Search results for: EXSOLUTION

• SEM images of (La0.3Sr0.6Ce0.1)0.9Me0.1Ti0.9O3-δ (Me=Co, Fe, Ni) powder materials after reduction at 1000 deg.C in hydrogen

  Open Research Data

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  • B. Bochentyn
  • K. Kujawska

  The dataset presents SEM images of (La0.3Sr0.6Ce0.1)0.9Me0.1Ti0.9O3-δ (Me=Co, Fe, Ni) powder materials after reduction at 1000 deg.C in hydrogen. The powders were synthesized via the Pechini method. The reduction was performed in order to force the exsolution process of metallic nanoparticles. 

• SEM images of (La0.3Sr0.6Ce0.1)0.9(Me1Me2Ti)O3-δ (Me1,Me2=Co, Fe, Ni) powder materials after reduction at 1000 deg.C in hydrogen

  Open Research Data

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  • B. Bochentyn
  • K. Kujawska

  The dataset presents SEM images of (La0.3Sr0.6Ce0.1)0.9(Me1Me2Ti)O3-δ (Me1,Me2=Co, Fe, Ni) powder materials after reduction at 1000 deg.C in hydrogen. The powders were synthesized via the Pechini method. The reduction was performed to force the exsolution process of bimetallic nanoparticles. 

• The XRD diffraction patterns of (La0.3Sr0.6Ce0.1)0.9FexTi(1-x)O3-δ (x=0.1, 0.2 and 0.3) materials after reduction at 900 deg.C in hydrogen

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  • B. Bochentyn
  • A. Ghosal

  The (La0.3Sr0.6Ce0.1)0.9FexTi(1-x)O3-δ (x=0.1, 0.2 and 0.3) materials were synthesized via the Pechini method. First, the reagents in the form of nitrates were weighed and dissolved in DI water. In another beaker, a stoichiometric amount of titanium (IV) butoxide (Ti(OBu)4) was mixed together with reagent-grade ethylene glycol (EG), and citric acid...

• SEM images of SFM, LSFM and SFMNb in as-prepared state and reduced

  Open Research Data

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  • A. Ducka
  • B. Bochentyn

  - series: SFM

  This dataset contains SEM images taken for pristine strontium ferrite molybdate, as well as ones doped with lanthanum or niobium. Materials were characterized in powder, under high vacuum in secondary electron mode. The images are divided into folders for as-prepared samples and reduced (H2, 800 deg, 4 h) ones. 

• The XRD diffraction patterns of (La0.3Sr0.6Ce0.1)0.9Me0.1Ti0.9O3-δ (Me= Co, Cu, Fe, Mn, Ni) materials after reduction at 1000 deg.C in hydrogen

  Open Research Data

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  • B. Bochentyn
  • A. Girma Berhanu

  - series: LSCMeT SSR

  The (La0.3Sr0.6Ce0.1)0.9Me0.1Ti0.9O3-δ (Me= Co, Cu, Fe, Mn, Ni) materials were synthesized via the solid state reaction method and examined as a potential anode material. First, the mixed oxide reagents were pressed into pellets and calcined at 1200 °C for 12 hours to decompose most of the organic compounds. The resulting calcined pellet was ground...

• The XRD diffraction patterns of (La0.3Sr0.6Ce0.1)0.9Me0.1Ti0.9O3-δ (Me= Co, Cu, Fe, Mn, Ni) materials after reduction at 1100 deg.C in hydrogen

  Open Research Data

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  • B. Bochentyn
  • A. Girma Berhanu

  - series: LSCMeT SSR

  The (La0.3Sr0.6Ce0.1)0.9Me0.1Ti0.9O3-δ (Me= Co, Cu, Fe, Mn, Ni) materials were synthesized via the solid state reaction method and examined as a potential anode material. First, the mixed oxide reagents were pressed into pellets and calcined at 1200 °C for 12 hours to decompose most of the organic compounds. The resulting calcined pellet was ground...

• Change of exhaust gases concentration for reference SOFC and SOFC with LSCNT layer fueled by biogas mixture at 750 C

  Open Research Data

  open access

  • P. Błaszczak
  • B. Bochentyn

  - series: Exsolution

  The dataset changes of exhaust gases concentrations (CH4,CO,CO2,H2) over working time for SOFC with La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s layer as well as reference SOFEC (unmodified). Concentrations were calculated based on the FTIR measurements and calibration curves presented in different dataset. Longterm measurements of SOFC were performed using in-house...

• Electrical power measurement of LSCNT modified SOFC fueled by biogas mixture at 750 C

  Open Research Data

  open access

  • P. Błaszczak
  • B. Bochentyn

  - series: Exsolution

  The dataset contains the electrical measurements of IV curves for SOFC with La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s layer working under biogas and H2 feeding stream. The SOFC was reduced at 900C and conditioned for 12 h under H2 prior the measurements. The measurements were performed using Gamry potentiostat/galvanostat

• The SEM images of LSCNT reduced at 900 degrees C under H2

  Open Research Data

  open access

  • P. Błaszczak
  • B. Bochentyn

  - series: Exsolution

  The dataset includes SEM image of La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s sintered at 1200oC under air atmosphere for 12 h and reduced at 900oC under H2 for 10 h. Samples were produced using aqueous soft chemistry methods (Pechini).

• FTIR spectra of SOFC with LSCNT layer fueled by biogas mixture at 750 C (pure)

  Open Research Data

  open access

  • P. Błaszczak
  • B. Bochentyn

  - series: Exsolution

  The dataset contains the FTIR spectra collected during the electrical measurements DIR-SOFC with LSCNT layer. The SOFC was reduced at 800degC in H2 prior to mesurements. The spectra were collected every 10 min.

• The SEM images of LSCNT sintered at 1200 degrees C in air

  Open Research Data

  open access

  • P. Błaszczak
  • B. Bochentyn

  - series: Exsolution

  The dataset includes SEM images of La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s sintered at 1200oC under air atmosphere for 12 h. Samples were produced using aqueous soft chemistry methods (Pechini). The grain structure can be seen on higher resolution image.

• Electrical performance measurement of reference and SOFC with LSCNT layer fueled by H2 and 20ppm H2S/biogas mixture at 750 C - cyclic measurements (12h per cycle)

  Open Research Data

  open access

  • P. Błaszczak
  • B. Bochentyn

  - series: Exsolution

  The dataset contains the electrical IV measurements collected during the cyclic measurements of H2S poisoning in DIR-SOFC with/-out LSCNT layer. The H2S poisoning and H2 regenrating cycles were 12 h each. The spectra were collected every 10 min.

• The XRD diffraction patterns of reduced LSCNT prepared using two methods and two sintering temperatures

  Open Research Data

  open access

  • P. Błaszczak
  • B. Bochentyn

  - series: Exsolution

  The dataset includes XRD diffraction patterns of La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s produced using two methods, namely organic (citrate assisted) and Pechini sintered at 1000 or 1200oC under air atmosphere and reduced at 900 for 12 h in wet H2.

• The XRD diffraction patterns of LSCNT of different A site nonstoichiometry

  Open Research Data

  open access

  • P. Błaszczak
  • B. Bochentyn

  - series: Exsolution

  The dataset includes XRD diffraction patterns of La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s and La0.3Sr0.6Ce0.1Ni0.1Ti0.9O3-s sintered at 1200oC under air atmosphere for 12 h. Samples were produced using aqueous soft chemistry methods (Pechini).

• The SEM images of LSCNT reduced at 800 degrees C under H2

  Open Research Data

  open access

  • P. Błaszczak
  • B. Bochentyn

  - series: Exsolution

  The dataset includes SEM images of La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s sintered at 1200oC under air atmosphere for 12 h and reduced at  800oC under H2 for 10 h. Samples were produced using aqueous soft chemistry methods (Pechini).

• Electrical power measurement of reference SOFC fueled by biogas mixture at 750 C

  Open Research Data

  open access

  • P. Błaszczak
  • B. Bochentyn

  - series: Exsolution

  The dataset contains the electrical measurements of IV curves for SOFC without La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s layer working under biogas and H2 feeding stream. The SOFC was reduced at 900C and conditioned for 12 h under H2 prior the measurements. The measurements were performed using Gamry potentiostat/galvanostat

• FTIR spectra of SOFC with LSCNT layer fueled by H2 and 20ppm H2S/biogas mixture at 750 C - cyclic measurements (12h per cycle)

  Open Research Data

  open access

  • P. Błaszczak
  • B. Bochentyn

  - series: Exsolution

  The dataset contains the FTIR spectra collected during the cyclic measurements of H2S poisoning in DIR-SOFC with LSCNT layer. The H2S poisoning and H2 regenrating cycles were 12 h each. The spectra were collected every 10 min.

• The SEM images of LSCNT reduced at 1000 degrees C under H2

  Open Research Data

  open access

  • P. Błaszczak
  • B. Bochentyn

  - series: Exsolution

  The dataset includes SEM images of La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s sintered at 1200oC under air atmosphere for 12 h and reduced at 1000oC under H2 for 10 h. Samples were produced using aqueous soft chemistry methods (Pechini).

• Change of exhaust gases concentration for LSCNT modified SOFC fueled by biogas mixture at 750 C

  Open Research Data

  open access

  • P. Błaszczak
  • B. Bochentyn

  - series: Exsolution

  The dataset changes of exhaust gases concentrations (CH4,CO,CO2,H2) over working time for SOFC with La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s layer. Concentrations were calculated based on the FTIR measurements and calibration files presented in coupled dataset. 

• FTIR spectra of reference SOFC fueled by H2 and 20ppm H2S/biogas mixture at 750 C - cyclic measurements (12h per cycle)

  Open Research Data

  open access

  • P. Błaszczak
  • B. Bochentyn

  - series: Exsolution

  The dataset contains the FTIR spectra collected during the cyclic measurements of H2S poisoning in DIR-SOFC without LSCNT layer. The H2S poisoning and H2 regenrating cycles were 12 h each. The spectra were collected every 10 min.

• The EDS elemental maps of reduced LSCNT (SEM)

  Open Research Data

  open access

  • P. Błaszczak
  • B. Bochentyn

  - series: Exsolution

  The dataset includes elemental maps of La, Ce, Ti, O, Sr, Ni in La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s produced using Pechini method sintered at 1200oC under air atmosphere and reduced at 900 for 12 h in wet H2.

• The XRD diffraction patterns of LSCNT sintered at various temperatures

  Open Research Data

  open access

  • P. Błaszczak
  • B. Bochentyn

  - series: Exsolution

  The dataset includes XRD diffraction patterns of La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s sintered at various temperatures under air atmosphere for 12 h. Samples were produced using aqueous soft chemistry methods (Pechini).

• The XPS spectra of LSCNT sintered at 1200C

  Open Research Data

  open access

  • P. Błaszczak
  • B. Bochentyn

  - series: Exsolution

  The dataset includes XPS spectra of La0.27Sr0.54Ce0.09Ni0.1Ti0.9O3-s sintered at various temperatures under air atmosphere for 12 h. Samples were produced using aqueous soft chemistry methods (Pechini). The XPS spectra were collected for all species.