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Search results for: SPEKTROSKOPIA MOSSBAUERA

  • Thermal analysis of bis(tetraethylammonium) tetrachloroferrate(II)

    Publication
    • E. Styczeń
    • A. Pattek-Jańczyk
    • M. Gazda
    • W. K. Jóźwiak
    • D. Wyrzykowski
    • Z. Warnke

    - THERMOCHIMICA ACTA - Year 2008

    Badano dekompozycję termiczną związków bis(tetraethylammonium) tetrachloroferrate(II). Stosowano następujące metody badawcze: TG-FTIR, TG-MS i DTA. Pomiary przeprowadzono w atmosferze obojętnej w zakresie temperatur od 293 K do 1073 K. Stałe produkty dekompozycji identyfikowano metodą spektroskopii w podczerwieni, spektroskopii Mössbauera oraz metodą dyfrakcji promieniowania rentgenowskiego. Przedyskutowano wpływ stopnia utlenienia...

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  • 237Np Mössbauer effect study on NpFeAsO

    Publication
    • P. Gaczyński
    • T. Klimczuk
    • H. Walker
    • R. Springell
    • E. Colineau
    • R. Eloirdi
    • J. Griveau
    • R. Caciuffo

    - JOURNAL OF PHYSICS-CONDENSED MATTER - Year 2014

    We report 237Np Mössbauer measurements on NpFeAsO. The Np atoms were found to occupy only one crystallographic site. The value of the isomer shift (δ ∼ 9.1 mm s−1 versus NpAl2) indicates a 5f4 electronic configuration (Np3+ ions). The magnetic ordering of the Np sublattice below 60 K is established and the saturated ordered magnetic moment is determined to be 1.73μB at 3.6 K. The unique set of hyperfine parameters exclude a modulated...

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  • Synthetic, Structural, and Spectroscopic Characterization of a Novel Family of High-Spin Iron(II) [(β-Diketiminate)(phosphanylphosphido)] Complexes

    Publication

    - INORGANIC CHEMISTRY - Year 2017

    This work describes a series of iron(II) phosphanylphosphido complexes. These compounds were obtained by reacting lithiated diphosphanes R2PP(SiMe3)Li (R = t-Bu, i-Pr) with an iron(II) β-diketiminate complex, [LFe(μ2-Cl)2Li(DME)2] (1), where DME = 1,2-dimethoxyethane and L = Dippnacnac (β-diketiminate). While the reaction of 1 with t-Bu2PP(SiMe3)Li yields [LFe(η1-Me3SiPPt- Bu2)] (2), that of 1 with equimolar amounts of i-Pr2PP(SiMe3)Li,...

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