TBAF Promoted Formation of Symmetrical Trisulfides

Sławomir Lach; Dariusz Witt

doi:10.1002/hc.21129

TBAF Promoted Formation of Symmetrical Trisulfides

Abstract

We have developed a new method for the synthesis of functionalized symmetrical trisulfides based on (5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorin-2-yl)disulfanyl derivatives prepared from readily available 5,5-dimethyl-2-sul-fanyl-2-thioxo-1,3,2-dioxaphosphorinane or bis(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl) disulfide. The symmetrical trisulfides can be obtained from aliphatic and aromatic thiols andL-cysteine derivatives under mild conditions with high yield and purity.

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Authors (2)

Sławomir Lach
Dariusz Witt prof. dr hab. inż.

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Category:: Articles
Type:: artykuł w czasopiśmie wyróżnionym w JCR
Published in:: HETEROATOM CHEMISTRY no. 25, edition 1, pages 10 - 14,
ISSN: 1042-7163
Language:: English
Publication year:: 2014
Bibliographic description:: Lach S., Witt D.: TBAF Promoted Formation of Symmetrical Trisulfides// HETEROATOM CHEMISTRY. -Vol. 25, iss. 1 (2014), s.10-14
DOI:: Digital Object Identifier (open in new tab) 10.1002/hc.21129
Verified by:: Gdańsk University of Technology