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Wyniki wyszukiwania dla: ANALYTICAL TECHNIQUE
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Analysis of pesticide residue in fruits and vegetables using analytical analytical protocol based on application of QuEChERS technique and GC-ECD system
PublikacjaQuEChERS sample preparation method was used for the determination of 10 pesticides and their metabolites in fruits (apple, grape) and vegetables (tomato, paprika), coupled to gas chromatography with electron capture detector (GC-ECD). The experimental parameters including amount of the sample, types of solvents, extraction time and types of sorbent at the purification stage were optimized. The GC-ECD method was validated in terms...
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Novel Analytical Techniques, GT
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NOVEL ANALYTICAL TECHNIQUES seminars
Kursy OnlineStudents will gain theexperience how to presents the knowledge in the range of analysis and monitoring of pullutants.
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Novel Analytical Techniques, GT 2022
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New Technique of preparation of standard gas mixtures needed for validation of analytical procedures used in environmental studies
PublikacjaStandard gas mixtures are indispensable reference materials for ensuring the reliability of analytical work. Paper presents one novel approach in the field of production of gaseous reference materials based on the application of thermal decomposition process of proper surface compound for obtaining the desired gaseous analyte. The main fields of application of reference materials are presented. The field of application of thermal...
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Mass Spectrometry-Based Direct Analytical Techniques
PublikacjaDirect analysis of samples is considered as one of the most environmentally sustainable solutions in analytical chemistry. In the ideal case, such solutions do not require sample preparation and analytes separation steps, therefore do not consumpt harmful substances (or consumpt only minimum amounts of them) and do not generate hazardous waste. Technical solutions for direct analysis also offer miniaturized and field-portable analyzers...
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Analysis of pesticide residue in tomato samples using analytical protocol based on application of QuEChERS technique and GC-ECD system
PublikacjaQuEChERS sample preparation method was used for the determination of 10 pesticides and their metabolites in tomato samples, coupled to gas chromatography with electron capture detector (GCECD). The experimental parameters including oven temperature program, amount of the sample and purifying agent were optimized. The GC-ECD method was validated in terms of linearity, selectivity and recovery. The limits of detection (LODs) of the...
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Analytical techniques used in monitoring of atmospheric air pollutants
PublikacjaW artykule opisano najczęściej spotykane zanieczyszczenia powietrza atmosferycznego, ich interakcje i wpływ na środowisko. Przedstawiono klasyfikację technik i metodyk stosowanych w badaniach zanieczyszczeń powietrza. Przeprowadzono przegląd technik pobierania i dozowania próbek gazowych. Zaprezentowano także przykłady typowych systemów służących do analizy zanieczyszczeń powietrza.
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Analytical Techniques Used in Monitoring of Atmospheric Air Pollutants
PublikacjaThe air pollution monitoring is one of the most pressing environmental problems today. The paper describes common air pollutants, their interaction and impact on the environment, and classifies the techniques and methods applied in air studies. Furthermore, the review characterizes the selected collection and sampling techniques used for gas sample analysis. Finally, the schematic diagrams of typical designs of systems applied...
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New and Fast Analytical Techniques in Food Quality Analysis
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Volume optimization of high-speed surface-mounted permanent magnet synchronous motor based on sequential quadratic programming technique and analytical solution
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Analytical techniques used in monitoring of atmospheric air andstack gases
PublikacjaPrzedstawiono klasyfikację metod i technik analitycznych wykorzystywanych w badaniach powietrza atmosferycznego i gazów odlotowych. Przedstawiono również typowe urządzenia wykorzystywane na etapie pobierania próbek.
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Application of analytical procedure based on accelerated solvent extraction and ion chromatography technique for determination of thiocyanate and other inorganic ions in human placenta samples
PublikacjaExposure of a pregnant woman during pregnancy is a special case of exposure to toxic substances. Samples of placenta collected for the studies had been prepared with the technique of accelerated solvent extraction and later analyzed for the presence of thiocyanate ion and other inorganic ions, with the use of the technique of ion chromatography. The concentration of thiocyanate ion in placenta samples collected from active smokers...
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NEW AND FAST ANALYTICAL TECHNIQUES IN FOOD QUALITY ANALYSIS 2024
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Analytical techniques in studies of the environmental fate of pharmaceuticals and personal-care products
PublikacjaW pracy przedstawiono dane literaturowe odnośnie źródeł emisji, dróg transportu, przemian i metabolizmu, pomiomu stężeń ksenobiotyków z grupy farmaceutyków i środków higieny osobistej w próbkach pobranych z różnych elementów środowiska (woda, gleba, osady denne) oraz próbek bioty. Szczególną uwagę zwrócono na techniki analityczne wykorzystywane w badaniach losu środowiskowego w/w zanieczyszczeń.
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Analytical Techniques for Determining Pharmaceutical Residues in Drinking Water – State of Art and Future Prospects
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Trends in edible vegetable oils analysis. Part B. Application of different analytical techniques
PublikacjaW publikacji przeglądowej przedstawiono najnowsze osiągnięcia w instrumentalnej analizie olejów roślinnych. Dotychczas w ocenie stabilności oksydatywnej stosuje się różne metody analityczne, jednak nie są one wystarczające. Dlatego ciągle istnieje potrzeba rozwoju nowych łączonych technik, które umożliwią lepszą kontrolę jakości olejów. Publikacja przedstawia zarówno techniki przygotowywania próbek do analiz jak i metody instrumentalne...
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Analytical techniques for trace organic compounds-III: Mass spectrometry in trace organic analysis
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The use of selected analytical techniques for pollutants determination in the environmental samples collected from the Arctic regions
PublikacjaThe paper concern importance of the use of analytical techniques for pollutants determination in the Arctic based on the example of total organic carbon, phenolsandformaldehyde determinationandmeasurementofpHand electrical conductivity parameters in surfacewater samples collected fromthe Revelva catchment.
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Journal of Analytical Techniques
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Analytical techniques for trace organic compounds - IV: Tandem mass spectrometry for organic trace analysis (Technical Report)
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Environmental problems and health risks with disposable baby diapers: Monitoring of toxic compounds by application of analytical techniques and need of education
PublikacjaDue to the widespread use of disposable diapers in healthy babies as well as children prone to allergiesand premature babies with reduced immunity, disposable diapers should only be made of non-toxic andnatural ingredients. Unfortunately, disposable diaper manufacturers are reluctant to present their exactchemical composition, claiming that their trade secrets apply. However, several reports show thatdisposable diapers of well-known...
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Multi-Analytical Techniques for the Study of Burial Clothes of Polish King Sigismund III Vasa (1566–1633) and His Wife Constance Habsburg (1588–1631)
PublikacjaThe subjects of this research are the burial clothes of Polish King Sigismund III Vasa and his wife Constance, which were woven and embroidered with silk and metal threads. Fragments of the textiles underwent spectroscopic, spectrometric, and thermogravimetric analyses. The hydrofluoric acid extraction method was improved to isolate various classes of dyes from the textile samples that had direct contact with human remains. High-performance...
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Analytical procedures for determination of cocaine and its metabolites in biological samples
PublikacjaThe dangerous effects and increased usage of illicit drugs have inspired the development of analytical methodologies. We based our review of analytical procedures for determination of cocaine (COC) and its metabolites on literature from the past two decades. Our main aim was to compare the capabilities of different analytical techniques. The diversity of matrices from which COC is determined (e.g., blood, hair, saliva, plasma,...
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Green Analytical Chemistry Approaches in Sample Preparation
PublikacjaThis chapter presents environmentally friendly solutions for sample preparation. Attention is focused on extraction techniques and the minimization of organic solvent consumption, as the large quantitiesused in analytical laboratories are a pressing environmental problem. Solventless sample preparation techniques, alternative solvents, mediated extractions are discussed. The principle of each technique isbriefly described, together...
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Multicriteria Decision Analysis and Grouping of Analytical Procedures for Phthalates Determination in Disposable Baby Diapers
PublikacjaThis study presents the application of one of the tools from the multicriteria decision analysis set (MCDA), the Technique for Order Preference by Similarity to Ideal Solution (TOPSIS). Selected green analytical chemistry metrics were used to rank analytical procedures for the phthalate determination in disposable baby diapers. Nine analytical procedures were assessed in order to find one that has the lowest environmental impact...
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Greener organic solvents in analytical chemistry
PublikacjaThe paper presents the most recent advances in analytical applications of greener organic solvents. Substitution of problematic solvents with more benign organic ones is much easier than shifting to technique applying alternative solvents, such as ionic liquids or supercritical fluids. In the area of liquid chromatography greener mobile phases, much attention is given to application ethanol or acetone instead of acetonitrile. Solvent-based...
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Coacervative extraction as a green technique for sample preparation for the analysis of organic compounds
PublikacjaOne of the present trends in analytical chemistry is miniaturization, which is one of the methods of green analytical chemistry application. A particular emphasis is placed on the elimination of the use of large amounts of organic solvents which are toxic and harmful to the environment, maintaining high efficiency of the extraction process, high recovery values and low values of quantification (LOQ) and detection (LOD) limits....
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Application of multivariate statistics in assessment of green analytical chemistry parameters of analytical methodologies
PublikacjaThe study offers a multivariate statistical analysis of a dataset, including the major metrological, “greenness” and methodological parameters of 43 analytical methodologies applied for aldrin determination (a frequently analyzed organic compound) in water samples. The variables (parameters) chosen were as follows: metrological (LOD, recovery, RSD), describing the “greenness” (amount of the solvent used, amount of waste generated)...
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Application of TOPSIS for Selection and Assessment of Analytical Procedures for Ibuprofen Determination in Wastewater
PublikacjaThis paper describes the possible implementation of the Technique for Order Preference by Similarity to Ideal Solution (TOPSIS) as green analytical chemistry metrics tools. TOPSIS is one of the multi-criteria decision analysis (MCDA) tools that is applied in the selection of the best alternative from many possible. In this case we have applied it to assess the nineteen analytical procedures for ibuprofen determination in wastewater...
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Green Analytical Chemistry: Summary of Existing Knowledge and Future Trends
PublikacjaAnalysis of recent publications in green analytical chemistry shows the current trends and future needs in this area. The main issues are related with search for cheaper, more efficient, more accurate, greener and miniaturized alternatives. Miniaturization is perhaps, the most notable current trend in analytical chemistry. Rapid developments and improvements in instrumentation have led to impressive range of benchtop technology...
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Introduction to MIP synthesis, characteristics and analytical application
PublikacjaOne of the trends in analytical chemistry is associated with designing and developing new types of sample preparation techniques, which might significantly increase the efficiency and selectivity of the analytes isolation or/and preconcentration process. One of the most widely employed solutions are selective sorption materials, defined as molecularly imprinted polymers (MIPs), as well as the sorbents with the molecular fingerprint....
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Hasse diagram as a green analytical metrics tool: ranking of methods for benzo[a]pyrene determination in sediments
PublikacjaThis study presents an application of the Hasse diagram technique (HDT) as the assessment tool to select the most appropriate analytical procedures according to their greenness or the best analytical performance. The dataset consists of analytical procedures for benzo[a]pyrene determination in sediment samples, which were described by 11 variables concerning their greenness and analytical performance. Two analyses with the HDT...
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Two-dimensional gas chromatography – principles and application in fruits analysis
PublikacjaTwo-dimensional gas chromatography is a rapidly developing analytical technique. One of the major uses of this technique is its use for food analysis. The paper presents the principle of operation and history of this analytical technique. The specification of the two-dimensional gas chromatography technique has been discussed. The principles of separation of ingredients and application of the method, particularly in the analysis...
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Neutral point balancing technique for 3-level neutral point clamped converter with servo system
PublikacjaNeutral point voltage drift compensation technique in 3-level NPC multilevel converter and servo system is described in the paper. Analytical expressions are obtained for power subsystem elements parameters of servo drive system. Simulation of servo system, based on PMSM motor with 3-level NPC converter is considered.
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Novel analytical method for detection of orange juice adulteration based on ultra-fast gas chromatography
PublikacjaThe food authenticity assessment is an increasingly important issue in food quality and safety. The application of an electronic nose based on ultra-fast gas chromatography technique enables rapid analysis of the volatile compounds from food samples. Due to the fact that this technique provides chemical profiling of natural products, it can be a powerful tool for authentication in combination with chemometrics. In this article,...
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Scattering and Propagation Analysis for the Multilayered Structures Based on Field Matching Technique
PublikacjaA semi-analytical method is employed to the analysis of scattering and guiding problems in multilayer dielectric structures. The approach allows to investigate objects with arbitrary convex cross section and is based on the direct field matching technique involving the usage of the field projection at the boundary on a fixed set of orthogonal basis functions. For the scattering problems the scattered field in the far zone is calculated...
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Metals and metal-binding ligands in wine: Analytical challenges in identification.
PublikacjaBackground Due to important role of metals in the vinification process as well as their impact on the human health, their content in this alcoholic beverage has been extensively studied by many researchers. It is already known that speciation of metals determines their toxicity and bioavailability as well as influences their activity. Understanding the chemistry and knowing the structures of metal complexes could have relevant...
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Using the Fingerprinting Method to Customize RTLS Based on the AoA Ranging Technique
PublikacjaReal-time Locating Systems (RTLSs) have the ability to precisely locate the position of things and people in real time. They are needed for security and emergency applications, but also for healthcare and home care appliances. The research aims for developing an analytical method to customize RTLSs, in order to improve localization performance in terms of precision. The proposed method is based on Angle of Arrival (AoA), a ranging...
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Membrane-SPME the best 'green' sample preparation technique for the gas chromatographic determination polar organic pollutants in polar media
PublikacjaOne of the most popular technique for sample preparation, which fulfill requirements of green analytical chemistry, is solid phase microextraction (SPME). Because of the undoubted advantages of SPME technique, solvent-free character of the extraction process and the enormous potential in analytical practice, a series of studies has been undertaken to develop new technical solutions, where improving the sensitivity and the extraction...
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Identification of pollutants at the adjacent areas to the landfill site using two dimensional gas chromatography with mass spectrometry technique
PublikacjaMunicipal landfills are considered one of the main sources of air pollutants. In this article is presented the use of a modern analytical technique: a two dimensional gas chromatography to identify the substances in the atmospheric air near a waste processing plant located in Gdansk. In order to determine the types of substances occurring in different atmospheric conditions, the study was conducted from February to April 2016....
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Quasi-analytical Near-to-Far Field Transformation Based on Field Matching Method for Scattering Problems
PublikacjaA new quasi-analytical near-to-far field transformation based on field matching method (field expansion in a base of Hankel functions) is presented. This approach uses finite element method to obtain near field, then the field is expressed in a base of Hankel functions. The evaluated coefficients allow to calculate the field outside the numerical domain, also in a far distance. The main advantage of the proposed technique is avoiding of...
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Porous material-based sorbent coatings in Solid-phase microextraction technique: Recent trends and future perspectives
PublikacjaThe use of porous materials as sorbents in sample preparation techniques has gained recent scientific attention in the context of developing novel fibers for the Solid-phase microextraction (SPME) technique. SPME requires the appropriate selection of a robust sorbent for successful utilization under variable conditions. A deeper understanding of the nature of newly developed porous SPME coatings and the impact of their structures...
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Application of passive sampling technique in monitoring research on quality of atmospheric air in the area of Tczew, Poland.
PublikacjaThis paper presents the results of atmospheric air quality research in Tczew (adjacent to the Vistula River) on the content of BTEX compounds. Analytical procedure applied during the sampling of the analytes from the air used the passive sampling technique (diffusive passive sampler, Radiello®). For determination of BTEX compounds in atmospheric air, two-stage thermal desorption technique combined with gas chromatography (TD-GC-FID)...
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Solution of the dike-break problem using finite volume method and splitting technique
PublikacjaIn the paper the finite volume method (FVM) is presented for the solution of two-dimensional shallow water equations. These equations are frequently used to simulate the dam-break and dike-break induced flows. The applied numerical algorithm of FVM is based on the wave-propagation algorithm which ensures a stable solution and simultaneously minimizes the numerical errors. The dimensional decomposition according to the coordinate...
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Matrix solid-phase dispersion (MSPD) as simple and useful sample preparation technique for determination of polybrominated diphenyl ethers (PBDEs) in dust
PublikacjaIn the present study a novel analytical procedure for the determination of polybrominated diphenylethers in dust samples was developed.The main aim of the research was the selection of the optimum conditions of the matrix solid-phasedispersion before thefinal determination of polybrominated diphenyl ethers in dust samples. In order toassess the best usefulness of this technique, a favourable ratio of sample amount to the mass ofdispersing...
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Application of hybrid finite-difference mode-matching method to analysis of structures loaded with axially-symmetrical posts
PublikacjaW artykule przedstawiono nową metodę hybrydową do analizy układów falowodowych zawierających dowolne konfiguracje obiektów osiowo-symetrycznych. Metoda oparta jest na połączeniu metody różnic skończonych, metody dopasowania rodzajów oraz iteracyjnej procedury rozpraszania. W pracy przedstawiono badania zbieżności metody. Uzyskane wyniki numeryczne porównano z wynikami odniesienia. Duża zgodność wyników potwierdziła poprawność opracowanego...
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An Analysis of Scattering from Ferrite Post of Arbitrary Convex Cross Section with the Use of Field Matching Method
PublikacjaA problem of electromagnetic wave scattering from ferrite post is presented. The post is assumed to be located in closed areas as waveguide junction, or in open area illuminated by a plane wave. The object is of arbitrary convex cross section and the method of analysis is semi-analytical, based on the direct field matching technique.
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POTENCJALNE MOŻLIWOŚCI APLIKACJ TECHNIKI E-NOS W DIAGNOSTYCE MEDYCZNEJ=APPLICATION POTENTIALITIES OF E-NOSE TECHNIQUE IN MEDICAL DIAGNOSTICS
PublikacjaW pracy przedstawiono i omówiono zasadę działania instrumentu analitycznego - elektronicznego nosa (e-nos) zdolnego rozróżnić i sklasyfikować intensywność zapachu. Urządzenia te służą do automatycznej analizy i rozróżniania próbek zapachowych o złożonym składzie, do rozpoznawania ich charakterystycznych właściwości i najczęściej przeznaczone są do szybkiej analizy jakościowej. Dzięki unikatowym właściwościom technika ta znalazła...
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Application of multicriteria decision analysis in solvent type optimization for chlorophenols determination with a dispersive liquid–liquid microextraction
PublikacjaThis study presents a novel support tool for the optimization and development of analytical methods. The tool is based on multi-criteria decision analysis (MCDA), namely the Technique for Order of Preference by Similarity to the Ideal Solution (TOPSIS), that allows users to rank possible solutions according to their requirements. In this study, we performed rankings of pairs of eight extraction and three dispersive solvents used...