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Determination of tributyltin (TBT) in marine sediment using pressurised liquid extraction–gas chromatography–isotope dilution mass spectrometry (PLE–GC–IDMS) with a hexane–tropolone mixture
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Preparation and evaluation of 1,3-alternate 25,27-dibenzyloxy-26,28-bis-[3-propyloxy]-calix[4]arene - bonded silica stationary phase for high performance liquid chromatography
PublikacjaOtrzymano nową fazę stacjonarną na bazie dibenzyloksy pochodnej kaliks[4]arenu w konformacji 1,3-naprzemianległej, chemicznie związaną z żelem krzemionkowym. Przeprowadzano badania selektywności i sprawności tej fazy w rozdzielaniu izomerów konstytucyjnych benzenu i pochodnych fenoli. Zaprezentowano wyniki badania wpływu pH fazy ruchomej oraz stężenia metanolu na zdolność rozdzielczą nowej fazy stacjonarnej.
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Determination of tributylotin (TBT) in marine sediment using pressurised liquid extraction-gas chromatography-isotope dilution mass spectrometry (PLE-GC-IDMS) with a hexane-tropolone mixture
PublikacjaOpracowano metodę oznaczania zawartości tributylocyny w próbkach osadu morskiego. Na etapie izolacji zastosowano technikę przyspieszonej ekstrakcji za pomocą roztworu tropolonu w heksanie.Na etapie oznaczeń końcowych wykorzystano technikę chromatografii gazowej, stosując metodę spektrometrii mas rozcieńczenia izotopowego. Wyznaczono parametry walidacyjne opracowanej metody: granicę wykrywalności, precyzję, poprawność i niepewność.
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Productivity Enhancement by Prediction of Liquid Steel Breakout during Continuous Casting Process in Manufacturing of Steel Slabs in Steel Plant Using Artificial Neural Network with Backpropagation Algorithms
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Ionic liquid-assisted sol-gel synthesis of Fe2O3-TiO2 for enhanced photocatalytic degradation of bisphenol a under UV illumination: Modeling and optimization using response surface methodology
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Application of multivariate mathematical-statistical methods to compare reversed-phase thin-layer and liquid chromatographic behaviour of tetrazolium salts in Quantitative Structure-Retention Relationships (QSRR) studies
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Utilization of ionic liquids for the enrichment of biogas
PublikacjaThis article discusses the dependence of biogas composition on organic feed material. High amounts of CO2 decrease the calorific value of biogas. Several technologies are reviewed which can be used to increase the calorific value. Special emphasis is laid on ionic liquids as a new absorbing material. ILs have a number of advantages due to their unique properties such as: low melting point, high thermal conductivity, no flammability,...
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Potentiometric Solid-Contact Ion-Selective Electrode for Determination of Thiocyanate in Human Saliva
PublikacjaA new solid-contact potentiometric ion-selective electrode for the determination of SCN− (SCN-ISE) has been described. Synthesized phosphonium derivative of calix[4]arene was used as a charged ionophore. The research included selection of the ion-selective membrane composition, determination of the ISEs metrological parameters and SCN-ISE application for thiocyanate determination in human saliva. Preparation of the ISEs included...
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Ongoing Progress on Pervaporation Membranes for Ethanol Separation
PublikacjaEthanol, a versatile chemical extensively employed in several fields, including fuel production, food and beverage, pharmaceutical and healthcare industries, and chemical manufacturing, continues to witness expanding applications. Consequently, there is an ongoing need for cost-effective and environmentally friendly purification technologies for this organic compound in both diluted (ethanol-water–) and concentrated solutions (water-ethanol–)....
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Numerical modelling of POC dynamics in the southern Baltic under possible future conditions determined by nutrients, light and temperature**The study was financially supported by the Polish Ministry of Science and Higher Education (grants: NN305 111636 and NN306 404338) and Baltic-C – the BONUS funded project.
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The effect of a miniature argon flow rate on the spectral characteristics of a direct current atmospheric pressure glow micro-discharge between an argon microjet and a small sized flowing liquid cathode
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Coupling of cold vapor generation with an atmospheric pressure glow microdischarge sustained between a miniature flow helium jet and a flowing liquid cathode for the determination of mercury by optical emission spectrometry
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Critical evaluation of recent achievements in low power glow discharge generated at atmospheric pressure between a flowing liquid cathode and a metallic anode for element analysis by optical emission spectrometry
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The improvement of the analytical performance of direct current atmospheric pressure glow discharge generated in contact with the small-sized liquid cathode after the addition of non-ionic surfactants to electrolyte solutions
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Application of gas flow headspace liquid phase micro extraction coupled with gas chromatography-mass spectrometry for determination of 4-methylimidazole in food samples employing experimental design optimization
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Method for introducing liquid modifiers into melt-blown nonwovens during their production Metoda wprowadzania modyfikatorów w postaci roztworów do włóknin pneumotermicznych podczas procesu ich wytwarzania
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Refractive index measurement in the range of 1.3 – 1.5 for 1550 nm wavelength (2nd serie)
Dane BadawczeThe low-coherence refractive index measurements of certified liquid samples provided by Cargille Labs were performed. The measurement system consisted of a broadband light source (central wavelength of 1550 nm), an optical spectrum analyzer, a 2x1 fiber-optic coupler (50:50 power split), and single-mode telecommunication optical fibers. A micromechanical...
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Refractive index measurement in the range of 1.3 – 1.5 for 1550 nm wavelength (1st serie)
Dane BadawczeThe low-coherence refractive index measurements of certified liquid samples provided by Cargille Labs were performed. The measurement system consisted of a broadband light source (central wavelength of 1550 nm), an optical spectrum analyzer, a 2x1 fiber-optic coupler (50:50 power split), and single-mode telecommunication optical fibers. A micromechanical...
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Bridge Structures
Kursy OnlineProject of simply supported grid bridge made of concrete. 2nd Semester Master Course, Civil Engineering
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Rain Gardens GC_MS analysis dataset
Dane BadawczeThis dataset contains the results of samples analysis (no-target analysis: scan mode) using gas chromatography coupled with mass spectrometry GC–MS (GC-2030 NEXIS MS, Shimadzu, Japan or Thermo Scientific, Waltham, USA).
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Fluid Mechanics and Hydraulics EE Msc sem. I r.a. 22/23
Kursy OnlineBasic definitions. Physical properties of liquids. Forces acting on fluids. Hydrostatics - basic equations. Pressure on a flat and curved wall. Buoyancy. Archimedes' law. Balance of submerged bodies. The balance of floating bodies. Hydrodynamics. Hydrodynamic quantities. Continuity equation for the liquid stream. Bernoulli equation. Basic laws of hydrodynamics. Equation of mass behavior, preservation of the amount of motion, Bernoulli's...
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Fluid Mechanics and Hydraulics EE Msc sem. I r.a. 23/24
Kursy OnlineBasic definitions. Physical properties of liquids. Forces acting on fluids. Hydrostatics - basic equations. Pressure on a flat and curved wall. Buoyancy. Archimedes' law. Balance of submerged bodies. The balance of floating bodies. Hydrodynamics. Hydrodynamic quantities. Continuity equation for the liquid stream. Bernoulli equation. Basic laws of hydrodynamics. Equation of mass behavior, preservation of the amount of motion, Bernoulli's...
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Katarzyna Merkel dr hab.
OsobyOver the past 15 years, my work has mainly been related to the study of liquid crystal compounds with a diverse structure (discotic, dendrimeric, banana, bimedogenic, uniaxial and biaxial nematics and smectics) as well as polymeric materials (biopolymers, nano-composites) and biological materials. My work concerned mainly the issues of organization, observation of orientation effects, studying the dynamics of molecular processes...
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Agata Kot-Wasik prof. dr hab. inż.
OsobyAgata Kot-Wasik, urodzona w 1964 r. w Siedlcach (woj. mazowieckie), ukończyła studia magisterskie w 1988 r. na Wydziale Chemicznym Politechniki Gdańskiej, w specjalności Analityka Techniczna i Przemysłowa. W latach 1988–1992 była zatrudniona w Katedrze Chemii Organicznej na macierzystym wydziale na stanowisku naukowo-technicznym. W 1990 r. ukończyła na PG studia podyplomowe „Techniki Instrumentalne w Analizie Śladów i Ochronie...
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Investigation of poly(3,4-ethylenedioxythiophene) deposition method influence on properties of ion-selective electrodes based on bis(benzo-15-crown-5) derivatives
PublikacjaGlassy carbon electrodes modified by conductive polymers and membrane with derivatives of bis(benzo-15-crown-5) were tested as solid contact ion selective electrodes for K+ ions concentration determination. PEDOT with PSS, Cl- and ClO4- counter ions was electrochemically deposited onto glassy carbon substrates using four different electrochemical approaches (potentiostatic, galvanostatic, potentiodynamic and potentiostatic pulses)....
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Determination of the content of saccharides and ethanol in samples of fermented beverages
Dane BadawczeThe data set presents the results of measurements of the content of mono- and disaccharides: glucose, maltose, fructose and ethanol in samples of beverages fermented by high performance liquid chromatography (HPLC-RID).
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Equations of tribological parameters for liquid flow in boundary layer on the tissue surface in bioreactor = Wyznaczanie parametrów tribologicznych dla przepływu cieczy w warstwie granicznej na powierzchni tkanki w bioreaktorze
PublikacjaW niniejszej pracy przedstawiony został problem tribologiczny wynikający z przepływu nieustalonego odżywczej cieczy lepkiej w cienkiej warstwie przyściennej w bezpośrednim kontakcie z zewnętrzną powierzchnią warstwy wierzchniej wzrastających komórek (chondrocytów) w trakcie procesu ich hodowli w bioreaktorze. Efektem rozważań będą wartości sił tarcia powstające na powierzchni wzrastającej tkanki. Najnowsze badania wykazały lepszą...
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Effect of the working liquid compressibility on the picture of volumetric and mechanical losses in a high pressure displacement pump used in a hydrostatic drive. Part I Energy losses in a drive system, volumetric losses in a pump
PublikacjaŚciśliwość cieczy roboczej może znacząco zmienić wartości i proporcje współczynników strat objętościowych i mechanicznych w pompie wyporowej zastosowanej w układzie napędu hydrostatycznego. Wpływ ten jest szczególnie widoczny w trakcie pracy pod wysokim ciśnieniem a także wówczas, gdy występuje zapowietrzenie cieczy roboczej. W części I przedstawiono wykres zaproponowany przez autora, wzrostu mocy w układzie napędu hydrostatycznego...
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Effect of the working liquid compressibility on the picture of volumetric and mechanical losses in a high pressure displacement pump used in a hydrostatic drive. Part I Energy losses in a drive system, volumetric losses in a pump
PublikacjaŚciśliwość cieczy roboczej może znacząco zmienić wartości i proporcje współczynników strat objętościowych i mechanicznych w pompie wyporowej zastosowanej w układzie napędu hydrostatycznego. Wpływ ten jest szczególnie widoczny w trakcie pracy pod wysokim ciśnieniem a także wówczas, gdy występuje zapowietrzenie cieczy roboczej. W części I przedstawiono wykres zaproponowany przez autora, wzrostu mocy w układzie napędu hydrostatycznego...
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Pyocyanin extraction - the comparison of typical organic solvents and ionic liquids
Dane BadawczePyocyanin is a pigment produced by Pseudomonas aeruginosa that recently gained importance as a valuable chemical. Most often, the method for its extraction is based on the use of chloroform, a recognized hazardous substance. Therefore, an efficient and more environment-friendly method is vital for further use. In this work, we compared different organic...
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Functionalization of Parylene During Its Chemical Vapor Deposition
PublikacjaTwo possible mechanisms for the reaction of four halogenated (metha)acrylate-based molecules with Parylene [poly (paraxylylene)] during its chemical vapor deposition were proposed. The chemical reactivity of acrylate double bond with the paraxylylene biradical was calculated for all four (metha)acrylate-based molecules. These calculations allowed the evaluation of the energetically favorable mechanism and indeed a direct correlation...
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Accurate, Direct, and High-Throughput Analyses of a Broad Spectrum of Endogenously Generated DNA Base Modifications with Isotope-Dilution Two-Dimensional Ultraperformance Liquid Chromatography with Tandem Mass Spectrometry: Possible Clinical Implication
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High-performance liquid chromatography of di- and trisubstituted aromatic positional isomers on 1,3-alternate 25,27-dipropoxy-26,28-bis-[3-propyloxy]-calix[4]arene-bonded silica gel stationary phase.
PublikacjaOtrzymano nową fazę stacjonarną na bazie dipropyloksy pochodnej kaliks[4]arenu w konformacji 1,3-naprzemianległej chemicznie związaną z żelem krzemionkowym. Przeprowadzono badanie selektywności i sprawności tej fazy w rozdzielaniu izomerów konstytucyjnych benzenu. Zaprezentowano wyniki badania wpływu warunków chromatograficznych (pH fazy ruchomej, temperatura, stężenie modyfikatora organicznego) na zdolność rodzielczą tej nowej...
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Ni-WC/Al2O3 and Ni-WC/MgWO4/MgAl2O4 catalysts for resource recovery via pyrolysis combined with the dry reforming of plastics (PCDR)
PublikacjaPlastic waste (PW) is currently one of an environmental threat. Despite the increasing share of recycled plastics, their disposal remains high. Therefore, there is a high demand for new PW management systems. Among them, pyrolysis combined with dry reforming (PCDR) is an advantageous solution because it allows for resource recovery in the form of gas and liquid fuels, with simultaneous utilization of CO2. To date, catalysts based...
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Lower Rim Substituted p-tert-Butyl Calix[4]arenes(V). Synthesis of New 5,11,17,22-tetrakis-p-tert-Butyl-25-27-bis(dialkoxyphosphorylmethoxy)calix[4] arenes and Cation Complexation Studies in Ion Selective Membrane Electrodes.
PublikacjaZaprezentowano syntezę i właściwości trzech nowych związków (2-4), bis podstawionych na dolnym obrzeżu grupami z resztą fosforylową. Związki te były badane jako jonofory w membranowych elektrodach jonoselektywnych (ISE) wykazując selektywność na kationy Rb+,K+ oraz duży i płaski kation guanidyniowyG+). Badano korelację pomiędzy stereo-strukturą związków a ich selektywnością w ISE. Stałe trwałości kompleksów z kationami metali...
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2,6-Bis((benzoyl-R)amino)pyridine (R = H, 4-Me, and 4-NMe2) Derivatives for the Removal of Cu(II), Ni(II), Co(II), and Zn(II) Ions from Aqueous Solutions in Classic Solvent Extraction and a Membrane Extraction
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Diagnosis of Damage in a Steel Tank Model by Shaking Table Harmonic Tests
PublikacjaThe aim of the present paper is to show the results of the shaking table experimental study concerning the diagnosis of damage in a model of cylindrical steel tank with self-supported roof which is filled with liquid. During the tests, the base of the structure was excited under the harmonic loading with variable frequency. The tests were repeated for different stages of damage, which was introduced in the model by easing the bolts...
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A modern solid waste management strategy – the generation of new by-products
PublikacjaTo benefit the environment and society, EU legislation has introduced a ‘zero waste’ strategy, in which waste material should be converted to resources. Such legislation is supported by the solid waste hierarchy concept, which is a set of priorities in waste management. Under this concept, municipal solid waste plants (MSWPs) should be equipped with sorting and recycling facilities, composting/incineration units and landfill prisms...
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Maciej Przybyłek Dr hab.
OsobyI. EDUCATION AND ACADEMIC DEGREES 1. A graduate of the Faculty of Technology and Chemical Engineering at the University of Technology and Life Science in Bydgoszcz (2010), field of study: Chemical Technology, field of specialization: Technology of Chemical Process. 2. Doctorate in Pharmacy at the Nicolaus Copernicus University (2016), PhD Thesis: "Studies on the orientation effect of crystallites and its application to cocrystal...
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Biological processes modelling for MBR systems: A review of the state-of-the-art focusing on SMP and EPS
PublikacjaA mathematical correlation between biomass kinetic and membrane fouling can improve the understanding and spread of Membrane Bioreactor (MBR) technology, especially in solving the membrane fouling issues. On this behalf, this paper, produced by the International Water Association (IWA) Task Group on Membrane modelling and control, reviews the current state-of-the-art regarding the modelling of kinetic processes of biomass, focusing on...
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Dariusz Mikielewicz prof. dr hab. inż.
OsobyDariusz Mikielewicz – urodził się 6 lutego 1967 roku w Gdańsku, w 1985r. zdał pomyślnie egzaminy wstępne na Wydział Budowy Maszyn Politechniki Gdańskiej, który ukończył z wynikiem bardzo dobrym w 1990 roku na specjalności Maszyny i Urządzenia Energetyczne. Zainteresowania pracą naukową skłoniły go do podjęcia badań na University of Manchester na wydziale mechanicznym i energetyki jądrowej (Mechanical and Nuclear Engineering Department)...
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In-situ generation of Ag, Cd, Hg, In, Pb, Tl and Zn volatile species by flowing liquid anode atmospheric pressure glow discharge operated in gaseous jet mode – Evaluation of excitation processes and analytical performance
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Bisphenols and their derivatives in baby diaper samples.
PublikacjaMany common products contain and leach hazardous chemicals, including endocrine-disrupting chemicals such as bisphenols that are harmful to human health. For toddlers, this dangerousness is higher because of their not fully developed detoxification system. Due to this, bisphenols content in products such as baby diapers, should be monitored. Baby diapers not only remain in close contact with the skin, but are also used from the...
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Variable Order Differential Models of Bone Remodelling * *This work was supported by FCT, through IDMEC, under LAETA, projects UID/EMS/50022/2013, BoneSys, joint Polish-Portuguese project Modelling and controlling cancer evolution using fractional calculus, PERSEIDS (PTDC/EMS-SIS/0642/2014) and IF/00653/2012
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Photoluminescence spectra of TiO2
Dane BadawczeThese data contain photoluminescence spectra of TiO2 measured at the temperature of liquid nitrogen. There is a comparison of the photoluminescence spectra of TiO2 heat treated at 400-600oC in the ambient (Ar) and reduced (H2) atmospheres. These emission spectra were recorded after TiO2 excitation with a wavelength of 290 nm
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Role of cholesterol in substrate recognition by -secretase
Publikacja-Secretase is an enzyme known to cleave multiple substrates within their transmembrane domains, with the amyloid precursor protein of Alzheimer’s Disease among the most prominent examples. The activity of -secretase strictly depends on the membrane cholesterol content, yet the mechanistic role of cholesterol in the substrate binding and cleavage remains unclear. In this work, we used all-atom molecular dynamics simulations to examine...
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Solventless and solvent-minimized sample preparation techniques for determining currently used pesticides in water samples: A review
PublikacjaThe intensification of agriculture means that increasing amounts of toxic organic and inorganic compounds are entering the environment. The pesticides generally applied nowadays are regarded as some of the most dangerous contaminants of the environment. Their presence in the environment, especially in water, is hazardous because they cause human beings to become more susceptible to disease. For these reasons, it is essential to...
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Separation of bacteria in UF process
Dane BadawczeLarge quantities of water are used in car washing, so it is necessary to recycle the water, which is made possible by membrane filtration. FP100 (100 kDa) membranes have been used to treat car wash wastewater by ultrafiltration (UF). With time of operation, the properties of the membranes change. The membranes need to be cleaned periodically to prevent...
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Kinetics of hexane and cyclohexane biodegradation using Candida subhashii in mineral salt medium in the presence of DES solution
Dane BadawczeDataset presents results of investigations on kinetics of biodegradation of hexane and cyclohexane in Candida subhashii.
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Leszek Jarzębowicz dr hab. inż.
OsobyLeszek Jarzębowicz ukończył studia jednolite magisterskie na Wydziale Elektrotechniki i Automatyki Politechniki Gdańskiej w 2005 r. Na tym samym wydziale uzyskał stopień doktora nauk technicznych (2010 r.) oraz doktora habilitowanego nauk inżynieryjno-technicznych (2019 r.). Jego zainteresowania naukowe koncentrują się na: sterowaniu i modelowaniu elektrycznych układów napędowych, diagnostyce pojazdów szynowych, efektywności energetycznej...