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Oxidation step in the preparation of benzocamalexin: The crystallographic evidence

Abstract

The study of oxidation step in the preparation of benzocamalexin by the α-amidoalkylation–oxidation sequence revealed the formation of perchloro-1,2-phenylene dibenzoate as the product of transformation of tetrachloro- 1,2-benzoquinone applied as the oxidant. The structures of benzocamalexin and perchloro-1,2-phenylene dibenzoate were confirmed by X-ray diffraction analysis. The extraction step in the final isolation of benzocamalexin is supposed to be crucial for the complete transformation of mono- and di- acylated perchloropyrocatechol.

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Category:
Articles
Type:
artykuły w czasopismach
Published in:
MENDELEEV COMMUNICATIONS no. 31, pages 824 - 826,
ISSN: 0959-9436
Language:
English
Publication year:
2021
Bibliographic description:
Stremski Y., Ahmedova A., Dołęga A., Statkova-Abeghe S., Kirkova D.: Oxidation step in the preparation of benzocamalexin: The crystallographic evidence// MENDELEEV COMMUNICATIONS -Vol. 31,iss. 6 (2021), s.824-826
DOI:
Digital Object Identifier (open in new tab) 10.1016/j.mencom.2021.11.018
Verified by:
Gdańsk University of Technology

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