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Implementation of multicriteria decision analysis in design of experiment for dispersive liquid-liquid microextraction optimization for chlorophenols determination
Abstract
A novel and efficient approach to optimization of extraction step prior the chromatographic determination of nine chlorinated phenols is described. It is based on the combination of design of experiments and multicriteria decision analysis. Such an approach is used to optimize dispersive liquid-liquid microextraction procedure for the determination of 9 chlorophenols in water samples. Three parameters are optimized – sample volume, volume of disperser solvent and extraction solvent. Combination of the technique for order of preference by similarity to ideal solution with central composite design allows to perform multi-analyte procedure optimization. It gives information about the efficiency of the system for every experimental plan point in terms of closeness to ideal solution. The optimal conditions for extraction of chlorophenols are 76 μL of extraction solvent, 0.6 mL of dispersive solvent and 6.7 mL of water sample. The presented approach has the potential to be applied in variety of optimization systems.
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- Category:
- Articles
- Type:
- artykuł w czasopiśmie wyróżnionym w JCR
- Published in:
-
JOURNAL OF CHROMATOGRAPHY A
no. 1553,
pages 25 - 31,
ISSN: 0021-9673 - Language:
- English
- Publication year:
- 2018
- Bibliographic description:
- Bigus P., Namieśnik J., Tobiszewski M.: Implementation of multicriteria decision analysis in design of experiment for dispersive liquid-liquid microextraction optimization for chlorophenols determination// JOURNAL OF CHROMATOGRAPHY A. -Vol. 1553, (2018), s.25-31
- DOI:
- Digital Object Identifier (open in new tab) 10.1016/j.chroma.2018.04.018
- Verified by:
- Gdańsk University of Technology
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