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  • Raman spectra of CPMH and CPMD

    Dane Badawcze
    open access

    These data contains Raman spectra of CPMH and CPMD. Raman scattering was measured with a RenishawmicroRaman spectrometer (785 nm). Sample abbreviations (CPMH, CPMD) are in agreement with the markings used in the linked publication. 

  • The results of the nitrogen adsorption/desorption measurements of CPMD and CPMH

    Dane Badawcze
    open access

    The results of the nitrogen adsorption/desorption measurements of CPMD and CPMH. The adsorption/desorption isothermswere carried out at 77 K using a Quantachrome Autosorb-1C-MS instrument. Sample abbreviations (CPMD, CPMH) are in agreement with the markings used in the linked publication. 

  • SEM (scanning electron microscopy) and TEM (transmission electron microscopy) images of PMD and PMH

    Dane Badawcze
    open access

    These data contains SEM (scanning electron microscopy) and TEM (transmission electron microscopy) images of PMD and PMH. TEM was performed on a FEI Tecnai F30 transmission electron microscope operating at an acceleration voltage of 200 kV. SEM was done with a SEM, XL30ESEM-FEG with an acceleration voltage of 20 KV. Sample abbreviations (PMH, PMD) are...

  • CV (cyclic voltammetry) curves of the CPMD sample at different scan rates

    Dane Badawcze
    open access

     These data contain CV curves of CPMD obtained at a scan rate from 1 mV s−1 to 20 mV s−1. Sample abbreviations (CPMD) are in agreement with the markings used in the linked publication. 

  • Evaluation of the electrochemical performance of CPMD in ZICs with 3M ZnSO4 electrolyte

    Dane Badawcze
    open access

    These data contain the results of the electrochemical performance measurements of CPMD in ZICs with 3M ZnSO4 electrolyte, incl. CGD (galvanostatic charge-discharge ) curve and cycling stability of CPMD. Sample abbreviations (CPMD) are in agreement with the markings used in the linked publication. 

  • XLS file with the key results from the experimental analysis of the imperfect dome's state of displacements

    Dane Badawcze
    embargo

    This dataset consists of an XLS file with the key results from the experimental analysis of the imperfect dome's state of displacements.

  • Thermal behavior of TeOx xerogel powder under different atmospheres

    Dane Badawcze
    open access - seria: TeO2-based materials

    The DataSet contains the results of the thermal behavior of the TeOx xerogel powder measured under different atmospheres. The material was obtained by the sol-gel method.  The starting solution was prepared by mixing telluric acid (precursor) with thetraetylene glycol, water, and ethanol. The sol was obtained by vigorously stirring precursor solution...

  • Thermal stability of vanadium xerogel powder under different atmpshere

    Dane Badawcze
    open access - seria: Vanadium oxides

    The DataSet contains the results of the thermal behavior of the vanadium xerogel powder. The information about xerogel powder synthesis is described in the Journal of Nanomaterials.

  • Thermal behaviour of vanadium xerogel powder under oxidizing atmosphere

    Dane Badawcze
    open access - seria: Vanadium oxides

    The DataSet contains the results of the thermal behavior of the vanadium xerogel powder. The information about xerogel powder synthesis is described in the Journal of Nanomaterials.

  • Changes in heat of vanadium xerogel powder under different atmosphere

    Dane Badawcze
    open access - seria: Vanadium oxides

    The DataSet contains the DSC curves of the vanadium xerogel powder. The information about xerogel powder synthesis is described in the Journal of Nanomaterials.

  • Thermal behaviour of vanadium xerogel powder under argon atmosphere

    Dane Badawcze
    open access - seria: Vanadium oxides

    The DataSet contains the results of the thermal behavior of the vanadium xerogel powder. The information about xerogel powder synthesis is described in the Journal of Nanomaterials.

  • XPS study of the YST ceramics

    Dane Badawcze
    open access

    Yttrium-doped strontium titanate  was prepared via conventional solid-state reaction method from Y2O3 (Sigma Aldrich, 99,9%), TiO2 (Sigma Aldrich, 99%) and SrCO3 (Sigma Aldrich,98%). For comparision, two other techniques were used for synthesis: Pechini and wet methods. Both kind of samples were measured, after and before reduction process (in a hydrogen)....

  • Continuum orbitals in low energy scattering of electrons from Ar, Kr, Xe, Rn and Og atoms

    Dane Badawcze
    open access

    The dataset includes relativistic continuum electron wave functions (continuum orbitals, continuum spinors) for elastic scattering of electrons from Argon (Ar), Krypton (Kr), Xenon (Xe), Radon (Rn) and Oganesson (Og) atoms, calculated using the Multiconfiguration Dirac-Hartree-Fock method (MCDHF), at very low electron energies (0.0001 - 0.001 eV). Only...

  • XPS analysis of TBBO glass

    Dane Badawcze
    open access

    Glasses and glass-ceramics with nominal composition 73 TeO2– 4BaO– 3Bi2O3–18SrF2-2RE2O3 (where RE = Eu, Dy) have been synthesized by conventional melt-quenching technique and subsequent heat treatment at 370 °C for 24 h in air atmosphere. Various Eu3+ to Dy3+ molar ratio have been applied to investigate luminescence properties in both glass and glass-ceramic...

  • XPS data of MXene catalyst

    Dane Badawcze
    open access

    Data contain results from XPS measurement of the Ti3C2Tx MXenes produced via acidic etching aluminum from MAX Phase (Ti3C2-Al-Ti3C2-Al-Ti3C2) using 48% HF etching agent (MXene HF). The X-ray spectroscopy (XPS) measurements were conducted using Mg Ka (hn = 1253.6 eV) radiation in a Prevac (Poland) system equipped with a Scienta SES 2002 (Sweden) electron...

  • The XAS spectra of O-K edges, M-L edges and Ce-M edges in Ce0.9M0.1O2

    Dane Badawcze
    embargo - seria: Ceria

    The dataset consists of XAS spectra of O-K edges, M-L edges of Ce0.9M0.1O2 (where M=Mn, Fe, Co, Ni, Cu) synthesised by reverse microemulsion method. XAS spectra were collected at PIRX beamline in SOLARIS National Synchrotron Radiation Centre. Measurements were perfomed under ultra high vacuum in total electron yield (TEY) mode. 

  • XPS-TiO2 heated in H2

    Dane Badawcze
    open access

    These XPS spectra were recorded for TiO2 heat-treated at 450-600oC in H2. Surface oxygen groups were determined. Deconvolution of Ti 2p peak allowed to determine Ti3+ on the titania surface.

  • Thermal behaviour of vanadium xerogel powder under different inert atmosphere

    Dane Badawcze
    open access - seria: Vanadium oxides

    The DataSet contains the results of the thermal behavior of the vanadium xerogel powder. The information about xerogel powder synthesis is described in the Journal of Nanomaterials.

  • The 3d Ce XPS spectra of Ce0.9M0.1O2

    Dane Badawcze
    embargo - seria: Ceria

    The dataset consists of 3d Ce XPS of Ce0.9M0.1O2 where (M=Mn, Fe, Co, Ni, Cu). X-ray Photoelectron Spectroscopy analysis (XPS) was performed using X-ray photoelectron spectrometer Omnicron NanoTechnology with 128-channel collector. XPS measurements were undertaken in ultra-high vacuum conditions, below 1.1x10-8 mbar. Photoelectrons were excited by an...

  • The XPS spectra of LSCNT sintered at 1200C

    Dane Badawcze
    open access - seria: Exsolution

    The dataset includes XPS spectra of La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s sintered at various temperatures under air atmosphere for 12 h. Samples were produced using aqueous soft chemistry methods (Pechini). The XPS spectra were collected for all species. 

  • XPS analysis of the GO based materials

    Dane Badawcze
    open access

    Graphene oxides samples were measured by XPS method. The X-ray photoemission spectroscopy measurements were carried out with Omicron NanoTechnology UHV equipment. The hemispherical spectrophotometer was equipped with a 128-channel collector. The XPS measurements were performed at room temperature at a pressure below 1.1 × 10−8 mBar. The photoelectrons...

  • SPTNO ceramics measured by XPS method

    Dane Badawcze
    open access

    SPTNO (Sr-Pr-Ti-Ni-O) ceramic were manufactured by solid state reaction, from oxides compounds. Synthesis conducted in air atmosphere at temperature in a range of 800-900 deg. Chemical composition of prepared materials were measured by XPS (X-Ray photoemision spectroscopy) method. UHV OmicronNanotechnology system with 128 channel Argus hemispherical...

  • Thermal behaviour of vanadium xerogel powder and V2O5 nanorods under helium atmosphere

    Dane Badawcze
    open access - seria: Vanadium oxides

    The DataSet contains the results of the thermal behavior of the vanadium xerogel powder and V2O5 nanorods obtained at 650C. The information about xerogel powder and V2O5 nanorods synthesis is described in the Journal of Nanomaterials.

  • XRD-TiO2 and SiO2

    Dane Badawcze
    open access

    Data contain results from XRD measurements of amorphous silica and TiO2 of antase and rutile phases. The commercial TiO2 named as P25 produced by Evonik was also analyzed.

  • XPS study of the TiO2-WO2 composites

    Dane Badawcze
    open access

    Valence state of W and Ti was measured in a TiO2-WO3 composites with a various composition.Powder samples of pure titanium dioxide, tungsten oxide and mix of 50% titanium oxide and 50% od tungsten oxide were measured.  Oxides were annealed at the temperature in the range of 300 Celsius degree up to 900 deg. Measurements were performed by XPS UHV Omicron...

  • Depth XPS profile of vanadium pentoxide

    Dane Badawcze
    open access

    Vanadium pentoxide sample was manufactured by sol-gel method and deposited on a substrate by spin coating technique. To determine depth profile of chemical composition of thin film, etching by Argon ion gun was used. Thin film was etched three times. Chemical composition was measured by XPS method.

  • XPS analysis of strontium titanate ceramics

    Dane Badawcze
    open access

    The chemical composition of the strontium titanite doped with yttrium and iron ceramic samples was investigated. Samples of Y0.07Sr0.93Ti0.8Fe0.2 were prepared by solid phase reaction and sintered for 24 and 48 hours. Chemical composition was measured by UHV OmicronNanotechnology XPS system.  The analysis confirmed the chemical composition of the ceramics...

  • XPS study of the NH4-VOx powders

    Dane Badawcze
    open access

    Vanadium pentoxide samples were prepared by sol-gel method. The starting solution was prepared by mixing vanadium (V) oxytripropoxide (Aldrich) in an anhydrous ethanol as solvent and acetylacetone. By drying the sol at 323 K for 48 h, it transforms via gel into a xerogel powder. Next, the precursor powder was pressed into the disk-shaped pellets. Samples...

  • The 2p XPS spectra of transition metals in Ce0.9M0.1O2

    Dane Badawcze
    embargo - seria: Ceria

    The dataset consists of 2p XPS spectra of transition metals in Ce0.9M0.1O2 where (M=Mn, Fe, Co, Ni, Cu). X-ray Photoelectron Spectroscopy analysis (XPS) was performed using X-ray photoelectron spectrometer Omnicron NanoTechnology with 128-channel collector. XPS measurements were undertaken in ultra-high vacuum conditions, below 1.1x10-8 mbar. Photoelectrons...

  • XPS study of the lithium titanate doped by copper

    Dane Badawcze
    open access

    Lithium titanate doped by copper was measured by X-ray photoemission spectroscopy. For sol-gel synthesis lithium acetate dehydrate from Alfa Aesar GmbH &Co and titanium (IV) butoxide 97% from Aldrich were used as reagents. Copper (II) nitrate from Alfa Aesar was used as a source of Cu dopant. It was added in the proper weight to get an x index equal...

  • Surface modifcation of PMMA polymer detected by XPS

    Dane Badawcze
    open access

    In order to obtain the experimental specimens, four PMMA/PC61BM samples with the following  mass proportions were prepared: 10%, 20%, 30%, and 40%. In addition, as a reference, a PMMA sample without  PC61BM was prepared as well. For the fabrication process, PC61BM 99.5% (Solenne BV), chloroform HPLC  (Sigma Aldrich), and PMMA (commercially available...

  • XRD patterns of V2O5 nanostructures

    Dane Badawcze
    open access - seria: Vanadium oxides

    The DataSet contains the XRD patterns of vanadium pentaoxide nanostructures obtained by the sol-gel with different annealing temperatures under synthetic air. The results show that crystallinity dependent on the annealing temperature.

  • XRD patterns of V2O3 nanostructures

    Dane Badawcze
    open access - seria: Vanadium oxides

    The DataSet contains the XRD patterns of V2O3 nanostructures obtained by the sol-gel with different reaction conditions. The xerogel powder was annealing under a reducing atmosphere (94% Ar, 6% H2) in the temperature range 350-700C. The results show that crystallinity dependent on the annealing temperature.

  • XRD patterns of MXenes catalysts

    Dane Badawcze
    open access

    Data contain results from XRD measurements of the Ti3C2Tx MXenes produced via acidic etching aluminum from MAX Phase (Ti3C2-Al-Ti3C2-Al-Ti3C2) using different etching agents, HF/HCl and HF/H2SO4 with different weight ratios (1:3, 1:4, and 1:5). The samples were labeled as MXene HF/HCl X:Y and MXene HF/H2SO4 X:Y, where X:Y means the acids weight ratios....

  • XRD patterns of TeOx powder

    Dane Badawcze
    open access - seria: TeO2-based materials

    The DataSet contains the XRD patterns of the TeOx powder. The material was obtained by the sol-gel method.  The starting solution was prepared by mixing telluric acid (precursor) with thetraetylene glycol, water, and ethanol. The sol was obtained by vigorously stirring precursor solution at 50°C for 2h, then the temperature was raised to 75°C for the...

  • XPS studies of PDA-modified TiO2 nanotubes

    Dane Badawcze
    open access

    This dataset contains the XPS results (survey and high-resolution spectra) of the samples from TiO2 nanotubes modified with polydopamine. The studies were presented as a part of the research on "Band Gap Engineering toward Semimetallic Character of Quinone-Rich Polydopamine" (DOI: 10.1021/acs.jpcc.2c08804).

  • XPS measurements of the iron elements covered by chromium

    Dane Badawcze
    open access

    Anticorrosive coatings are an important issue in modern materials engineering. One of the most commonly used, for that coating materials, is chrome. Three metal elements were measured, named as Turcja, WB Tech and Nomet. Names were given according to producer of elements. XPS measurements of the Cr 2p region give an ansver concering on surface chemical...

  • XPS measurements of the Fe-Bi based glass

    Dane Badawcze
    open access

    Fe-Si-O and Fe-Si-Pb-O glass was measured by XPS method. The influence of Pb dopand on the glass structure, including the valence of iron, was investigated. The influence of the annealing temperature on the behavior of iron in glass was also investigated. Studies have confirmed the mixed valence of iron in glasses and a high proportion of metallic Fe.

  • Formation of gold nanostructures detected by XPS method

    Dane Badawcze
    open access

    Gold nanostructers were manufactured by thermal dewetting of thin film. Film with thickness of 2.8 nm was deposited by magnetron sputtering method. As a result of annealing at 550 deg, nanostructures appear. Bulk gold, as-deposited gold film and metallic nanostructures were measured by XPS method. 

  • Dewetting of silver films detected by XPS method

    Dane Badawcze
    open access

    Dewetting of silver thin films was detected by XPS method. Thin metallic films were deposited by magnetron sputtering method. Formation of nanostructures , as a result of thermal annealing, was confirmed by SEM microscope. For comparision three samples were measured. Bulg gold, as-deposited silver film with thickness of 3 nm and nanostructures.

  • XPS measurement of the Fe-Ti based materials

    Dane Badawcze
    open access

    The mono‐ and bimetal‐modified (Pd, Cu) titanium(IV) oxide and iron oxide (III) photocatalysts were prepared by chemical reduction method and characterized using XPS method. The composition of elements incorporated in the surface layer of mono- and bimetallic photocatalysts was determined by XPS analysis, as well as the valence state of elements. Measurements...

  • SEM images of symmetrical cell interface with SrTi1-xFexO3-d electrodes and CGO-20 substrate sintered at 800 °C

    Dane Badawcze
    open access - seria: Effect of sintering temperature on electrochemical performance of porous SrTi1-xFexO3-δ oxygen electrodes

    This dataset contains  images of polished cross section of symmetrical cell interface with SrTi1-xFexO3-d  (x=0.35; 0.50; 0..70) electrodes and CGO-20 substrate sintered at 800 °C. Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope (SEM) with an accelerating voltage of 12 kV in a high vacuum...

  • The XPS spectra of Ce0.8Ni0.2O2 prepared using microemulsion method

    Dane Badawcze
    open access - seria: DIR-SOFC

    The dataset includes XPS spectra of Ce0.8Ni0.2O2-s sintered under air atmosphere. Samples were produced using aqueous soft chemistry methods (microemulsion). The XPS spectra were collected for all species. 

  • The XPS spectra of Ce0.8Cu0.2O2 prepared using microemulsion method

    Dane Badawcze
    open access - seria: DIR-SOFC

    The dataset includes XPS spectra of Ce0.8Cu0.2O2-s sintered under air atmosphere. Samples were produced using aqueous soft chemistry methods (microemulsion). The XPS spectra were collected for all species. 

  • Electrochemical data for carbonized metal-organic framworks with cobalt

    Dane Badawcze
    open access

    The data includes the Metal-Organic Frameworks (MOF) measurements, where cobalt was added. The research focuses on the impact of aluminium on Oxygen Evolution Reaction (OER). The measurements were conducted on [EC Lab]. The techniques included are Linear Sweep Voltammetry (LSV), Tafel slope, Chronopotentiometry (CP) and Electrochemical Impedance Spectroscopy...

  • XPS measurements of the Fe-Pb-Si based glass

    Dane Badawcze
    open access

    Glass samples with nominal compositions of xFe2O3-(50-x)PbO–50SiO2, where x = 12.5, 15, 17.5 (mol%) were prepared. Analytical grade substrates were used: Fe2O3, SiO2, and PbO. The appropriate amounts of reagents were mixed in an agate mortar. The powders obtained were melted in porcelain un-enamelled crucibles in an electric furnace at a temperature...

  • API 5L X65 steel - CMOD-force record in -10°C, along rolling direction

    Dane Badawcze
    open access - seria: API 5L X65 steel

    Steel designated as API 5L X65 is often used for oil and gas transportation pipelines. It is caused due to its high ductility, weldability and good corrosion resistance. API 5L X65 is a low alloy steel with carbon content less than 0.3% (depends on delivery condition). Once installed, a pipeline remains in place for many years. Throughout its life,...

  • API 5L X65 steel - CMOD-force record in -10°C, across rolling direction

    Dane Badawcze
    open access - seria: API 5L X65 steel

    Steel designated as API 5L X65 is often used for oil and gas transportation pipelines. It is caused due to its high ductility, weldability and good corrosion resistance. API 5L X65 is a low alloy steel with carbon content less than 0.3% (depends on delivery condition). Once installed, a pipeline remains in place for many years. Throughout its life,...

  • XRD for MoS2-Carbon Based Materials

    Dane Badawcze
    open access

    The presented data showcases the results of XRD analysis conducted on molybdenum sulfide modified with carbon. The MoS2-carbon base materials were prepared via a facile hydrothermal method. Structural characterization confirmed the successful incorporation of carbon into the MoS2 support. XRD was recorded using an X-ray diffractometer (Philips X”Pert...

  • XRD patterns of ammonium vanadate nanocrystals

    Dane Badawcze
    open access - seria: Ammonium vanadate

    The DataSet contains the XRD patterns of ammonium vanadate nanobelts obtained by the hydrothermal method with different conditions. The results show that the structure and phase compositions of samples dependent on reaction conditions.