Determination of phenylbutazone, sulfamethazine, carbendazim and linuron using a novel pine bark biosorbent for solid-phase extraction (SPE) with high-performance liquid chromatography (HPLC)

Hassen Khazri; Grzegorz Boczkaj; Ibtissem Ghorbel-Abid; Malika Trabelsi-Ayadi

doi:10.1080/10739149.2022.2043357

Determination of phenylbutazone, sulfamethazine, carbendazim and linuron using a novel pine bark biosorbent for solid-phase extraction (SPE) with high-performance liquid chromatography (HPLC)

Abstract

The paper presents a novel pine bark based biosorbent for solid-phase extraction (SPE). The morphology and composition of the pine bark were characterized using Fourier transform infrared spectroscopy (FTIR) and scanning electron microscopy (SEM). The biosorbent was used for the preparation of wastewater for the determination of phenylbutazone, sulfamethazine, carbendazim, and linuron by high performance liquid chromatography with ultraviolet detection (HPLC-UV). The SPE conditions were optimized with respect to elution solvent, sample volume, and extraction pH. The results showed that developed sorbent provides good repeatability. The relative standard deviation (n = 3), was between 0.3 and 2.2%. The limits of detection (LOD) were between 0.11 and 0.4 µg.L−1. The developed method was used for determination of the analytes in effluent from a wastewater treatment plant.

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Authors (4)

Hassen Khazri
- Laboratory of Application Chemistry to the Resources and Natural Substances and the Environment (LACReSNE), Faculty of Science of Bizerte, Zarzouna, Bizerte Tunisia
Grzegorz Boczkaj dr hab. inż.
Ibtissem Ghorbel-Abid
- Laboratory of Application Chemistry to the Resources and Natural Substances and the Environment (LACReSNE), Faculty of Science of Bizerte, Zarzouna, Bizerte Tunisia;c Useful Materials Laboratory (LMU), National Institute for Physical and Chemical Research
Malika Trabelsi-Ayadi
- Laboratory of Application Chemistry to the Resources and Natural Substances and the Environment (LACReSNE), Faculty of Science of Bizerte, Zarzouna, Bizerte Tunisia;c Useful Materials Laboratory (LMU), National Institute for Physical and Chemical Research

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Category:: Articles
Type:: artykuły w czasopismach
Published in:: INSTRUMENTATION SCIENCE & TECHNOLOGY no. 50, pages 507 - 519,
ISSN: 1073-9149
Language:: English
Publication year:: 2022
Bibliographic description:: Khazri H., Boczkaj G., Ghorbel-Abid I., Trabelsi-Ayadi M.: Determination of phenylbutazone, sulfamethazine, carbendazim and linuron using a novel pine bark biosorbent for solid-phase extraction (SPE) with high-performance liquid chromatography (HPLC)// INSTRUMENTATION SCIENCE & TECHNOLOGY -Vol. 50,iss. 5 (2022), s.507-519
DOI:: Digital Object Identifier (open in new tab) 10.1080/10739149.2022.2043357
Verified by:: Gdańsk University of Technology