspects of corrosion of the SUPERSTON alloy after laser treatment
PublicationW artykule przedstawiono rezultaty obróbki laserowej stopu SUPERSTON w warunkach kriogenicznych i jej wpływ na mikrostrukturę i odporność korozyjną. Badania korozyjne zostały zrealizowane metodą potencjostatyczną w 3% NaCl, odporność korozyjna stopu zmieniała się wraz ze zmianą parametrów nadtapiania laserowego.
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Microstructural and electrical properties of Y0.07Sr0.93-xTiO3-δ perovskite ceramics
PublicationIn order to find a relationship between electrical and microstructural properties, yttrium-doped strontiumtitanate (7 mol%) with various values of strontium nonstoichiometry was investigated and shown in this work.It has been observed that yttrium doping can affect the electrical properties of SrTiO3 to a great extent.Moreover, the microstructural and electrical properties can be influenced by strontium nonstoichiometry.The defect...
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Impact of blending with polystyrene on the microstructural and electrochemical properties of SiOC ceramic
PublicationIn this work, we present the electrochemical behavior and microstructural analysis of silicon oxycarbide (SiOC) ceramics influenced by an addition of polystyrene (PS). Polymer-derived ceramics were obtained by pyrolysis (1000°C, Ar atmosphere) of different polysiloxanes prepared by sol–gel synthesis. This method is very effective to obtain desired composition of final ceramic. Two alkoxysilanes phenylthriethoxysilane and diphenyldimethoxysilane...
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Induction Assisted Hybrid Friction Stir Welding of Dissimilar Materials AA5052 Aluminium Alloy and X12Cr13 Stainless Steel
PublicationThis research aimed to study the induction in-situ heated hybrid friction stir welding (IAFSW) method to join AA5052 aluminium alloy with X12Cr13 stainless steel (SS) to enhance joint strength. The potency of this method on the mechanical properties and microstructural characterizations were also investigated. The results show that the transverse tensile strength gained was 94% of the AA5052 base metal that is 229.5 MPa. This superior...
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Microstructural and electrical properties of Y0:07Sr0:93−xTiO3− perovskite ceramics
PublicationIn order to find a relationship between electrical and microstructural properties, yttrium-doped strontium titanate (7 mol%) with various values of strontium nonstoichiometry was investigated and shown in this work. It has been observed that yttrium doping can affect the electrical properties of SrTiO3 to a great extent. Moreover, the microstructural and electrical properties can be influenced by strontium nonstoichiometry. The...
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Microstructural aspects of hydrogen degradation of the 26H2MF and 34HNM constructional alloy steels
PublicationPodatność na degradację wywołaną przez wodór, dwóch gatunków polskich stali konstrukcyjnych stopowych: 26H2MF i 34HNM, określano przy pomocy próby powolnego rozciągania. Mierzono następujące parametry: energię pękania, wydłużenie, wytrzymałość na rozciąganie i przewężenie. Degradację stali obserwowano w 0,01M kwasie siarkowym przy gęstości prądu 20 mA/cm2 wraz z rodzajem przełomów. Poziom degradacji był zgodny z ilością wodoru...
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Synthesis and characterisation of starch cuprate
PublicationThe cupration of granular potato starch with ammonium tetrachlorocuprate(II) was performed by a 20 min lasting microwave-assisted process and by 40 min convectional heating. In both cases the degree of esterification (DE) did not exceed 0.0064. A higher dose of cuprate had a positive effect on DE, regardless of whether the microwave irradiation or the convectional heating was applied, and on the thermal stability of the starch...
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Microstructure and Dielectric Properties of Barium-vanadate Glasses
PublicationThe ac and dc conductivity in barium-vanadate glasses was investigated as a function of temperature and frequency with the use of impedance spectroscopy. The topography and microstructure of glasses were investigated by the means of X-ray diffraction (XRD) and scanning electron microscopy (SEM) methods. The XRD results show that all samples are amorphous but microscopy investigation reveals that glasses with greater amount of V2O5...
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Microstructure and electrical properties of manganese borosilicate glasses
PublicationThe structure, optical and electrical properties of manganese borosilicate glasses of the composition xMnO–(80 − x)SiO 2 –20B 2 O 3 (x = 40, 50, and 60 mol%) were investigated. The dependence of the glass structure on its composition was discussed and related to electrical properties. A separation of two amorphous phases was observed. It was suggested that one phase is MnO-rich and the other is SiO 2 -rich. It was found that...
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An investigation of microstructural basis for corrosion behavior of Al-CNT composites fabricated by SPS
PublicationIn this research effect of the addition of multi-wall carbon nanotubes (MWCNTs) as additive powder on microstructure and corrosion behavior of fabricated Al-CNT composites was studied. The aluminum powder and CNTs were mixed with high energy planetary ball-mill. It is observed that by increasing milling time, the uniformity of CNTs on aluminum matrix and consequently corrosion resistance of Al-CNT composite is increased. On the...
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Some Introductory and Historical Remarks on Mechanics of Microstructured Materials
PublicationHere we present few remarks on the development of the models of microstuctured media and the generalized continua.
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Analysis of microstructured optical fibers using compact macromodels
PublicationW niniejszym artykule zaproponowano nową technikę analizy światłowodów fotonicznych. Zaprezentowany algorytm jest kombinacją metody redukcji rzędu modelu oraz techniki dyskretnych rozwinięć funkcyjnych i pozwala w znaczącym stopniu zmniejszyć liczbę zmiennych (nawet do 85%), redukując (nawet 16 krotnie) czas symulacji.
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Development of Microstructured Carbon Coatings by Substrate-Catalytic CVD
PublicationCarbon nanostructured films were synthesized by chemical vapor deposition (CVD) on H18 stainless steel (AISI 440C) sheets with an H2/CH4/N2 gas mixture at various substrate temperatures. During the synthesis, the iron and chromium oxide layer was formed between the steel and carbonaceous layer. The carbon films exhibited wall-like and spherical morphologies and structures, as characterized by scanning electron microscopy and Raman...
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Relation between Structure and Magnetic Properties of Microstructured PrAlO3
PublicationPrzedstawiono porównanie właściwości magnetycznych perowskitowego związku PrAlO3 i mikrostrukturalne wersji w formie eutektycznej PrAlO3 - PrAl11O18.
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Comparative characterisation of durian, mango and avocado
PublicationCelem przeprowadzonych badan była ocena właściwości odżywczych i bioaktywnych stosunkowo mało znanych egzotycznych owoców duriana i ich porównanie z parametrami charakteryzującymi powszechnie znane owoce mango i gruszki adwokackiej. W badaniach wykorzystano takie techniki jak HPLC, trójwymiarowa fluorescencja (3D-FL), testy oparte na zastosowaniu rodników (ABTS i DPPH) oraz zaawansowane techniki chemometryczne. na podstawie uzyskanych...
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Studies on the Preparation and Characterisation of Carbon Nanostructures
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Investigation of the microstructure on the nanoporous carbon based capacitive performance
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Effect of microstructure on mechanical properties of BA1055 bronze castings
PublicationThe article presents research results performed on aluminum bronze CuAl10Fe5Ni5 (BA1032) castings used for marine propellers. Metallographic studies were made on light microscope and a scanning electron microscope to assess quantitatively and qualitatively the alloy microstructure. It has been shown that the shape, size and distribution of the iron-rich phase precipitates in bronze microstructure significantly affect its mechanical...
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Optimization of microstructure and properties of acceptor-doped barium cerate
PublicationThe presented research concerns acceptor doped barium cerate and the attempts of improvement of its production method that would allow obtaining the solid electrolyte characterized by the particular properties. The authors suggest combining two production methods, molten salt synthesis and self-combustion, in order to achieve the compound material that has some of the advantages of both of the initial methods. An impact of nickel...
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Microstructure and corrosion properties of the laser treated SUPERSTON alloy
PublicationPrzedstwiono wyniki laserowego nadtapiania powierzchni stopu SUPERSTON w warunkach kriogenicznych. Zaprezentowano obraz powierzchni stopu po badaniach korozyjnych oraz wyniki pomiarów mikrotwardości i odporności korozyjnej.
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Microstructure and residual stresses in surface coatings with PTFE reservoirs
PublicationThe paper presents the results of experimental study into the microstructure and changes in residual stresses resulting from sliding and rolling/sliding loaded interaction between metallic surface coatings with embedded PTFE reservoirs and various counter faces. It was found that before testing surface coatings had compressive residual stresses. Molybdenum coating with all types of PTFE reservoirs displayed, as a result of testing,...
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Structural and physical characterization of NpPt2In7
PublicationA new neptunium intermetallic compound, NpPt2In7, has been synthesized in polycrystalline form and characterized by several macroscopic techniques. A Rietveld analysis of its powder x-ray diffraction pattern shows that NpPt2In7 crystallizes in a tetragonal lattice with I4/mmm symmetry and lattice parameters a = 4.58471(3) Å, c = 21.5065(3) Å. Magnetic susceptibility, electrical resistivity, Hall effect, and heat capacity measurements indicate...
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Characterization of CaTi0.9Fe0.1O3/La0.98Mg0.02NbO4 composite
PublicationA composite of CaTi0.9Fe0.1O3 and electrolyte material, i.e. magnesium doped La0.98Mg0.02NbO4 was prepared and studied. The phase content and the sample microstructure was examined by an X-ray diffraction method and scanning electron microscopy. EDS measurements were done both for composite samples and the diffusion couple. The electrical properties were studied by four terminal DC method. The Ahigh-temperature interaction between...
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Characteristics of microstructural phenomena occurring on the surface of protective gloves by the action of mechanical and chemical factors
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Insight into the microstructural and durability characteristics of 3D printed concrete: Cast versus printed specimens
PublicationThis study presents the comparison of microstructural and durability characteristics of 3D printed concrete (3DPC) depending on its production method (printing or casting). Printed samples with different numbers of layers, as well as a cast specimen with an identical mix composition, were produced and compared, with their microstructural pore and solid characteristics quantitatively and qualitatively investigated. For this purpose,...
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Microstructural evolution of 6061 aluminium alloy subjected to static and dynamic compression at low temperature
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Deformation Behavior and Microstructural Evolution during Hot Stamping of TA15 Sheets: Experimentation and Modelling
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Polarization Conversion of Solitons Propagating in Birefringent Microstructured Optical Fibers
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On effective surface elastic moduli for microstructured strongly anisotropic coatings
PublicationThe determination of surface elastic moduli is discussed in the context of a recently proposed strongly anisotropic surface elasticity model. The aim of the model was to describe deformations of solids with thin elastic coatings associated with so-called hyperbolic metasurfaces. These metasurfaces can exhibit a quite unusual behaviour and concurrently a very promising wave propagation behaviour. In the model of strongly anisotropic...
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Efficient finite difference analysis of microstructured optical fibers [on line]
PublicationW pracy przedstawiono nową technikę numerycznej analizy mikrostruktur światłowodowych. Technika ta polega na połączeniu metody różnic skończonych i dyskretnych rozwinięć funkcyjnych. Pozwala to na zmniejszenie rozmiaru macierzy powstających przy analizie problemu, a jednocześnie na bezpośrednią implementację radiacyjnych warunków brzegowych. Testy algorytmu przeprowadzono dla kilku wybranych struktur, uzyskując bardzo dobrą zgodność...
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Efect of ageing on microstructure and impact properties of 9Cr-1Mo steel
PublicationBadano wpływ długotrwałego starzenia na mikrostrukturę i właściwości udarnościowe trzech przemysłowych wytopów stali typu 9Cr-1Mo. Wczesniejsze badania wykazały, że w stali 9Cr-1Mo starzonej w 550C przez 10 000 godzin występuje kruchość odpuszczania, a przy dłuższych czasach ekspozycji tworzy się krucha faza Lavesa (FeCr)2Mo na granicach ziaren. Powoduje to wzrost teperatury przejściowej kruchości oraz spadek energii łamania powyżej...
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Effect of microstructure on impact toughness of duplex and superduplex stainless steels
PublicationW artykule przedstawiono wpływ wyżarzania stali dupleks 2205 i superdupleks 2507 na przemiany strukturalne oraz udarność. Obróbkę cieplną przeprowadzono w zakresie temperatur 500-900C i w czasie 6 - 600 min. Określono i porównano podatność obu stali do zmian właściwości po wyżarzaniu
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Cavitation Erosion Resistance of Austenitic Microstructure Created byLaser Beam
PublicationPraca przedstawia własności kawitacyjne różnych mikfrostruktur austenitycznych tworzonych za pomocą wiązki lasera na stalach X5CrNi18-10 oraz C45. Stal X5CrNi18-10 była laserowo stopowana węglikiem TiC oraz stopowana Ni, Mn, Cr i Nb. Jako żródło mocy stosowany był laser CO2. Własności kawitacyjne oceniane były na stanowisku z wirującą tarczą. Badania ujawniły różną podatność struktury austenicycznej do odkształceń plastycznych...
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The Influence of Nano-Fe3O4 on the Microstructure and Mechanical Properties of Cementitious Composites
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Food microstructure systems modelling regarding interaction and contact phenomena.
PublicationPrzedstawiono wybrane fragmenty teorii modelowania w strukturach rozproszonych mikrostruktury żywności, w których zostały uwzględnione wzajemne oddziaływania cząstek oraz występujące zjawiska kontaktowe. Do oszacowania tych oddziaływań wykorzystano zmodyfikowany przez autora model Buczkowskiego i Kleibera.
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Seafloor Characterisation Using Underwater Acoustic Devices
PublicationThe problem of seafloor characterisation is important in the context of management as well as investigation and protection of the marine environment. In the first part of the paper, a review of underwater acoustic technology and methodology used in seafloor characterisation is presented. It consists of the techniques based on the use of singlebeam echosounders and seismic sources, along with those developed for the use of sidescan...
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Using multibeam echoes in seafloor characterisation and classification
PublicationThe method of seabed identification and classification from multibeam sonar echoes is presented. The proposed approach is based on calculation of a set of parameters of an echo envelope, similarly as in seafloor classification using single beam echosounder. These parameters are extracted for each consecutive beam allowing the estimation of their dependence on the seafloor incident angle. The relation between seabed type and calculated...
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Multibeam sonar data processing for seafloor characterisation
PublicationThe approach to seafloor characterisation was investigated. It relies on calculation of several descriptors (parameters) related to seabed type using three types of multibeam sonar data obtained during seafloor sensing: 1) the grey-level sonar images of seabed, 2) the 3D model of the seabed surface which consist of (x, y, z) points, 3) the set of time domain echo envelopes corresponding to several beams. The proposed method has...
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Preparation and characterisation of solution-cast Nafion membrane
PublicationNafion is a commercial name for a perfluorosulfonic polymer, which has been developed in 1962 by Dupont de Nemours. This polymer consists of a polytetrafluoroethylene backbone and regular spaced long perfluorovinyl ether pendant side chains terminated by a sulfonate ionic group. These sulfonate groups are responsible for cation-exchange properties of Nafion. Thanks to the ion-exchange properties, water permeability, good chemical,...
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Carbon nanotubes linked with pitavastatin: synthesis and characterisation
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