Search results for: Α-AMIDOALKYLATION - Bridge of Knowledge

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Search results for: Α-AMIDOALKYLATION

Search results for: Α-AMIDOALKYLATION

  • Oxidation step in the preparation of benzocamalexin: The crystallographic evidence

    Publication
    • Y. Stremski
    • A. Ahmedova
    • A. Dołęga
    • S. Statkova-Abeghe
    • D. Kirkova

    - MENDELEEV COMMUNICATIONS - Year 2021

    The study of oxidation step in the preparation of benzocamalexin by the α-amidoalkylation–oxidation sequence revealed the formation of perchloro-1,2-phenylene dibenzoate as the product of transformation of tetrachloro- 1,2-benzoquinone applied as the oxidant. The structures of benzocamalexin and perchloro-1,2-phenylene dibenzoate were confirmed by X-ray diffraction analysis. The extraction step in the final isolation of benzocamalexin...

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