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Abstract
We have developed a convenient methods for the synthesis of symmetrical trisulfides under mild conditions in very good yields. The described methods are based on the straightforward preparation of 5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinane-2-disulfanyl derivatives from readily available 5,5-dimethyl-2-sulfanyl-2-thioxo-1,3,2-dioxaphosphorinane or bis(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl) disulfide. The symmetrical trisulfides can be obtained from aliphatic, aromatic thiols and L-cysteine derivatives as well.
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- Publication version
- Accepted or Published Version
- DOI:
- Digital Object Identifier (open in new tab) 10.1055/s-0028-1088161
- License
- Copyright (2009 Georg Thieme Verlag Stuttgart)
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- Category:
- Articles
- Type:
- artykuł w czasopiśmie wyróżnionym w JCR
- Published in:
-
SYNTHESIS-STUTTGART
pages 1459 - 1462,
ISSN: 0039-7881 - Language:
- English
- Publication year:
- 2009
- Bibliographic description:
- Kertmen A., Lach S., Rachoń J., Witt D.: Novel and Efficient Methods for the Synthesis of Symmetrical Trisulfides// SYNTHESIS-STUTTGART. -, nr. iss. 9 (2009), s.1459-1462
- Verified by:
- Gdańsk University of Technology
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