Organic Acids and Polyphenols Determination in Polish Wines by Ultrasound-Assisted Solvent Extraction of Porous Membrane-Packed Liquid Samples - Publikacja - MOST Wiedzy

Twoje konto

zaloguj

Wyszukiwarka

Organic Acids and Polyphenols Determination in Polish Wines by Ultrasound-Assisted Solvent Extraction of Porous Membrane-Packed Liquid Samples

Abstrakt

In the near future, Poland is going to have more and more favorable conditions for viticulture. Organic acids and polyphenols are among the most commonly analyzed compounds due to their beneficial properties for human health and their importance in the winemaking process. In this work, a new technique involving ultrasound-assisted solvent extraction of porous membrane-packed liquid samples (UASE-PMLS) was for the first time described and applied for real samples. The methodology based on UASE-PMLS for organic acids and polyphenols in wine samples was optimized and validated. Using the new technique coupled to GC–MS, organic acids and polyphenols were evaluated in Polish wine samples. Extraction solvent, extraction temperature, derivatization time and sample pH were optimized. Chemometric tools were used for data treatment. Good linearity was obtained for the concentration ranges evaluated with r values between 0.9852 and 0.9993. All parameters of method validation (intra- and inter-day precision and matrix effect) were over 80% with coefficient of variation (CV) up to 17%. Recovery was between (92.0 ± 8.5)% and (113 ± 16)%. Finally, green assessment was evaluated using Analytical Eco-Scale and Green Analytical Procedure Index (GAPI). The UASE-PMLS is characterized by many advantages, e.g., the extraction process is fast and easy coupled to GC–MS. Regarding other extraction techniques, the amount of used solvent is minimum, and no waste is generated. Therefore, it is an environmentally friendly technique.

Cytowania

  • 2 6

    CrossRef

  • 0

    Web of Science

  • 2 5

    Scopus

Autorzy (4)

Cytuj jako

Pełna treść

pobierz publikację
pobrano 81 razy
Wersja publikacji
Accepted albo Published Version
Licencja
Creative Commons: CC-BY otwiera się w nowej karcie

Słowa kluczowe

Informacje szczegółowe

Kategoria:
Publikacja w czasopiśmie
Typ:
artykuły w czasopismach
Opublikowano w:
MOLECULES nr 24, strony 4376 - 4396,
ISSN: 1420-3049
Język:
angielski
Rok wydania:
2019
Opis bibliograficzny:
Robles A., Fabjanowicz M., Płotka-Wasylka J., Konieczka P.: Organic Acids and Polyphenols Determination in Polish Wines by Ultrasound-Assisted Solvent Extraction of Porous Membrane-Packed Liquid Samples// MOLECULES -Vol. 24,iss. 23 (2019), s.4376-4396
DOI:
Cyfrowy identyfikator dokumentu elektronicznego (otwiera się w nowej karcie) 10.3390/molecules24234376
Bibliografia: test
  1. Tarko, T.; Duda-Chodak, A.; Sroka, P.; Satora, P.; Jurasz, E. Polish wines: Characteristics of cool-climate wines. J. Food Compos. Anal. 2010, 23, 463-468. [CrossRef] otwiera się w nowej karcie
  2. Jurado-Sánchez, B.; Ballesteros, E.; Gallego, M. Gas chromatographic determination of 29 organic acids in foodstuffs after continuous solid-phase extraction. Talanta 2011, 84, 924-930. [CrossRef] otwiera się w nowej karcie
  3. Sumby, K.M.; Grbin, P.R.; Jiranek, V. Implications of new research and technologies for malolactic fermentation in wine. Appl. Microbiol. Biotechnol. 2014, 98, 8111-8132. [CrossRef] [PubMed] otwiera się w nowej karcie
  4. Iqbal, K.; Khan, A.; Ali, M.M.; Khattak, K. Biological Significance of Ascorbic Acid (Vitamin C) in Human Health-A Review. Pak. J. Nutr. 2004, 3, 5-13.
  5. Bortz, J.D.; Kirschner, M.I. A1 Methods and Compositions for Enhancing Iron Absorption Patent Application Publication Pub. No. US 2016/0022631, 28 June 2016.
  6. Nagai, R.; Nagai, M.; Shimasaki, S.; Baynes, J.W.; Fujiwara, Y. Biochemical and Biophysical Research Communications Citric acid inhibits development of cataracts, proteinuria and ketosis in streptozotocin (type 1) diabetic rats. Biochem. Biophys. Res. Commun. 2010, 393, 118-122. [CrossRef] [PubMed] otwiera się w nowej karcie
  7. Marunaka, Y. The Proposal of Molecular Mechanisms of Weak Organic Acids Intake-Induced Improvement of Insulin Resistance in Diabetes Mellitus via Elevation of Interstitial Fluid pH. Int. J. Mol. Sci. 2018, 19, 3244. [CrossRef] otwiera się w nowej karcie
  8. Tomás-Barberán, F.A. Los polifenoles de los alimentos y la salud. Aliment. Nutr. Y Salud 2003, 10, 41-53.
  9. Galarce-Bustos, O.; Novoa, L.; Pavon-Perez, J.; Henriquez-Aedo, K.; Aranda, M. Chemometric Optimization of QuEChERS Extraction Method for Polyphenol Determination in Beers by Liquid Chromatography with Ultraviolet Detection. Food Anal. Methods 2019, 12, 448-457. [CrossRef] otwiera się w nowej karcie
  10. Caprioli, G.; Boarelli, M.C.; Ricciutelli, M.; Sagratini, G.; Fiorini, D. Micro-scaled Quantitative Method to Analyze Olive Oil Polyphenols. Food Anal. Methods 2019, 12, 1133-1139. [CrossRef] otwiera się w nowej karcie
  11. Perumalla, A.V.S.; Hettiarachchy, N.S. Green tea and grape seed extracts-Potential applications in food safety and quality. Food Res. Int. 2011, 44, 827-839. [CrossRef] otwiera się w nowej karcie
  12. Ferrandino, A.; Carlomagno, A.; Baldassarre, S.; Schubert, A. Varietal and pre-fermentative volatiles during ripening of Vitis vinifera cv Nebbiolo berries from three growing areas. Food Chem. 2012, 135, 2340-2349. [CrossRef] [PubMed] otwiera się w nowej karcie
  13. Liang, Z.; Sang, M.; Fan, P.; Wu, B.; Wang, L.; Duan, W.; Li, S. Changes of Polyphenols, Sugars, and Organic Acid in 5 Vitis Genotypes during Berry Ripening. J. Food Sci. 2011, 76, 1231-1238. [CrossRef] [PubMed] otwiera się w nowej karcie
  14. Walorczyk, S.; Drozdzynski, D.; Gnusowski, B. Multiresidue determination of 160 pesticides in wines employing mixed-mode dispersive-solid phase extraction and gas chromatography-tandem mass spectrometry. Talanta 2011, 85, 1856-1870. [CrossRef] [PubMed] otwiera się w nowej karcie
  15. Tuzimski, T. Determination of pesticides in wines samples by HPLC-DAD and HPTLC-DAD. J. Liq. Chromatogr. Relat. Technol. 2012, 35, 1415-1428. [CrossRef] otwiera się w nowej karcie
  16. Raczkowska, J.; Mielcarz, G.; Howard, A.; Raczkowski, M. UPLC and Spectrophotometric Analysis of Polyphenols in Wines Available in the Polish Market. Int. J. Food Prop. 2011, 14, 514-522. [CrossRef] otwiera się w nowej karcie
  17. Adamski, J.; Kochana, J.; Nowak, P.; Parczewski, A. On the electrochemical biosensing of phenolic compounds in wines. J. Food Compos. Anal. 2016, 46, 1-6. [CrossRef] otwiera się w nowej karcie
  18. Plotka-Wasylka, J.; Rutkowska, M.; Cieslik, B.; Tyburcy, A.; Namieśnik, J. Determination of Selected Metals in Fruit Wines by Spectroscopic Techniques. J. Anal. Methods Chem. 2017, 2017, 5283917. [CrossRef] otwiera się w nowej karcie
  19. Plotka-Wasylka, J.; Namiesnik, J.; Klodzinska, E. Determination of Biogenic Amines in Wine using Micellar Electrokinetic Chromatography. J. Res. Anal. 2017, 3, 62-66. otwiera się w nowej karcie
  20. Piasta, A.M.; Jastrzebska, A.; Krzeminski, M.P.; Muziol, T.M.; Szlyk, E. New procedure of selected biogenic amines determination in wine samples by HPLC. Anal. Chim. Acta 2014, 834, 58-66. [CrossRef] otwiera się w nowej karcie
  21. Papageorgiou, M.; Lambropoulou, D.; Morrison, C.; Namiesnik, J.; Plotka-Wasylka, J. Direct solid phase microextraction combined with gas chromatography-Mass spectrometry for the determination of biogenic amines in wine. Talanta 2018, 183, 276-282. [CrossRef] otwiera się w nowej karcie
  22. Barros, P.E.; Moreira, N.; Pereira, E.G.; Gomes Ferreira Leite, S.; Moraes Rezende, C.; Guedes de Pinho, P. Development and validation of automatic HS-SPME with a gas chromatography-ion trap/mass spectrometry method for analysis of volatiles in wines. Talanta 2012, 101, 177-186. [CrossRef] [PubMed] otwiera się w nowej karcie
  23. Viñas, P.; Campillo, N.; Martínez-Castillo, N.; Hernández-Córdoba, M. Solid-phase microextraction on-fiber derivatization for the analysis of some polyphenols in wine and grapes using gas chromatography-mass spectrometry. J. Chromatogr. A 2009, 1216, 1279-1284. [CrossRef] [PubMed] otwiera się w nowej karcie
  24. Sajid, M.; Płotka-Wasylka, J. Combined extraction and microextraction techniques: Recent trends and future perspectives. Trends Anal. Chem. 2018, 103, 74-86. [CrossRef] otwiera się w nowej karcie
  25. Yang, P.; Li, H.; Wang, H.; Han, F.; Jing, S.; Yuan, C.; Guo, A.; Zhang, Y.; Xu, Z. Dispersive Liquid-Liquid Microextraction Method for HPLC Determination of Phenolic Compounds in Wine. Food Anal. Methods 2017, 10, 2383-2397. [CrossRef] otwiera się w nowej karcie
  26. Sun, S.Y.; Jiang, W.G.; Zhao, Y.P. Comparison of aromatic and phenolic compounds in cherry wines with different cherry cultivars by HS-SPME-GC-MS and HPLC. Int. J. Food Sci. Technol. 2012, 47, 100-106. [CrossRef] otwiera się w nowej karcie
  27. Hashim, S.N.N.S.; Schwarz, L.J.; Boysen, R.I.; Yang, Y.; Danylec, B.; Hearn, M.T.W. Rapid solid-phase extraction and analysis of resveratrol and other polyphenols in red wine. J. Chromatogr. A 2013, 1313, 284-290. [CrossRef] otwiera się w nowej karcie
  28. Antalick, G.; Perello, M.; Revel, G. De Development, validation and application of a specific method for the quantitative determination of wine esters by headspace-solid-phase microextraction-gas chromatography-Mass spectrometry. Food Chem. 2010, 121, 1236-1245. [CrossRef] otwiera się w nowej karcie
  29. Fariña, L.; Boido, E.; Carrau, F.; Dellacassa, E. Determination of volatile phenols in red wines by dispersive liquid-Liquid microextraction and gas chromatography-Mass spectrometry detection. J. Chromatogr. A 2007, 1157, 46-50. [CrossRef] otwiera się w nowej karcie
  30. Li, J.; Jia, S.; Jun, S.; Ji, S.; Won, S.; Lee, J. Ion-pair dispersive liquid-Liquid microextraction solidification of floating organic droplets method for the rapid and sensitive detection of phenolic acids in wine samples using liquid chromatography combined with a core-Shell particle column. J. Food Compos. Anal. 2016, 45, 73-79. [CrossRef] otwiera się w nowej karcie
  31. Fontana, A.R.; Bottini, R. High-throughput method based on quick, easy, cheap, effective, rugged and safe followed by liquid chromatography-multi-wavelength detection for the quantification of multiclass polyphenols in wines. J. Chromatogr. A 2014, 1342, 44-53. [CrossRef] otwiera się w nowej karcie
  32. Basheer, C.; Alnedhary, A.A.; Rao, B.S.M.; Valliyaveettil, S.; Lee, H.K. Development and Application of Porous Membrane-Protected Carbon Nanotube Micro-Solid-Phase Extraction Combined with Gas Chromatography/Mass Spectrometry. Anal. Chem. 2006, 78, 2853-2858. [CrossRef] [PubMed] otwiera się w nowej karcie
  33. Basheer, C.; Chong, H.G.; Hii, T.M.; Lee, H.K. Application of Porous Membrane-Protected Micro-Solid-Phase Extraction Combined with HPLC for the Analysis of Acidic Drugs in Wastewater. Anal. Chem. 2007, 79, 6845-6850. [CrossRef] [PubMed] otwiera się w nowej karcie
  34. Basheer, C.; Wong, W.; Makahleh, A.; Tameem, A.A.; Salhin, A.; Saad, B.; Lee, H.K. Hydrazone-based ligands for micro-solid phase extraction-high performance liquid chromatographic determination of biogenic amines in orange juice. J. Chromatogr. A 2011, 1218, 4332-4339. [CrossRef] [PubMed] otwiera się w nowej karcie
  35. Lashgari, M.; Basheer, C.; Lee, H.K. Application of surfactant-templated ordered mesoporous material as sorbent in micro-solid phase extraction followed by liquid chromatography-Triple quadrupole mass spectrometry for determination of perfluorinated carboxylic acids in aqueous. Talanta 2015, 141, 200-206. [CrossRef] otwiera się w nowej karcie
  36. Sajid, M.; Basheer, C.; Narasimhan, K.; Choolani, M.; Lee, H.K. Application of microwave-assisted micro-solid-phase extraction for determination of parabens in human ovarian cancer tissues. J. Chromatogr. B 2015, 1000, 192-198. [CrossRef] otwiera się w nowej karcie
  37. Sajid, M.; Wozniak, M.K.; Plotka-Wasylka, J. Ultrasound-assisted solvent extraction of porous membrane packed solid samples: A new approach for extraction of target analytes from solid samples. Microchem. J. 2019, 144, 117-123. [CrossRef] otwiera się w nowej karcie
  38. Dobrowolska-Iwanek, J.; Gąstoł, M.; Wanat, A.; Krośniak, M.; Jancik, M.; Zagrodzki, P. Wine of Cool-climate Areas in South Poland. S. Afr. J. Enol. Vitic. 2014, 35, 1-9. [CrossRef] otwiera się w nowej karcie
  39. Ohira, S.; Kuhara, K.; Shigetomi, A.; Yamasaki, T.; Kodama, Y.; Dasguota, P.K.; Toda, K. On-line electrodialytic matrix isolation for chromatographic determination of organic acids in wine. J. Chromatogr. A 2014, 1372, 18-24. [CrossRef] otwiera się w nowej karcie
  40. Zeravik, J.; Fohlerova, Z.; Milovanovic, M.; Kubesa, O.; Zeisbergerova, M.; Lacina, K.; Petrovic, A.; Glatz, Z.; Skladal, P. Various instrumental approaches for determination of organic acids in wines. Food Chem. 2016, 194, 432-440. [CrossRef] otwiera się w nowej karcie
  41. Minuti, L.; Pellegrino, R.M.; Tesei, I. Simple extraction method and gas chromatography-Mass spectrometry in the selective ion monitoring mode for the determination of phenols in wine. J. Chromatogr. A 2006, 1114, 263-268. [CrossRef] otwiera się w nowej karcie
  42. Anli, R.E.; Vural, N.; Kizile, E. An alternative method for the determination of some of the antioxidant phenolics in varietal Turkish red wines. J. Inst. Brew. 2008, 114, 239-245. [CrossRef] otwiera się w nowej karcie
  43. Šeruga, M.; Novak, I.; Jakobek, L. Determination of polyphenols content and antioxidant activity of some red wines by differential pulse voltammetry, HPLC and spectrophotometric methods. Food Chem. 2011, 124, 1208-1216. [CrossRef] otwiera się w nowej karcie
  44. Mato, I.; Suarez-Luque, S.; Huidoro, J.F. Simple determination of main organic acids in grape juice and wine by using capillary zone electrophoresis with direct UV detection. Food Chem. 2007, 102, 104-112. [CrossRef] otwiera się w nowej karcie
  45. Cunha, S.C.; Fernandes, J.O.; Faria, M.A.; Ferreira, I.M.P.L.V.O.; Ferreira, M.A. Quantification of Organic Acids in grape musts and Port Wines. CYTA J. Food 2002, 3, 212-216. otwiera się w nowej karcie
  46. do Nascimento Silva, F.L.; Schmidt, E.M.; Messias, C.L.; Nogueira Eberlin, M.; Sawaya Frankland, H.A.C. Quantitation of organic acids in wine and grapes by direct infusion electrospray ionization mass spectrometry. Anal. Methods 2015, 7, 53-62. [CrossRef] otwiera się w nowej karcie
  47. Bai, S.; Cui, C.; Liu, J.; Li, P.; Li, Q.; Bi, K. Quantification of polyphenol composition and multiple statistical analyses of biological activity in Portuguese red wines. Eur. Food Res. Technol. 2018, 244, 2007-2017. [CrossRef] otwiera się w nowej karcie
  48. Gonçalves, J.; Mendes, B.; Silva, C.L.; Câmara, J.S. Development of a novel microextraction by packed sorbent-based approach followed by ultrahigh pressure liquid chromatography as a powerful technique for quantification phenolic constituents of biological interest in wines. J. Chromatogr. A 2012, 1229, 13-23. [CrossRef] otwiera się w nowej karcie
  49. Plotka-Wasylka, J. A new tool for the evaluation of the analytical procedure: Green Analytical Procedure Index. Talanta 2018, 181, 204-209. [CrossRef] otwiera się w nowej karcie
  50. Konieczka, P.; Namieśnik, J. Quality Assurance and Quality Control in the Analytical Chemical Laboratory. A Practical Approach, 2nd ed.; CRC Press Taylor & Francis Group: Boca Raton, FL, USA, 2018; ISBN 9781138196728. otwiera się w nowej karcie
  51. Sajid, M.; Basheer, C.; Alsharaa, A.; Narasimhan, K.; Buhmeida, A.; Qahtani, M.; Al-ahwal, M.S. Development of natural sorbent based micro-solid-phase extraction for determination of phthalate esters in milk samples. Anal. Chim. Acta 2016, 924, 35-44. [CrossRef] otwiera się w nowej karcie
  52. Sample Availability: Samples of the compounds are available from the authors. © 2019 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (http://creativecommons.org/licenses/by/4.0/). otwiera się w nowej karcie
Weryfikacja:
Politechnika Gdańska

wyświetlono 113 razy

Publikacje, które mogą cię zainteresować

Determination and identification of organic acids in wine samples. Problems and challenges.

2019

Multivariate Statistical Analysis for Mutual Dependence Assessment of Selected Polyphenols, Organic Acids and Metals in Cool-Climate Wines

2022

Metals and metal-binding ligands in wine: Analytical challenges in identification.

2021

Detection of Bioactive Compounds in Organically and Conventionally Grown Asparagus Spears

2018
Meta Tagi