Dynamic Electrochemical Impedance Spectroscopy (DEIS) as a Tool for Analyzing Surface Oxidation Processes on Boron-Doped Diamond Electrodes - Publikacja - MOST Wiedzy

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Dynamic Electrochemical Impedance Spectroscopy (DEIS) as a Tool for Analyzing Surface Oxidation Processes on Boron-Doped Diamond Electrodes

Abstrakt

Surface oxidation processes play a key role in understanding electrochemical properties of boron-doped diamond (BDD) electrodes. The type of surface termination groups, which create the potential window of electrolytic water stability or hydrophobicity, influences such properties. In this study the kinetics of oxidation process under anodic polarization were studied in situ by means of Dynamic Electrochemical Impedance Spectroscopy (DEIS) technique. This novel approach allows for obtaining the impedance data for non-stationary systems. It has been proven that for [B] dopant level of 10k ppm, polarization to 1.5 V vs. Ag|AgCl is sufficient to initiate transformation of the film terminating BDD electrodes. XPS analysis and wettability measurements confirmed oxidation under given conditions

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Kategoria:
Publikacja w czasopiśmie
Typ:
artykuł w czasopiśmie wyróżnionym w JCR
Opublikowano w:
JOURNAL OF THE ELECTROCHEMICAL SOCIETY nr 161, wydanie 6, strony 359 - 364,
ISSN: 0013-4651
Język:
angielski
Rok wydania:
2014
Opis bibliograficzny:
Ryl J., Bogdanowicz R., Ślepski P., Sobaszek M., Darowicki K.: Dynamic Electrochemical Impedance Spectroscopy (DEIS) as a Tool for Analyzing Surface Oxidation Processes on Boron-Doped Diamond Electrodes// JOURNAL OF THE ELECTROCHEMICAL SOCIETY. -Vol. 161, iss. 6 (2014), s.359-364
Weryfikacja:
Politechnika Gdańska

wyświetlono 184 razy

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