Journal of the Chemical Society, Perkin Transactions 1 - Journal - Bridge of Knowledge

Journal of the Chemical Society, Perkin Transactions 1

ISSN:

0300-922X

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https://v2.sherpa.ac.uk/id/publication/32190

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total: 1

Year 2002

Synthesis of S-thioacyl dithiophosphates, efficient and chemoselectivethioacylating agents
Publication
- L. Doszczak
- J. Rachoń
- Journal of the Chemical Society, Perkin Transactions 1 - Year 2002
Łatwo dostępne ditiofosforany acylu izomeryzują do monotiofosforanów O- iS-tioacylu. Reakcja jest odwracalna, więc ogrzewanie ditiofosforanów acylu prowadzi zazwyczaj do powstania mieszaniny izomerycznych bezwodników, która nie może być wykorzystana do wydajnego tioacylowania. Jednak działaniem kwasu ditiofosforowego na mieszaninę izomerycznych bezwodników można wydajnie otrzymać ditiofosforany tioacylu. Związki te to doskonałe...

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