Optimization of a Fabric Phase Sorptive Extraction protocol for the isolation of six bisphenols from juice pouches to be analysed by high performance liquid chromatography coupled with diode array detector - Publication - Bridge of Knowledge

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Optimization of a Fabric Phase Sorptive Extraction protocol for the isolation of six bisphenols from juice pouches to be analysed by high performance liquid chromatography coupled with diode array detector

Abstract

Fabric Phase Sorptive Extraction (FPSE) combined with high pressure liquid chromatography using to diode array detection (HPLC-DAD) was applied for the simultaneous determination of bisphenols (BPA, BPB, BPC, BPE, BPF, BPS) in juice pouches. The FPSE procedure was optimized with regards to the critical parameters that affect the performance of the method including the selection of the FPSE membrane type and size, adsorption time, extraction time, solvent volume desorption, magnetic stirring ratio, and salt addition. The FPSE membrane could be reused up to 14 times. The developed FPSE-HPLC-DAD method was validated in terms of linearity, sensitivity, accuracy andprecision. The limits of detection (LODs) were lower than 6.9 ng/mL, while the limits of quantification (LOQs) were lower than 21 ng/mL. The results obtained are satisfactory in terms of precision, accuracy and repeatability, with recoveries above 86% and CV values below 9.5%. The FPSE-HPLC-DAD method was successfully applied in the determination of six bisphenols in juice samples stored in pouches.

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Category:
Articles
Type:
artykuły w czasopismach
Published in:
JOURNAL OF CHROMATOGRAPHY A no. 1708,
ISSN: 0021-9673
Language:
English
Publication year:
2023
Bibliographic description:
Kubica P., Kalogiouri N., Kabir A., Furton K. G., Samanidou V. F.: Optimization of a Fabric Phase Sorptive Extraction protocol for the isolation of six bisphenols from juice pouches to be analysed by high performance liquid chromatography coupled with diode array detector// JOURNAL OF CHROMATOGRAPHY A -Vol. 1708, (2023), s.464366-
DOI:
Digital Object Identifier (open in new tab) 10.1016/j.chroma.2023.464366
Sources of funding:
  • Free publication
Verified by:
Gdańsk University of Technology

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