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A magnetic stir bar sorbent of metal organic frameworks, carbon foam decorated zinc oxide and cryogel to enrich and extract parabens and bisphenols from food samples
Abstract
A porous composite magnetic stir bar adsorbent was fabricated for the extraction and enrichment of parabens and bisphenols from selected beverage samples. The adsorbent comprised a metal organic framework, carbon foam decorated zinc oxide and magnetic nanoparticles embedded in polyvinyl alcohol cryogel. The porous composite stir bar adsorbent could adsorb parabens and bisphenols via hydrogen bonding, π-π and hydrophobic interactions. In the best conditions, linearity was good from 5.0 to 200.0 µg/L for methyl paraben, ethyl paraben and bisphenol A and from 10.0 to 200.0 µg/L for bisphenol B and butyl paraben. Limits of detection ranged from 1.5 to 3.0 µg/L. The developed composite stir bar was successfully applied to extract and determine parabens and bisphenols in fruit juice, beer and milk. Recoveries ranged from 89.5 to 99.5 % with RSDs lower than 6 %. The developed sorbent and new methodology were evaluated in terms of its green character with satisfactory results.
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Authors (4)
-
Sirintorn Jullakan
-
Natnaree Rattanakunsong
-
Opas Bunkoed
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Details
- Category:
- Articles
- Type:
- artykuły w czasopismach
- Published in:
-
JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES
no. 1232,
ISSN: 1570-0232 - Language:
- English
- Publication year:
- 2024
- Bibliographic description:
- Jullakan S., Rattanakunsong N., Płotka-Wasylka J., Bunkoed O.: A magnetic stir bar sorbent of metal organic frameworks, carbon foam decorated zinc oxide and cryogel to enrich and extract parabens and bisphenols from food samples// JOURNAL OF CHROMATOGRAPHY B-ANALYTICAL TECHNOLOGIES IN THE BIOMEDICAL AND LIFE SCIENCES -Vol. 1232, (2024), s.123970-
- DOI:
- Digital Object Identifier (open in new tab) 10.1016/j.jchromb.2023.123970
- Sources of funding:
-
- COST_FREE
- Verified by:
- Gdańsk University of Technology
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