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• Efficient Synthesis of Functionalized Unsymmetrical Dialkyl Trisulfanes

  Publication

  • S. Lach
  • D. Witt

  - SYNLETT - Year 2013

  We have developed a convenient method for the synthesis of functionalized unsymmetrical dialkyl trisulfanes under mild conditions in very good yields. The designed method is based on the reaction of (5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl)-disulfanyl derivatives with alkyl disulfanyl anions generated in situ from S-acetyl disulfanyl derivatives and sodium methoxide. The developed method allows for the preparation of...

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