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Search results for: ambient mass spectrometry
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=4.40, b=0.42) and (C=5.50, b=0.37) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a pressure relief valve arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere,...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=7.30, b=0.49) and (C=6.00, b=0.25) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in parallel. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.30, b=0.38) and (C=5.50, b=0.37) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a pressure relief valve arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere,...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.30, b=0.38) and (C=2.40, b=026.) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a pressure relief valve arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere,...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=4.40, b=0.42) and (C=5.30, b=0.38) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for two pressure relief valves arranged in parallel. Three test configurations were used: (1) being emptied tank -> the first PRV -> ambient atmosphere, (2) being...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.50, b=0.37) and (C=6.00, b=0.25) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV ->...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=4.40, b=0.42) and (C=3.30, b=0.40) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for two pressure relief valves arranged in parallel. Three test configurations were used: (1) being emptied tank -> the first PRV -> ambient atmosphere, (2) being...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=4.40, b=0.42) and (C=5.70, b=0.32) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a pressure relief valve arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere,...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.30, b=0.38) and (C=2.10, b=0.14) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a pressure relief valve arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere,...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.70, b=0.32) and (C=7.30, b=0.49) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a pressure relief valve arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere,...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=2.40, b=0.26) and (C=6.00, b=0.25) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV ->...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=2.80, b=0.25) and (C=6.00, b=0.25) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV ->...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.30, b=0.38) and (C=7.30, b=0.49) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for two pressure relief valves arranged in parallel. Three test configurations were used: (1) being emptied tank -> the first PRV -> ambient atmosphere, (2) being...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.30, b=0.38) and (C=6.20, b=0.38) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for two pressure relief valves arranged in parallel. Three test configurations were used: (1) being emptied tank -> the first PRV -> ambient atmosphere, (2) being...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=2.00, b=0.11) and (C=6.00, b=0.25) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV ->...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=2.10, b=0.14) and (C=6.00, b=0.25) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV ->...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=6.20, b=0.38) and (C=6.00, b=0.25) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in parallel. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.70, b=0.32) and (C=6.00, b=0.25) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV ->...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.30, b=0.38) and (C=6.40, b=0.45) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for two pressure relief valves arranged in parallel. Three test configurations were used: (1) being emptied tank -> the first PRV -> ambient atmosphere, (2) being...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.30, b=0.38) and (C=5.70, b=0.32) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a pressure relief valve arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere,...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.30, b=0.38) and (C=6.00, b=0.25) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in parallel. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.30, b=0.38) and (C=2.80, b=0.25) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a pressure relief valve arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere,...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.30, b=0.38) and (C=3.30, b=0.40) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for two pressure relief valves arranged in parallel. Three test configurations were used: (1) being emptied tank -> the first PRV -> ambient atmosphere, (2) being...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=4.40, b=0.42) and (C=2.00, b=0.11) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a pressure relief valve arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere,...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=4.40, b=0.42) and (C=6.40, b=0.45) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for two pressure relief valves arranged in parallel. Three test configurations were used: (1) being emptied tank -> the first PRV -> ambient atmosphere, (2) being...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=4.40, b=0.42) and (C=6.00, b=0.25) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in parallel. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=4.40, b=0.42) and (C=2.40, b=026.) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a pressure relief valve arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere,...
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Determination of flow properties of a serial connection of a pressure relief valve with (C=4.4, b=0.42) and a air blow gun from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.70, b=0.32) and (C=3.30, b=0.40) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a pressure relief valve arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere,...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=4.40, b=0.42) and (C=2.10, b=0.14) from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a pressure relief valve arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere,...
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Determination of flow properties of a serial connection of a pressure relief valve with (C=5.3, b=0.38) and a air blow gun from changes in air pressure in a tank being emptied
Open Research DataThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Improving operating efficiency of a gas turboset via cooperation with an absorption refrigerating machine
PublicationThe analysis of increase of ambient air temperature entering the compressor on reduction in power output from the turbine and increase fuel use was conduced. For medium size gas turbine operates in winter and summer conditions elementary power and economical values was calculated. Conditions of the determination of turbine inlet air cooling solution (using thermal storage for reduce equipment size) are presented
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Boron Difluoride Complexes of Carbamoyl Meldrum's Acids
Publication5-[Hydroxy(aryl/alkylamino)methylene]-2,2-dimethyl-1,3-dioxane-4,6-diones react with BF3•Et2O in mild conditions leading to the formation of boron difluoride complexes of carbamoyl Meldrum's acids. The X-ray structure has been obtained for one representative complex. The obtained new compounds are fairly stable at standard ambient conditions and easily isolable.
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Bartłomiej Luks dr
PeopleI'm a snow researcher, working in the Arctic for almost 20 years. I've started as a field assistant on a geological expedition to Bellsund (Spitsbergen), then did my masters on soil pollution in the vicinity of Polish Polar Station Hornsund and PhD on dynamics of snowpack in the SW Spitsbergen. Since 2013 I'm an Assistant Professor at the Department of Polar and Marine Research IG PAS in Warsaw. My main research interests are the...
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TiO2 /SrTiO3 and SrTiO3 microspheres decorated with Rh, Ru or Pt nanoparticles: Highly UV–vis responsible photoactivity and mechanism
PublicationA series of TiO2/SrTiO3 and SrTiO3 microspheres decorated by Rh, Ru or Pt NPs were prepared by facile hydrothermal method. The as-prepared samples were characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), transmission electron microscopy (TEM) with energy-dispersive Xray (EDX) spectroscopy, scanning electron microscopy (SEM), photoluminescence spectrometry (PL), Fourier transform infrared (FT-IR) and...
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α-Pinene, 3-carene and d-limonene in indoor air of Polish apartments: The impact on air quality and human exposure
PublicationMonoterpenes are among most ubiquitous volatile organic compounds (VOCs) to be detected in indoor air. Since the quality of indoor air is considered important for inhabitants' well-being, the present study aimed at investigating impact of human activity on levels of selected monoterpenes applying passive sampling technique followed by thermal desorption and gas chromatography coupled mass spectrometry. One of the objectives of...
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Modern approach for determination of lactulose, mannitol and sucrose in human urine using HPLC-MS/MS for the studies of intestinal and upper digestive tract permeability
PublicationA new analytical procedure was described for the simultaneous determination of lactulose, mannitol and sucrose in urine, in which HILIC chromatography and tandem mass spectrometry detection are used. Sugars are orally administered for the estimation of intestinal permeability in children digestive tract. Samples were purified by dispersive solid phase extraction (d-SPE) using Amberlite MB150 resin. Raffinose was selected as an...
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Influence of Storage Time and Temperature on the Toxicity, Endocrine Potential, and Migration of Epoxy Resin Precursors in Extracts of Food Packaging Materials
PublicationThe aim of the present study was to establish a standard methodology for the extraction of epoxy resin precursors from several types of food packages (cans, multi-layered composite material, and cups) with selected simulation media (distilled water, 5% ethanol, 3% dimethyl sulfoxide, 5% acetic acid, artificial saliva) at different extraction times and temperatures (factors). Biological analyses were conducted to determine the acute...
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Exhaled breath analysis by resistive gas sensors
PublicationBreath analysis has attracted human beings for centuries. It was one of the simplest methods to detect various diseases by using human smell sense only. Advances in technology enable to use more reliable and standardized methods, based on different gas sensing systems. Breath analysis requires the detection of volatile organic compounds (VOCs) of the concentrations below individual ppm (parts per million). Therefore, advanced detection...
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Determination of Glycerol, Propylene Glycol, and Nicotine as the Main Components in Refill Liquids for Electronic Cigarettes
PublicationRefill liquids for electronic cigarettes are an important area of research due to the health safety and quality control of such products. A method was developed for the determination of glycerol, propylene glycol, and nicotine in refill liquids using liquid chromatography, coupled with tandem mass spectrometry (LC-MS/MS) in multiple reaction monitoring (MRM) mode with electrospray ionisation (ESI). Sample preparation was based...
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Searching for the primary metabolic alterations of polycystic ovary syndrome by application of the untargeted metabolomics approach
PublicationDespite a large number of studies, the pathogenesis of polycystic ovary syndrome (PCOS) still remains unexplained. In light of ambiguous observations reported in metabolomics, there is a need to carry out studies focusing on confirming the discriminating power of the proposed metabolomics biomarkers. Our research aimed to perform a validation study of metabolites detected in our previous study from serum samples, on the new set...
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A comprehensive lipidomic analysis of oilseeds using LC-Q-TOF-MS and dispersive micro-solid phase (D-μ-SPE) extraction techniques
PublicationGrowing public health awareness increased the demand for natural products with positive health benefits. Vegetable oils containing omega-3 fatty acids (FA) such as alpha-linolenic acid (ALA) has been proposed as a possible source of eicosapentaenoic acid (EPA) and docosahexaenoic acid (DHA). In this work, a comprehensive lipidome analysis and comparison of seven oilseeds, including flaxseed, chia, hemp, black cumin, white sesame,...
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Untargeted Lipidomics Reveals Differences in the Lipid Pattern among Clinical Isolates of Staphylococcus aureus Resistant and Sensitive to Antibiotics
PublicationStaphylococcus aureus resistance to antibiotics is a significant clinical problem worldwide. In this study, an untargeted lipidomics approach was used to compare the lipid fingerprints of S. aureus clinical isolates that are resistant and sensitive to antibiotics. High-performance liquid chromatography coupled with time-of-flight mass spectrometry was employed to rapidly and comprehensively analyze bacterial lipids. Chemometric...
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The content of biogenic amines in Rondo and Zweigelt wines and correlations between selected wine parameters
PublicationThe purpose of this study was to evaluate the content of biogenic amines (BAs) in wines using dispersive liquid–liquid microextraction–gas chromatography–mass spectrometry (DLLME-GC–MS). An additional objective was to assess the correlations between selected parameters characterizing the samples such as the content of BAs, sugars, and organic acids, pH, and total acidity. Wines produced from the same grape variety in which alcoholic...
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Anticancer and antimicrobial properties of novel η6-p-cymene ruthenium(ii) complexes containing a N,S-type ligand, their structural and theoretical characterization
PublicationRuthenium(II) complexes are lately of great scientific interest due to their chemotherapeutic potential asanticancer and antimicrobial agents. Here we present the synthesis of new pyrazole carbothioamidederivatives and their four arene–ruthenium complexes. The title compounds were characterized with theapplication of IR, NMR, mass spectrometry, elemental analysis and X-ray diffraction. Additionally, for newcomplexes DFT calculations...
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The potential of LC–MS technique in direct analysis of perfume content
PublicationPerfumes are products that consist of a wide range of natural and synthetic compounds. Due to complex composition, the determination of their ingredients is a difficult task. Most of the perfume components are either volatile or semi-volatile; however, most of the attention has been paid to volatile ones, and thus, gas chromatography or electronic noses are generally used. Nevertheless, in this study, liquid chromatography coupled...
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Density, sound velocity, viscosity, and refractive index of new morpholinium ionic liquids with amino acid-based anions: Effect of temperature, alkyl chain length, and anion
PublicationIn this work, room temperature synthesis of twenty new ionic liquids (ILs) based on the N-alkyl-N-methylmorpholinium ([Mor1,R], R = 2, 3, 4, 6, 8) cation and N-acetyl-L-amino acid anions (L-alaninate, L-valinate, L-leucinate, L-isoleucinate) was described. The synthesized ILs were characterized by various spectroscopic techniques and high-resolution mass spectrometry. Furthermore, density (ρ), sound velocity (v), viscosity (η)...
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Presence of antibiotics in the aquatic environment in Europe and their analytical monitoring: Recent trends and perspectives
PublicationThe presence of antibiotics and their metabolites in the aquatic environment exerts a negative impact on all organisms. Moreover, the easy migration of these substances to drinking water may also have serious consequences for public health, such as drug resistance. Although antibiotics and their metabolites are detected in surface waters and wastewater, there are still no systemic solutions preventing environmental pollution with...
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UV-induced electron transfer between triethylamine and 5-bromo-2′-deoxyuridine. A puzzle concerning the photochemical debromination of labeled DNA
Publication5-Bromo-2'-deoxyuridine (BrdU) photosensitizes DNA to strand break formation. However, this type of photodamage is completely quenched by the presence of triethylamine (TEA) which originates from RP-HPLC purification commonly employed by oligonucleotide providers. While the presence of TEA in oligonucleotide samples does not interfere with PCR or other molecular biology applications, the mechanism of photochemical reaction proceeding...
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Primary degradation of antidiabetic drugs
PublicationType 2 diabetes is a chronic disease affecting a large portion of the world population and is treated by orally administered drugs. Since these drugs are often taken in high doses and are excreted unchanged or partially metabolised many of them are nowadays detected in surface waters or wastewater treatment plants effluents. Unmetabolised antidiabetics or some of their transformation products retain their pharmacological activity,...