Optimization of liquid chromatographic separation of pharmaceuticals within green analytical chemistry framework - Publikacja - MOST Wiedzy

Twoje konto

zaloguj

Wyszukiwarka

Optimization of liquid chromatographic separation of pharmaceuticals within green analytical chemistry framework

Abstrakt

The contribution is aimed at the development of methodology that allows to consider green analytical chemistry criteria during optimization of liquid chromatographic separation with design of experiment. The objectives of the optimization are maximization of peak areas of five non-steroid anti-inflammatory drugs, maximization of resolution between peaks, with simultaneous shortening of chromatographic separation time and minimization of mobile phase environmental impact. This is obtained with design of experiment to consider many experimental conditions and Derringer's desirability function to combine many optimization objectives. The possibilities of introduction different green analytical chemistry metrics are discussed and the methodology of mobile phase greenness assessment is proposed. The optimal response for all objectives is obtained for 0.96 mL min−1 of mobile phase flow rate, 61% of MeOH content, temperature of 25°C and pH equal to 4.5. The separation takes less than 9 min.

Cytowania

  • 1 6

    CrossRef

  • 0

    Web of Science

  • 1 6

    Scopus

Autorzy (2)

Cytuj jako

Pełna treść

pobierz publikację
pobrano 83 razy
Wersja publikacji
Accepted albo Published Version
Licencja
Creative Commons: CC-BY-NC-ND otwiera się w nowej karcie

Słowa kluczowe

Informacje szczegółowe

Kategoria:
Publikacja w czasopiśmie
Typ:
artykuły w czasopismach
Opublikowano w:
MICROCHEMICAL JOURNAL nr 152, strony 1 - 5,
ISSN: 0026-265X
Język:
angielski
Rok wydania:
2020
Opis bibliograficzny:
Dogan A., Tobiszewski M.: Optimization of liquid chromatographic separation of pharmaceuticals within green analytical chemistry framework// MICROCHEMICAL JOURNAL -Vol. 152, (2020), s.1-5
DOI:
Cyfrowy identyfikator dokumentu elektronicznego (otwiera się w nowej karcie) 10.1016/j.microc.2019.104323
Bibliografia: test
  1. J. Namieśnik, Trends in environmental analytics and monitoring, Crit. Rev. Anal. Chem. 30 (2000) 221-269 https://doi.org/10.1080/10408340091164243. otwiera się w nowej karcie
  2. P.T. Anastas, Green chemistry and the role of analytical methodology development, Crit. Rev. Anal. Chem. 29 (1999) 167-175 https://doi.org/10.1080/ 10408349891199356. otwiera się w nowej karcie
  3. M. Koel, M. Kaljurand, Application of the principles of green chemistry in analytical chemistry, Pure Appl. Chem. 78 (2006) 1993-2002 https://doi.org/10.1351/ pac200678111993. otwiera się w nowej karcie
  4. M. Tobiszewski, A. Mechlińska, J. Namieśnik, Green analytical chemistry-theory and practice, Chem. Soc. Rev. 39 (2010) 2869-2878 https://doi.org/10.1039/ B926439F. otwiera się w nowej karcie
  5. C.J. Welch, N. Wu, M. Biba, R. Hartman, T. Brkovic, X. Gong, ... L. Zhou, Greening analytical chromatography, TrAC Trends Anal. Chem. 29 (7) (2010) 667-680 https://doi.org/10.1016/j.trac.2010.03.008. otwiera się w nowej karcie
  6. J. Płotka, M. Tobiszewski, A.M. Sulej, M. Kupska, T. Gorecki, J. Namieśnik, Green chromatography, J. Chromatogr. A 1307 (2013) 1-20 https://doi.org/10.1016/j. chroma.2013.07.099. otwiera się w nowej karcie
  7. H. Shaaban, New insights into liquid chromatography for more eco-friendly analysis of pharmaceuticals, Anal. Bioanal. Chem. 408 (25) (2016) 6929-6944 https://doi. org/10.1007/s00216-016-9726-2. otwiera się w nowej karcie
  8. H.M. Mohamed, Green, environment-friendly, analytical tools give insights in pharmaceuticals and cosmetics analysis, Trends Anal. Chem. 66 (2015) 176-192 https://doi.org/10.1016/j.trac.2014.11.010. otwiera się w nowej karcie
  9. A. Gałuszka, Z. Migaszewski, J. Namieśnik, The 12 principles of green analytical chemistry and the significance mnemonic of green analytical practices, Trends Anal. Chem. 50 (2013) 78-84 https://doi.org/10.1016/j.trac.2013.04.010. otwiera się w nowej karcie
  10. D.B. Hibbert, Experimental design in chromatography: a tutorial review, J. Chromatogr. B 910 (2012) 2-13 https://doi.org/10.1016/j.jchromb.2012.01. 020Get. otwiera się w nowej karcie
  11. G. Derringer, R. Suich, Simultaneous optimization of several response variables, J. Qual. Tech. 12 (1980) 214-219 https://doi.org/10.1080/00224065.1980. 11980968. otwiera się w nowej karcie
  12. M.A. Bezerra, S.L.C. Ferreira, C.G. Novaes, A.M.P. dos Santos, G.S. Valasques, U.M. da Mata Cerqueira, J.P. dos Santos Alves, Simultaneous optimization of multiple responses and its application in analytical chemistry-a review, Talanta 194 (2019) 941-959 https://doi.org/10.1016/j.talanta.2018.10.088. otwiera się w nowej karcie
  13. L.V. Candioti, M.M. De Zan, M.S. Camara, H.C. Goicoechea, Experimental design and multiple response optimization. Using the desirability function in analytical methods development, Talanta 124 (2014) 123-138 https://doi.org/10.1016/j. talanta.2014.01.034. otwiera się w nowej karcie
  14. N.H. Abou-Taleb, D.R. El-Wasseef, D.T. El-Sherbiny, S.M. El-Ashry, Multiobjective optimization strategy based on desirability functions used for the microemulsion liquid chromatographic separation and quantification of norfloxacin and tinidazole in plasma and formulations, J. Sep. Sci. 38 (2015) 901-908 https://doi.org/10. 1002/jssc.201401203. otwiera się w nowej karcie
  15. K. Abu-Izza, L. Garcia-Contreras, D.R. Lu, Preparation and evaluation of zidovu- dine-loaded sustained-release microspheres. 2. Optimization of multiple response variables, J. Pharm. Sci. 85 (1996) 572-576 https://doi.org/10.1021/js960021k. otwiera się w nowej karcie
  16. P. Barmpalexis, F.I. Kanaze, E. Georgarakis, Developing and optimizing a validated isocratic reversed-phase high-performance liquid chromatography separation of nimodipine and impurities in tablets using experimental design methodology, J. Pharm. Biomed. Anal. 49 (2009) 1192-1202 https://doi.org/10.1016/j.jpba.2009. 03.003. otwiera się w nowej karcie
  17. M. Cruz-Monteagudo, F. Borges, M.N.D. Cordeiro, Desirability-based multiobjective optimization for global QSAR studies: application to the design of novel NSAIDs with improved analgesic, antiinflammatory, and ulcerogenic profiles, J. Comput. Chem. 29 (2008) 2445-2459 https://doi.org/10.1002/jcc.20994. otwiera się w nowej karcie
  18. P. Cutroneo, M. Beljean, R.P.T. Luu, A.-.M. Siouffi, Optimization of the separation of some psychotropic drugs and their respective metabolites by liquid chromato- graphy, J. Pharm. Biomed. Anal. 41 (2006) 333-340 https://doi.org/10.1016/j. jpba.2005.10.050. otwiera się w nowej karcie
  19. R. Djang'eing'a Marini, P. Chiap, B. Boulanger, W. Dewe, P. Hubert, J. Crommen, LC method for the simultaneous determination of R-timolol and other closely related impurities in S-timolol maleate: optimization by use of an experimental design, J. Sep. Sci. 26 (2003) 809-817 https://doi.org/10.1002/jssc.200301367. otwiera się w nowej karcie
  20. P. Giriraj, T. Sivakkumar, Development and validation of a rapid chemometrics assisted RP-HPLC with PDA detection method for the simultaneous estimation of pyridoxine HCl and doxylamine succinate in bulk and pharmaceutical dosage form, Chromatogr. Res. Int. 2014 (2014), http://dx.doi.org/10.1155/2014/827895. otwiera się w nowej karcie
  21. P. Giriraj, T. Sivakkumar, A rapid-chemometrics assisted RP-HPLC method with PDA detection for the simultaneous estimation of ofloxacin and nimorazole in pharmaceutical formulation, J. Liq. Chromatogr. Related Technol. 38 (2015) 904-910 https://doi.org/10.1080/10826076.2014.991870. otwiera się w nowej karcie
  22. N. Hatambeygi, G. Abedi, M. Talebi, Method development and validation for op- timised separation of salicylic, acetyl salicylic and ascorbic acid in pharmaceutical formulations by hydrophilic interaction chromatography and response surface methodology, J. Chromatogr. A 1218 (2011) 5995-6003 https://doi.org/10.1016/ j.chroma.2011.06.009. otwiera się w nowej karcie
  23. V.S. Janardhanan, R. Manavalan, K. Valliappan, Chemometric technique for the optimization of chromatographic system: simultaneous HPLC determination of ro- suvastatin, telmisartan, ezetimibe and atorvastatin used in combined cardiovascular therapy, Arab. J. Chem. 9 (2016) S1378-S1387 https://doi.org/10.1016/j.arabjc. 2012.03.001. otwiera się w nowej karcie
  24. B. Otašević, S. Milovanović, M. Zečević, J. Golubović, A. Protić, UPLC method for determination of moxonidine and its degradation products in active pharmaceutical ingredient and pharmaceutical dosage form, Chromatographia 77 (2014) 109-118 https://doi.org/10.1007/s10337-013-2580-x. otwiera się w nowej karcie
  25. T. Sivakumar, R. Manavalan, C. Muralidharan, K. Valliappan, Multi-criteria deci- sion making approach and experimental design as chemometric tools to optimize HPLC separation of domperidone and pantoprazole, J. Pharm. Biomed. Anal. 43 (2007) 1842-1848 https://doi.org/10.1016/j.jpba.2006.12.007. otwiera się w nowej karcie
  26. T. Sivakumar, R. Manavalan, C. Muralidharan, K. Valliappan, An improved HPLC method with the aid of a chemometric protocol: simultaneous analysis of amlodi- pine and atorvastatin in pharmaceutical formulations, J. Sep. Sci. 30 (2007) 3143-3153 https://doi.org/10.1002/jssc.200700148. otwiera się w nowej karcie
  27. R.S. Sundar, K. Valliappan, An improved RP-HPLC method for the simultaneous estimation of aspirin, atorvastatin, and clopidogrel in pharmaceutical formulation using experimental design methodology, Int. J. Pharm. Pharm. Sci. 6 (2014) 279-283. otwiera się w nowej karcie
  28. R. Suresh, R. Manavalan, K. Valliappan, Developing and optimizing a validated RP- HPLC method for the analysis of amlodipine and ezetimibe with atorvastatin in pharmaceutical dosage forms applying response surface methodology, Int. J. Pharm. Pharm. Sci. 4 (2012) 550-558.
  29. P. Venkatesan, V.S. Janardhanan, C. Muralidharan, K. Valliappan, Improved HPLC method with the aid of chemometric strategy: determination of loxoprofen in pharmaceutical formulation, Acta Chim. Slov. 59 (2012) 242-248.
  30. L.H. Keith, L.U. Gron, J.L. Young, Green analytical methodologies, Chem. Rev. 107 (2007) 2695-2708 https://doi.org/10.1021/cr068359e. otwiera się w nowej karcie
  31. A. Gałuszka, Z.M. Migaszewski, P. Konieczka, J. Namieśnik, Analytical Eco-Scale for assessing the greenness of analytical procedures, TrAC Trends Anal. Chem. 37 (2012) 61-72 https://doi.org/10.1016/j.trac.2012.03.013. otwiera się w nowej karcie
  32. J. Płotka-Wasylka, A new tool for the evaluation of the analytical procedure: green analytical procedure index, Talanta 181 (2018) 204-209 https://doi.org/10.1016/ j.talanta.2018.01.013. otwiera się w nowej karcie
  33. M. Tobiszewski, J. Namieśnik, Scoring of solvents used in analytical laboratories by their toxicological and exposure hazards, Ecotoxicol. Environ. Saf. 120 (2015) 169-173 https://doi.org/10.1016/j.ecoenv.2015.05.043. otwiera się w nowej karcie
  34. F.P. Byrne, S. Jin, G. Paggiola, T.H. Petchey, J.H. Clark, T.J. Farmer, A.J. Hunt, C.R. McElroy, J. Sherwood, Tools and techniques for solvent selection: green sol- vent selection guides, Sustain. Chem. Process. 4 (2016) 7 https://doi.org/10.1186/ s40508-016-0051-z. otwiera się w nowej karcie
  35. D. Prat, J. Hayler, A. Wells, A survey of solvent selection guides, Green Chem. 16 (2014) 4546-4551 https://doi.org/10.1039/C4GC01149J. otwiera się w nowej karcie
  36. P. Bigus, J. Namieśnik, M. Tobiszewski, Implementation of multicriteria decision analysis in design of experiment for dispersive liquid-liquid microextraction opti- mization for chlorophenols determination, J. Chromatogr. A 1553 (2018) 25-31 https://doi.org/10.1016/j.chroma.2018.04.018. otwiera się w nowej karcie
  37. Y. Gaber, U. Törnvall, M.A. Kumar, M.A. Amin, R. Hatti-Kaul, HPLC-EAT (Environmental Assessment Tool): a tool for profiling safety, health and environ- mental impacts of liquid chromatography methods, Green Chem. 13 (8) (2011) 2021-2025, https://doi.org/10.1039/C0GC00667J. otwiera się w nowej karcie
  38. M.B. Hicks, W. Farrell, C. Aurigemma, L. Lehmann, L. Weisel, K. Nadeau, ... otwiera się w nowej karcie
  39. P. Ferguson, Making the move towards modernized greener separations: introduc- tion of the analytical method greenness score (AMGS) calculator, Green Chem. 21 (7) (2019) 1816-1826, https://doi.org/10.1039/C8GC03875A. otwiera się w nowej karcie
Weryfikacja:
Politechnika Gdańska

wyświetlono 169 razy

Publikacje, które mogą cię zainteresować

Chemometrics approaches to green analytical chemistry procedure development

2021

Diethyl carbonate as a green extraction solvent for chlorophenol determination with dispersive liquid–liquid microextraction

2019

Rapid multi-objective design of integrated on-chip inductors by means of Pareto front exploration and design extrapolation

2019

Multi-objective antenna design by means of sequential domain patching

2016
Meta Tagi