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Abstract
We developed a simple and efficient method for the synthesis of functionalized unsymmetrical disulfanes under mild conditions in good yields. The designed method is based on the reaction of bis(5,5- dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl)disulfane with thiols in the presence of 2,3-dichloro-5,6-dicyanobenzoquinone (DDQ). The developedmethod allows the preparation of unsymmetrical disulfanes bearing additional hydroxy, carboxy, or amino functionalities.
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- Publication version
- Accepted or Published Version
- DOI:
- Digital Object Identifier (open in new tab) 10.1039/c5ra04173b
- License
- Copyright (2015 The Royal Society of Chemistry)
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- Category:
- Articles
- Type:
- artykuł w czasopiśmie wyróżnionym w JCR
- Published in:
-
RSC Advances
no. 5,
edition 40,
pages 31347 - 31351,
ISSN: 2046-2069 - Language:
- English
- Publication year:
- 2015
- Bibliographic description:
- Musiejuk M., Klucznik T., Rachoń J., Witt D.: DDQ-mediated synthesis of functionalized unsymmetrical disulfanes// RSC Advances. -Vol. 5, iss. 40 (2015), s.31347-31351
- DOI:
- Digital Object Identifier (open in new tab) 10.1039/c5ra04173b
- Verified by:
- Gdańsk University of Technology
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