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Diastereoselective Synthesis of Z‐Alkenyl Disulfides from α‐Thiophosphorylated Ketones and Thiosulfonates
Abstract
We developed a simple and efficient method for the synthesis of functionalized unsymmetrical Z‐alkenyl disulfides under mild conditions in moderate to good yields. The designed method is based on the reaction of α‐thiophosphorylated carbonyl compounds with thiotosylates in the presence of a base. The developed method allows the preparation of unsymmetrical Z‐alkenyl disulfides bearing additional hydroxy, carboxy, or ester functionalities
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- Category:
- Articles
- Type:
- artykuły w czasopismach
- Published in:
-
ADVANCED SYNTHESIS & CATALYSIS
no. 362,
pages 618 - 626,
ISSN: 1615-4150 - Language:
- English
- Publication year:
- 2020
- Bibliographic description:
- Musiejuk M., Doroszuk J., Jędrzejewski B., Ortiz Nieto G., Marin Navarro M., Witt D.: Diastereoselective Synthesis of Z‐Alkenyl Disulfides from α‐Thiophosphorylated Ketones and Thiosulfonates// ADVANCED SYNTHESIS & CATALYSIS -Vol. 362,iss. 3 (2020), s.618-626
- DOI:
- Digital Object Identifier (open in new tab) 10.1002/adsc.201901208
- Sources of funding:
- Verified by:
- Gdańsk University of Technology
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