Optimization of a Fabric Phase Sorptive Extraction protocol for the isolation of six bisphenols from juice pouches to be analysed by high performance liquid chromatography coupled with diode array detector - Publikacja - MOST Wiedzy

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Optimization of a Fabric Phase Sorptive Extraction protocol for the isolation of six bisphenols from juice pouches to be analysed by high performance liquid chromatography coupled with diode array detector

Abstrakt

Fabric Phase Sorptive Extraction (FPSE) combined with high pressure liquid chromatography using to diode array detection (HPLC-DAD) was applied for the simultaneous determination of bisphenols (BPA, BPB, BPC, BPE, BPF, BPS) in juice pouches. The FPSE procedure was optimized with regards to the critical parameters that affect the performance of the method including the selection of the FPSE membrane type and size, adsorption time, extraction time, solvent volume desorption, magnetic stirring ratio, and salt addition. The FPSE membrane could be reused up to 14 times. The developed FPSE-HPLC-DAD method was validated in terms of linearity, sensitivity, accuracy andprecision. The limits of detection (LODs) were lower than 6.9 ng/mL, while the limits of quantification (LOQs) were lower than 21 ng/mL. The results obtained are satisfactory in terms of precision, accuracy and repeatability, with recoveries above 86% and CV values below 9.5%. The FPSE-HPLC-DAD method was successfully applied in the determination of six bisphenols in juice samples stored in pouches.

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Kategoria:
Publikacja w czasopiśmie
Typ:
artykuły w czasopismach
Opublikowano w:
JOURNAL OF CHROMATOGRAPHY A nr 1708,
ISSN: 0021-9673
Język:
angielski
Rok wydania:
2023
Opis bibliograficzny:
Kubica P., Kalogiouri N., Kabir A., Furton K. G., Samanidou V. F.: Optimization of a Fabric Phase Sorptive Extraction protocol for the isolation of six bisphenols from juice pouches to be analysed by high performance liquid chromatography coupled with diode array detector// JOURNAL OF CHROMATOGRAPHY A -Vol. 1708, (2023), s.464366-
DOI:
Cyfrowy identyfikator dokumentu elektronicznego (otwiera się w nowej karcie) 10.1016/j.chroma.2023.464366
Źródła finansowania:
  • Publikacja bezkosztowa
Weryfikacja:
Politechnika Gdańska

wyświetlono 69 razy

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