ISSN: 0169-4332

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A 2017 35
A 2016 35
A 2015 35
A 2014 35
A 2013 30
A 2011 30
A 2008 32

Prace opublikowane w tym czasopiśmie

  1. 2018

  2. Binder-induced surface structure evolution effects on Li-ion battery performance

    J. Rezvani , M. Pasqualini , A. Witkowska , R. Gunnella , A. Birrozzi , M. Minicucci , H. Rajantie , M. Copley , F. Nobili , A. Dicicco - APPLIED SURFACE SCIENCE - 2018
    A comparative investigation on binder induced chemical and morphological evolution of Li4Ti5O12 electrodes was performed via X-ray photoemission spectroscopy, scanning electron microscopy, and electrochemical measurements. Composite electrodes were obtained using three different binders (PAA, PVdF, and CMC) with 80:10:10 ratio of active material:carbon:binder. The electrochemical performances of the electrodes, were found to be...
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  3. Electrochemical and photoelectrochemical properties of the interface between titania nanotubes covered by conducting polymer in aqueous by conducting polymer in aqueous electrolytes – The effect of various geometry and electrolytes concentration

    In the present work we show the impact of nanotubes (NTs) geometry of titania utilized as a substrate in organic-inorganic systems acting as a p-n junction on efficient conversion of radiation energy into electrochemical energy. The electrolytic bath composition and electrolysis conditions were controlled in order to obtain TiO2NTs of various geometry as a result of electrochemical oxidation of titanium foil. The electrode material...
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  4. Mono- and bimetallic nanoparticles decorated KTaO 3 photocatalysts with improved Vis and UV–Vis light activity

    A. Krukowska , G. Trykowski , M. Winiarski , T. Klimczuk , W. Lisowski , A. Mikolajczyk , H. Pinto , A. Zaleska-Medynska - APPLIED SURFACE SCIENCE - 2018
    New mono- and bimetallic nanoparticle-decorated perovskite-type KTaO3 photocatalysts were successfully synthesized by hydrothermal reaction followed by photodeposition of MNPs/BNPs. The effect of noble metal type, amount of metal precursor as well as photoreduction method on the physicochemical and photocatalytic properties of MNPs- and BNPs-KTaO3 have been investigated. Photocatalytic activity under Vis light irradiation was estimated...
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  5. Salt melt synthesis of curved nitrogen-doped carbon nanostructures: ORR kinetics boost

    Implementing metal-free electrocatalysts for the oxygen reduction reaction (ORR) and revealing crucial chemical or topographical parameters driving their activity are vital for the development of power cells. The carbon-based catalysts are very often synthesized through carbonization of biopolymers, in particular, those one containing nitrogen groups such as chitosan. Unfortunately, the resulting carbonaceous materials usually...
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  6. Tailoring properties of reduced graphene oxide by oxygen plasma treatment

    We report an easily controllable, eco-friendly method for tailoring the properties of reduced graphene oxide (rGO) by means of oxygen plasma. The effect of oxygen plasma treatment time (1, 5 and 10 minutes) on the surface properties of rGO was evaluated. Physicochemical characterization using microscopic, spectroscopic and thermal techniques was performed. The results revealed that different oxygen-containing groups (e.g. carboxyl,...
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  7. Toughness augmentation by fibrillation and yielding in nanostructured blends with recycled polyurethane as a modifier

    A. Reghunadhan , J. Datta , N. Kalarikkal , J. Haponiuk , S. Thomas - APPLIED SURFACE SCIENCE - 2018
    In the present paper, we have carefully investigated the morphology and fracture mechanism of the recycled polyurethane (RPU) /epoxy blend system. The second phase (RPU) added to the epoxy resin has a positive effect on the overall mechanical properties. Interestingly, the recycled polymer has a remarkable effect on the fracture toughness of epoxy resin. The mechanism behind the fracture toughness improvement up on the addition...
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  8. 2017

  9. Nanostructuring of thin Au films deposited on ordered Ti templates for applications in SERS

    K. Grochowska , K. Siuzdak , Ł. Macewicz , F. Skiba , J. Karczewski , M. Szkoda , Ł. Burczyk , G. Śliwiński - APPLIED SURFACE SCIENCE - 2017
    In this work the results on thermal nanostructuring of the Au films on Ti templates as well as morphology and optical properties of the obtained structures are reported. The bimetal nanostructures are fabricated in a multi-step process. First, the titania nanotubes are produced on the surface of Ti foil by anodization in an ethylene glycol-water solution containing fluoride ions. This is followed by chemical etching in oxalic acid...
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  10. The effect of microemulsion composition on the morphology of Pd nanoparticles deposited at the surface of TiO2 and photoactivity of Pd-TiO2

    A series of microemulsion (ME) system, constituted by different water to surfactant molar ratios (Wo) and oil to surfactant mass ratios (S), have been applied for Pd-TiO2 preparation. The effect of ME properties on the morphology of Pd nanoparticles formed at TiO2 surface and an effect of Pd size and distribution on the surface and photocatalytic properties of Pd-TiO2 were investigated. Microemulsion systems were characterized...
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  11. Various types of semiconductor photocatalysts modified by CdTe QDs and Pt NPs for toluene photooxidation in the gas phase under visible light

    M. Marchelek , E. Grabowska , T. Klimczuk , W. Lisowski , A. Zaleska-Medynska - APPLIED SURFACE SCIENCE - 2017
    A novel synthesis process was used to prepare TiO2 microspheres, TiO2 P-25, SrTiO3 and KTaO3 decorated by CdTe QDs and/or Pt NPs. The effect of semiconductor matrix, presence of CdTe QDs and/or Pt NPs on the semiconductor surface as well as deposition technique of Pt NPs (photodeposition or radiolysis) on the photocatalytic activity were investigated. The as-prepared samples were characterized by X-ray powder diffractometry (XRD),...
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  12. 2016

  13. Enhanced photocatalytic, electrochemical and photoelectrochemical properties of TiO2 nanotubes arrays modified with Cu, AgCu and Bi nanoparticles obtained via radiolytic reduction

    M. Nischk , P. Mazierski , Z. Wei , K. Siuzdak , N. Kouame , E. Kowalska , H. Remita , A. Zaleska-Medynska - APPLIED SURFACE SCIENCE - 2016
    TiO2 nanotubes arrays (NTs), obtained via electrochemical anodization of Ti foil, were modified with monometallic (Cu, Bi) and bimetallic (AgCu) nanoparticles. Different amounts of metals’ precursors were deposited on the surface of NTs by the spin-coating technique, and the reduction of metals was performed via gamma radiolysis. Surface modification of titania was studied by EDS and XPS analysis. The results show that AgCu nanoparticles...
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  14. Enhanced photoelectrochemical performance of inorganic-organic hybrid consisting of BiVO4 and PEDOT:PSS

    K. Trzciński , M. Szkoda , K. Siuzdak , M. Sawczak , A. Lisowska-Oleksiak - APPLIED SURFACE SCIENCE - 2016
    The PEDOT:PSS (poly(3,4-ethylenedioxythiophene):poly(styrenesulfonate)) was electrodeposited on a thin layer of bismuth vanadate (BiVO 4 ) prepared using the pulsed laser deposition technique onto FTO. The inorganic-organic junction was characterized by Raman spectroscopy, UV-Vis spectroscopy and sc anning electron microscopy. Chronoamperometry curves, recorded under simulated solar light illumination,...
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  15. Optical and electrical properties of boron doped diamond thin conductive films deposited on fused silica glass substrates

    This paper presents boron-doped diamond (BDD) film as a conductive coating for optical and electronic purposes. Seeding and growth processes of thin diamond films on fused silica have been investigated. Growth processes of thin diamond films on fused silica were investigated at various boron doping level and methane admixture. Two step pre-treatment procedure of fused silica substrate was applied to achieve high seeding density....
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  16. Properties of ordered titanium templates covered with Au thin films for SERS applications

    K. Grochowska , K. Siuzdak , M. Sokołowski , J. Karczewski , M. Szkoda , G. Sliwiński - APPLIED SURFACE SCIENCE - 2016
    tCurrently, roughened metal nanostructures are widely studied as highly sensitive Raman scattering sub-strates that show application potential in biochemistry, food safety or medical diagnostic. In this workthe structural properties and the enhancement effect due to surface enhanced Raman scattering (SERS) ofhighly ordered nano-patterned titanium templates covered with thin (5–20 nm) gold films are reported.The templates are formed...
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  17. Semi-transparent ordered TiO2 nanostructures prepared by anodization of titanium thin films deposited onto the FTO substrate

    M. Szkoda , A. Lisowska-Oleksiak , K. Grochowska , Ł. Skowroński , J. Karczewski , K. Siuzdak - APPLIED SURFACE SCIENCE - 2016
    In a significant amount of cases, the highly ordered TiO2nanotube arrays grow through anodic oxidationof a titanium metal plate immersed in electrolyte containing fluoride ions. However, for some practicalapplications, e.g. solar cells or electrochromic windows, the semi-transparent TiO2formed directly onthe transparent, conductive substrate is very much desired. This work shows that high-quality Ti coatingcould be formed at room...
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  18. The effect of metal cluster deposition route on structure and photocatalytic activity of mono- and bimetallic nanoparticles supported on TiO2 by radiolytic method

    J. Nadolna , A. Gołębiewska , P. Mazerski , T. Klimczuk , H. Remita , A. Zaleska-Medynska , M. Klein - APPLIED SURFACE SCIENCE - 2016
    TiO2 (P25) was modified with small and relatively monodisperse mono- and bimetallic clusters (Ag, Pd, Pt, Ag/Pd, Ag/Pt and Pd/Pt) induced by radiolysis to improve its photocatalytic activity. The as-prepared samples were characterized by X-ray fluorescence spectrometry (XRF), photoluminescence spectrometry (PL), diffuse reflectance spectroscopy (DRS), X-ray powder diffractometry (XRD), scanning transition electron microscopy (STEM)...
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  19. Visible light activity of pulsed layer deposited BiVO4/MnO2 films decorated with gold nanoparticles: The evidence for hydroxyl radicals formation

    Thin films containing BiVO4 and MnO2 deposited on FTO and modified by Au nanoparticles were studied towards their photoelectrochemical and photocatalytical activities in an aqueous electrolyte. Electrodes were prepared by the pulsed laser deposition (PLD) method. The surfactant-free ablation process was used for preparation of the gold nanoparticles (GNP) water suspension. Obtained layers of varied thicknesses (27–115 nm) were...
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  20. 2015

  21. Functionalization of indium-tin-oxide electrodes by laser-nanostructured gold thin films for biosensing applications

    K. Grochowska , K. Siuzdak , J. Karczewski , G. Śliwiński - APPLIED SURFACE SCIENCE - 2015
    of a relatively large area formed by pulsed laser nanostructuring of thin gold films arereported and discussed. The SEM inspection of modified electrodes reveals the presence of the nearlyspherical and disc-shaped particles of dimensions in the range of 40–120 nm. The NP-array geometry canbe controlled by selection of the laser processing conditions. It is shown that particle size and packingdensity of the array are important factors...
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  22. The effect of nanoparticles size on photocatalytic and antimicrobial properties of Ag-Pt/TiO2 photocatalysts

    A. Zielińska-Jurek , Z. Wei , I. Wysocka , P. Szweda , E. Kowalska - APPLIED SURFACE SCIENCE - 2015
    Ag-Pt-modified TiO2 nanocomposites were synthesized using the sol–gel method. Bimetallic modified TiO2 nanoparticles exhibited improved photocatalytic activity under visible-light irradiation, better than monometallic Ag/TiO2 and Pt/TiO2 nanoparticles (NPs). All modified powders showed localized surface plasmon resonance (LSPR) in visible region. The photocatalysts’ characteristics by X-ray diffractometry (XRD), scanning transmission...
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  23. Thin layer of ordered boron-doped TiO2 nanotubes fabricated in a novel type of electrolyte and characterized by remarkably improved photoactivity

    This paper reports a novel method of boron doped titania nanotube arrays preparation by electrochemical anodization in electrolyte containing boron precursor – boron trifluoride diethyl etherate (BF3 C4H10O), simultaneously acting as an anodizing agent. A pure, ordered TiO2 nanotubes array, as a reference sample, was also prepared in solution containing a standard etching compound: ammonium fluoride. The doped and pure titania...
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  24. 2014

  25. Lanthanide co-doped TiO2: the effect of metal type and amount on surface properties and photocatalytic activity

    J. Reszczyńska , T. Grzyb , J. Sobczak , W. Lisowski , M. Gazda , B. Ohtani , A. Zaleska-Medynska - APPLIED SURFACE SCIENCE - 2014
    Preparation of new rare earth metal-containing TiO2 nanocomposites (Nd3+/Er3+, Nd3+/Eu3+, Eu3+/Ho3+-TiO2) using sol–gel route and their photoactivity under visible and ultraviolet light is reported. The obtained photocatalysts were subsequently characterized by Brunauer–Emmett–Teller (BET) method, UV–Vis diffuse-reflectance spectroscopy (DRS), luminescence spectroscopy, X-ray photoelectron spectroscopy (XPS) and X-ray powder diffraction...
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  26. Visible light photoactivity of TiO2loaded with monometallic(Au or Pt) and bimetallic (Au/Pt) nanoparticles

    A. Gołąbiewska , W. Lisowski , M. Jarek , G. Nowaczyk , A. Zielińska-Jurek , A. Zaleska-Medynska - APPLIED SURFACE SCIENCE - 2014
    TiO2modified with monometallic (Au or Pt) and bimetallic (Au/Pt) nanoparticles have been preparedusing a water-in-oil microemulsion system (water/AOT/cyclohexane) followed by calcination step. Theeffect of metal ratio, reducing agent type (NaBH4or N2H4), TiO2matrix type (P-25, ST-01, TiO-5, TiO2nano-tubes or TiO2obtained by TIP hydrolysis) as well as calcination temperature (from 350 to 650◦C) weresystematically investigated. Obtained...
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  27. 2009

  28. CdS thin films obtained by thermal treatment of cadmium(II) complexprecursor deposited by MAPLE technique

    A. Rotaru , A. Mietlarek-Kropidłowska , C. Constantinescu , N. Scărişoreanu , M. Dumitru , M. Strankowski , P. Rotaru , V. Ion , C. Vasiliu , B. Becker , M. Dinescu - APPLIED SURFACE SCIENCE - 2009
    Cienkie warstwy kompleksu [Cd{SSi(O-But)3}(S2CNEt2)]2 zostały osadzone na podłożach Si przy użyciu techniki MAPLE (ablacja laserowa z zamrożoną matrycą). Otrzymanie warstw CdS było możliwe dzięki zastosowaniu obróbki termicznej podłoży z naniesionym prekursorem. Powierzchnia filmów była analizowana pod kątem morfologii przy użyciu mikroskopii sił atomowych (AFM) oraz pomiarów elipsometrycznych (SE).
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wyświetlono 64 razy