Thermal behaviour of ammonium vanadate nanocrystals

Description

The DataSet contains the thermal behavior of the ammonium vanadate nanostructures obtained by the hydrothermal method with different conditions. Thermogravimetric analysis (TG) was carried out under an argon atmosphere from 40C to 560C (with a heating rate of 10 C/min) using Netzsch STA 449 F1. The thermal behavior was also studied with mass spectrum (MS). The gases that come out from the samples during heating were monitored by the quadruple mass spectrometer Netzsch QMS 403C Aeolos. The mass spectra were measured from m/z 2 to 60. The results reveal the differences in registered ion currents.

These results are part of a project defined in Electrochimica Acta journal (10.1016/j.electacta.2020.135919). In this paper, the information about samples and synthesis details are reported.

Dataset file

TG-DTG-MS.zip

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Attribution
Raw data:: Data contained in dataset was not processed.

Details

Year of publication:

2020

Verification date:

2021-05-24

Creation date:

2018

Dataset language:

English

Fields of science:

materials engineering (Engineering and Technology)

DOI:

10.34808/2zmc-1g96

Funding:

Różnorodność form i rozmiarów - nowa droga syntezy nanostruktur związków z grupy (NH4)xMyOz (M = V, Mo, W)

Series:

Ammonium vanadate

Verified by:

Gdańsk University of Technology

Keywords

References

publication Pressure in charge. Neglected parameter in hydrothermal synthesis turns out to be crucial for electrochemical properties of ammonium vanadates

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