Wyszukiwarka
Mikołaj Walter
Zatrudnienie
- Doktorant w Politechnika Gdanska
Publikacje
Filtry
wszystkich: 1
Katalog Publikacji
Rok 2024
-
Convenient and efficient N-methylation of secondary amines under solvent-free ball milling conditions
PublikacjaIn the present work, we report the development of a rapid, efcient, and solvent-free procedure for the N-methylation of secondary amines under mechanochemical conditions. After optimization of the milling parameters, a vibrational ball mill was used to synthesize 26 tertiary N-methylated amine derivatives in a short time of 20 min (30 Hz frequency) and high yields ranging from 78 to 95%. An exception was compounds having a hydroxyl...
wyświetlono 386 razy