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“Green” nature of the process of derivatization in analytical sample preparation

Abstract

Nowadays, the idea of Green Analytical Chemistry (GAC) is of high importance what impacts on the rapid growth in the sample preparation area with special emphasis on sample preparation simplification, miniaturization, and automation. Because the derivatization process is often an essential element of the analytical procedure, it should be important to focus on this issue from GAC perspective and conduct a series of experiments in order to develop the most favorable conditions. Application of microextraction techniques coupled with the derivatization perfectly meets the specified requirements. Other approaches to perform derivatization process in “green” way include the application of eco-friendly solvents/reagents, enhanced parameters such as microwaves or ultrasound and application of in-port, on-column/ in-capillary derivatization modes. This review describes factors that allow making derivatization process more green, different modes and ways of derivatization procedures involving less toxic, hazardous reagents/ solvents and more efficient forms of energy. Moreover, microextraction techniques that are often coupled to derivatization are described with examples.

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Category:
Articles
Type:
artykuł w czasopiśmie wyróżnionym w JCR
Published in:
TRAC-TRENDS IN ANALYTICAL CHEMISTRY no. 102, pages 16 - 31,
ISSN: 0165-9936
Language:
English
Publication year:
2018
Bibliographic description:
Płotka-Wasylka J., Sajid, M.: “Green” nature of the process of derivatization in analytical sample preparation// TRAC-TRENDS IN ANALYTICAL CHEMISTRY. -Vol. 102, (2018), s.16-31
DOI:
Digital Object Identifier (open in new tab) 10.1016/j.trac.2018.01.005
Verified by:
Gdańsk University of Technology

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