Natural deep eutectic solvent based ultrasound assisted liquid-liquid micro-extraction method for methyl violet dye determination in contaminated river water - Publikacja - MOST Wiedzy

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Natural deep eutectic solvent based ultrasound assisted liquid-liquid micro-extraction method for methyl violet dye determination in contaminated river water

Abstrakt

Simple and green natural deep eutectic solvent (NADES) based ultrasound assisted liquid-liquid micro-extraction (UA-LLME) method was developed for extraction and determination of methyl violet dye in contaminated river water samples using UV/Vis spectrophotometry. Choline chloride - decanoic acid based natural deep eutectic solvent was used for extraction. Important analytical parameters like pH, deep eutectic solvent volume/phase ratio, tetrahydrofuran volume, sonication time, and temperature were optimized. Limit of detection (LOD) and limit of quantification (LOQ) were 2.20 μg/L and 7.34 μg/L respectively. Relative standard deviation was 2.35–3.21%. Linearity of method was investigated in a concentration range 10–400 μg/L. Enrichment factor was calculated as 20. For 20 mL sample, the optimized parameters were as deep eutectic solvent volume 1.5 mL, tetrahydrofuran volume was 0.6 mL, pH = 6, sonication time 2 min. The optimized method was tested for extraction of methyl violet in real water samples confirming its applicability in routine environmental analysis.

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Informacje szczegółowe

Kategoria:
Publikacja w czasopiśmie
Typ:
artykuły w czasopismach
Opublikowano w:
Water Resources and Industry nr 29,
ISSN: 2212-3717
Język:
angielski
Rok wydania:
2023
Opis bibliograficzny:
Haq H., Wali A., Safi F., Arain M. B., Kong L., Boczkaj G.: Natural deep eutectic solvent based ultrasound assisted liquid-liquid micro-extraction method for methyl violet dye determination in contaminated river water// Water Resources and Industry -Vol. 29, (2023), s.100210-
DOI:
Cyfrowy identyfikator dokumentu elektronicznego (otwiera się w nowej karcie) 10.1016/j.wri.2023.100210
Źródła finansowania:
Weryfikacja:
Politechnika Gdańska

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