Optimization of a Fabric Phase Sorptive Extraction protocol for the isolation of six bisphenols from juice pouches to be analysed by high performance liquid chromatography coupled with diode array detector - Publication - Bridge of Knowledge

Your account

login

Search

Optimization of a Fabric Phase Sorptive Extraction protocol for the isolation of six bisphenols from juice pouches to be analysed by high performance liquid chromatography coupled with diode array detector

Abstract

Fabric Phase Sorptive Extraction (FPSE) combined with high pressure liquid chromatography using to diode array detection (HPLC-DAD) was applied for the simultaneous determination of bisphenols (BPA, BPB, BPC, BPE, BPF, BPS) in juice pouches. The FPSE procedure was optimized with regards to the critical parameters that affect the performance of the method including the selection of the FPSE membrane type and size, adsorption time, extraction time, solvent volume desorption, magnetic stirring ratio, and salt addition. The FPSE membrane could be reused up to 14 times. The developed FPSE-HPLC-DAD method was validated in terms of linearity, sensitivity, accuracy andprecision. The limits of detection (LODs) were lower than 6.9 ng/mL, while the limits of quantification (LOQs) were lower than 21 ng/mL. The results obtained are satisfactory in terms of precision, accuracy and repeatability, with recoveries above 86% and CV values below 9.5%. The FPSE-HPLC-DAD method was successfully applied in the determination of six bisphenols in juice samples stored in pouches.

Citations

  • 6

    CrossRef

  • 0

    Web of Science

  • 5

    Scopus

Authors (5)

Cite as

Full text

full text is not available in portal

Keywords

Details

Category:
Articles
Type:
artykuły w czasopismach
Published in:
JOURNAL OF CHROMATOGRAPHY A no. 1708,
ISSN: 0021-9673
Language:
English
Publication year:
2023
Bibliographic description:
Kubica P., Kalogiouri N., Kabir A., Furton K. G., Samanidou V. F.: Optimization of a Fabric Phase Sorptive Extraction protocol for the isolation of six bisphenols from juice pouches to be analysed by high performance liquid chromatography coupled with diode array detector// JOURNAL OF CHROMATOGRAPHY A -Vol. 1708, (2023), s.464366-
DOI:
Digital Object Identifier (open in new tab) 10.1016/j.chroma.2023.464366
Sources of funding:
  • Free publication
Verified by:
Gdańsk University of Technology

seen 66 times

Recommended for you

Comparative study of bisphenols in e-cigarette liquids: evaluating fabric phase sorptive extraction, ultrasound-assisted membrane extraction, and solid phase extraction techniques

2024

Extraction and Analysis of Bisphenols and Their Derivatives in Infant and Toddler Ready-to-feed Meals by Ultrasound-assisted Membrane Extraction Followed by LC MS/MS

2023

An air-assisted dispersive liquid phase microextraction method based on a hydrophobic magnetic deep eutectic solvent for the extraction and preconcentration of melamine from milk and milk-based products

  • A. Elik,
  • S. Fesliyan,
  • N. Gürsoy
  • + 3 authors
2023

Simultaneous Determination of Indolic Compounds in Plant Extracts by Solid-Phase Extraction and High-Performance Liquid Chromatography with UV and Fluorescence Detection

2015
Meta Tags