Miniaturized, green salting-out liquid–liquid microextraction coupled with GC–MS used to evaluate biogenic amines in wine samples - Publikacja - MOST Wiedzy

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Miniaturized, green salting-out liquid–liquid microextraction coupled with GC–MS used to evaluate biogenic amines in wine samples

Abstrakt

Monitoring of the biogenic amines (BAs) content in food products, including wine, is important due to the health and safety of consumers and from the quality control point of view. In a given study, simultaneous derivatization and salting-out liquid–liquid microextraction (SALLME) coupled with GC–MS for BAs determination from wine samples was developed. For the optimization the Box-Behnken design was applied, where three independent factors were evaluated: the amount of NaCl, amount of EtAc and vortexing time. The proposed approach is characterized by good sensitivity expressed in the detection limit between 1.5 and 8.1 µg/L, good recovery on the level 84 – 106% and good reproducibility, it is fast (20 min) and easy to perform. Moreover, the BAs index (BAI) was applied in order to assess the quality of examined wines. BAI value for most of wine samples were below 2 mg/L what indicates that selected wines were of high quality.

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Wersja publikacji
Accepted albo Published Version
DOI:
Cyfrowy identyfikator dokumentu elektronicznego (otwiera się w nowej karcie) 10.1016/j.microc.2022.107616
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Creative Commons: CC-BY otwiera się w nowej karcie

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Kategoria:
Publikacja w czasopiśmie
Typ:
artykuły w czasopismach
Opublikowano w:
MICROCHEMICAL JOURNAL nr 180,
ISSN: 0026-265X
Język:
angielski
Rok wydania:
2022
Opis bibliograficzny:
Fabjanowicz M., Różańska A., Kalinowska K., Płotka-Wasylka J.: Miniaturized, green salting-out liquid–liquid microextraction coupled with GC–MS used to evaluate biogenic amines in wine samples// MICROCHEMICAL JOURNAL -Vol. 180, (2022), s.107616-
DOI:
Cyfrowy identyfikator dokumentu elektronicznego (otwiera się w nowej karcie) 10.1016/j.microc.2022.107616
Źródła finansowania:
  • Publikacja bezkosztowa
Weryfikacja:
Politechnika Gdańska

wyświetlono 114 razy

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