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Abstract
We have developed a convenient method for the synthesis of unsymmetrical trisulfides under mild conditions in very good yields. The designed method is based on the straightforward preparation of 1-[(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl)trisulfanyl]dodecane from readily available 5,5-dimethyl-2-sulfanyl-2-thioxo-1,3,2-dioxaphosphorinane, sulfur dichloride (SCl2) and dodecane-1-thiol. The unsymmetrical trisulfides can be obtained from aliphatic, aromatic thiols and l-cysteine derivatives as well.
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- Category:
- Articles
- Type:
- artykuł w czasopiśmie wyróżnionym w JCR
- Published in:
-
SYNLETT
pages 2857 - 2860,
ISSN: 0936-5214 - Language:
- English
- Publication year:
- 2010
- Bibliographic description:
- Lach S., Śliwka-Kaszyńska M., Witt D.: Novel and Efficient Synthesis of Unsymmetrical Trisulfides// SYNLETT. -, nr. iss. 19 (2010), s.2857-2860
- DOI:
- Digital Object Identifier (open in new tab) 10.1055/s-0030-1259033
- Verified by:
- Gdańsk University of Technology
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