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Wyniki wyszukiwania dla: ambient mass spectrometry
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=4.40, b=0.42) and (C=5.30, b=0.38) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for two pressure relief valves arranged in parallel. Three test configurations were used: (1) being emptied tank -> the first PRV -> ambient atmosphere, (2) being...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.50, b=0.37) and (C=6.00, b=0.25) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV ->...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=4.40, b=0.42) and (C=3.30, b=0.40) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for two pressure relief valves arranged in parallel. Three test configurations were used: (1) being emptied tank -> the first PRV -> ambient atmosphere, (2) being...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=4.40, b=0.42) and (C=5.70, b=0.32) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a pressure relief valve arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere,...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.30, b=0.38) and (C=2.10, b=0.14) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a pressure relief valve arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere,...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.30, b=0.38) and (C=7.30, b=0.49) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for two pressure relief valves arranged in parallel. Three test configurations were used: (1) being emptied tank -> the first PRV -> ambient atmosphere, (2) being...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.30, b=0.38) and (C=6.20, b=0.38) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for two pressure relief valves arranged in parallel. Three test configurations were used: (1) being emptied tank -> the first PRV -> ambient atmosphere, (2) being...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=2.00, b=0.11) and (C=6.00, b=0.25) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV ->...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=2.10, b=0.14) and (C=6.00, b=0.25) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV ->...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=6.20, b=0.38) and (C=6.00, b=0.25) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in parallel. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.70, b=0.32) and (C=6.00, b=0.25) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a air blow gun (with nozzle removed) arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV ->...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.30, b=0.38) and (C=6.40, b=0.45) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for two pressure relief valves arranged in parallel. Three test configurations were used: (1) being emptied tank -> the first PRV -> ambient atmosphere, (2) being...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.30, b=0.38) and (C=5.70, b=0.32) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a pressure relief valve arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere,...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.30, b=0.38) and (C=6.00, b=0.25) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in parallel. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.30, b=0.38) and (C=2.80, b=0.25) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a pressure relief valve arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere,...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=5.30, b=0.38) and (C=3.30, b=0.40) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for two pressure relief valves arranged in parallel. Three test configurations were used: (1) being emptied tank -> the first PRV -> ambient atmosphere, (2) being...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=4.40, b=0.42) and (C=2.00, b=0.11) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a pressure relief valve arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere,...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=4.40, b=0.42) and (C=6.40, b=0.45) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for two pressure relief valves arranged in parallel. Three test configurations were used: (1) being emptied tank -> the first PRV -> ambient atmosphere, (2) being...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=4.40, b=0.42) and (C=6.00, b=0.25) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in parallel. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=4.40, b=0.42) and (C=2.40, b=026.) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a pressure relief valve arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere,...
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Determination of flow properties of a serial connection of a pressure relief valve with (C=4.4, b=0.42) and a air blow gun from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Determination of flow properties of a parallel connection of two pneumatic elements with (C=4.40, b=0.42) and (C=2.10, b=0.14) from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of parallel connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a directional control valve and a pressure relief valve arranged in parallel. Three test configurations were used: (1) being emptied tank -> DCV -> ambient atmosphere,...
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Determination of flow properties of a serial connection of a pressure relief valve with (C=5.3, b=0.38) and a air blow gun from changes in air pressure in a tank being emptied
Dane BadawczeThe aim of the study was to determine the flow properties of serial connection of pneumatic components.The experiments were to measure the pressure changes in a being emptied tank for a pressure relief valve and a air blow gun (with nozzle removed) arranged in-line. Three test configurations were used: (1) being emptied tank -> PRV -> ambient...
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Wave Method for Structural Health Monitoring: Testing Using Full-Scale Shake Table Experiment Data
PublikacjaAn algorithm of the wave method for structural health monitoring (SHM) is tested and calibrated using shake table experiment data of a full-scale, seven-story, reinforced-concrete building slice. The method is based on monitoring changes in the velocity of waves propagating vertically through the structure, identified by least-squares (LSQ) fit of beam models. The experiment was conducted by a team from the University of California,...
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Improving operating efficiency of a gas turboset via cooperation with an absorption refrigerating machine
PublikacjaThe analysis of increase of ambient air temperature entering the compressor on reduction in power output from the turbine and increase fuel use was conduced. For medium size gas turbine operates in winter and summer conditions elementary power and economical values was calculated. Conditions of the determination of turbine inlet air cooling solution (using thermal storage for reduce equipment size) are presented
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Boron Difluoride Complexes of Carbamoyl Meldrum's Acids
Publikacja5-[Hydroxy(aryl/alkylamino)methylene]-2,2-dimethyl-1,3-dioxane-4,6-diones react with BF3•Et2O in mild conditions leading to the formation of boron difluoride complexes of carbamoyl Meldrum's acids. The X-ray structure has been obtained for one representative complex. The obtained new compounds are fairly stable at standard ambient conditions and easily isolable.
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TiO2 /SrTiO3 and SrTiO3 microspheres decorated with Rh, Ru or Pt nanoparticles: Highly UV–vis responsible photoactivity and mechanism
PublikacjaA series of TiO2/SrTiO3 and SrTiO3 microspheres decorated by Rh, Ru or Pt NPs were prepared by facile hydrothermal method. The as-prepared samples were characterized by X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), transmission electron microscopy (TEM) with energy-dispersive Xray (EDX) spectroscopy, scanning electron microscopy (SEM), photoluminescence spectrometry (PL), Fourier transform infrared (FT-IR) and...
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α-Pinene, 3-carene and d-limonene in indoor air of Polish apartments: The impact on air quality and human exposure
PublikacjaMonoterpenes are among most ubiquitous volatile organic compounds (VOCs) to be detected in indoor air. Since the quality of indoor air is considered important for inhabitants' well-being, the present study aimed at investigating impact of human activity on levels of selected monoterpenes applying passive sampling technique followed by thermal desorption and gas chromatography coupled mass spectrometry. One of the objectives of...
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Modern approach for determination of lactulose, mannitol and sucrose in human urine using HPLC-MS/MS for the studies of intestinal and upper digestive tract permeability
PublikacjaA new analytical procedure was described for the simultaneous determination of lactulose, mannitol and sucrose in urine, in which HILIC chromatography and tandem mass spectrometry detection are used. Sugars are orally administered for the estimation of intestinal permeability in children digestive tract. Samples were purified by dispersive solid phase extraction (d-SPE) using Amberlite MB150 resin. Raffinose was selected as an...
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Primary degradation of antidiabetic drugs
PublikacjaType 2 diabetes is a chronic disease affecting a large portion of the world population and is treated by orally administered drugs. Since these drugs are often taken in high doses and are excreted unchanged or partially metabolised many of them are nowadays detected in surface waters or wastewater treatment plants effluents. Unmetabolised antidiabetics or some of their transformation products retain their pharmacological activity,...
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Determination of Glycerol, Propylene Glycol, and Nicotine as the Main Components in Refill Liquids for Electronic Cigarettes
PublikacjaRefill liquids for electronic cigarettes are an important area of research due to the health safety and quality control of such products. A method was developed for the determination of glycerol, propylene glycol, and nicotine in refill liquids using liquid chromatography, coupled with tandem mass spectrometry (LC-MS/MS) in multiple reaction monitoring (MRM) mode with electrospray ionisation (ESI). Sample preparation was based...
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The content of biogenic amines in Rondo and Zweigelt wines and correlations between selected wine parameters
PublikacjaThe purpose of this study was to evaluate the content of biogenic amines (BAs) in wines using dispersive liquid–liquid microextraction–gas chromatography–mass spectrometry (DLLME-GC–MS). An additional objective was to assess the correlations between selected parameters characterizing the samples such as the content of BAs, sugars, and organic acids, pH, and total acidity. Wines produced from the same grape variety in which alcoholic...
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Comparative Study on Assisted Solvent Extraction Techniques for the Extraction of Biologically Active Compounds from Sideritis raeseri and Sideritis scardica
PublikacjaThe plants in the Sideritis genus are postulated to exhibit several important medicinal properties due to their unique chemical composition. To isolate the targeted phytochemical compounds, the selection of a suitable extraction method is of primary importance. In this work, a comparative study on the phytochemical profiles of various Sideritis raeseri and Sideritis scardica extracts has been carried out. An untargeted metabolomics...
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A comprehensive lipidomic analysis of oilseeds using LC-Q-TOF-MS and dispersive micro-solid phase (D-μ-SPE) extraction techniques
PublikacjaGrowing public health awareness increased the demand for natural products with positive health benefits. Vegetable oils containing omega-3 fatty acids (FA) such as alpha-linolenic acid (ALA) has been proposed as a possible source of eicosapentaenoic acid (EPA) and docosahexaenoic acid (DHA). In this work, a comprehensive lipidome analysis and comparison of seven oilseeds, including flaxseed, chia, hemp, black cumin, white sesame,...
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Searching for the primary metabolic alterations of polycystic ovary syndrome by application of the untargeted metabolomics approach
PublikacjaDespite a large number of studies, the pathogenesis of polycystic ovary syndrome (PCOS) still remains unexplained. In light of ambiguous observations reported in metabolomics, there is a need to carry out studies focusing on confirming the discriminating power of the proposed metabolomics biomarkers. Our research aimed to perform a validation study of metabolites detected in our previous study from serum samples, on the new set...
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Density, sound velocity, viscosity, and refractive index of new morpholinium ionic liquids with amino acid-based anions: Effect of temperature, alkyl chain length, and anion
PublikacjaIn this work, room temperature synthesis of twenty new ionic liquids (ILs) based on the N-alkyl-N-methylmorpholinium ([Mor1,R], R = 2, 3, 4, 6, 8) cation and N-acetyl-L-amino acid anions (L-alaninate, L-valinate, L-leucinate, L-isoleucinate) was described. The synthesized ILs were characterized by various spectroscopic techniques and high-resolution mass spectrometry. Furthermore, density (ρ), sound velocity (v), viscosity (η)...
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Presence of antibiotics in the aquatic environment in Europe and their analytical monitoring: Recent trends and perspectives
PublikacjaThe presence of antibiotics and their metabolites in the aquatic environment exerts a negative impact on all organisms. Moreover, the easy migration of these substances to drinking water may also have serious consequences for public health, such as drug resistance. Although antibiotics and their metabolites are detected in surface waters and wastewater, there are still no systemic solutions preventing environmental pollution with...
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Influence of Storage Time and Temperature on the Toxicity, Endocrine Potential, and Migration of Epoxy Resin Precursors in Extracts of Food Packaging Materials
PublikacjaThe aim of the present study was to establish a standard methodology for the extraction of epoxy resin precursors from several types of food packages (cans, multi-layered composite material, and cups) with selected simulation media (distilled water, 5% ethanol, 3% dimethyl sulfoxide, 5% acetic acid, artificial saliva) at different extraction times and temperatures (factors). Biological analyses were conducted to determine the acute...
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Exhaled breath analysis by resistive gas sensors
PublikacjaBreath analysis has attracted human beings for centuries. It was one of the simplest methods to detect various diseases by using human smell sense only. Advances in technology enable to use more reliable and standardized methods, based on different gas sensing systems. Breath analysis requires the detection of volatile organic compounds (VOCs) of the concentrations below individual ppm (parts per million). Therefore, advanced detection...
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UV-induced electron transfer between triethylamine and 5-bromo-2′-deoxyuridine. A puzzle concerning the photochemical debromination of labeled DNA
Publikacja5-Bromo-2'-deoxyuridine (BrdU) photosensitizes DNA to strand break formation. However, this type of photodamage is completely quenched by the presence of triethylamine (TEA) which originates from RP-HPLC purification commonly employed by oligonucleotide providers. While the presence of TEA in oligonucleotide samples does not interfere with PCR or other molecular biology applications, the mechanism of photochemical reaction proceeding...
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Untargeted Lipidomics Reveals Differences in the Lipid Pattern among Clinical Isolates of Staphylococcus aureus Resistant and Sensitive to Antibiotics
PublikacjaStaphylococcus aureus resistance to antibiotics is a significant clinical problem worldwide. In this study, an untargeted lipidomics approach was used to compare the lipid fingerprints of S. aureus clinical isolates that are resistant and sensitive to antibiotics. High-performance liquid chromatography coupled with time-of-flight mass spectrometry was employed to rapidly and comprehensively analyze bacterial lipids. Chemometric...
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The potential of LC–MS technique in direct analysis of perfume content
PublikacjaPerfumes are products that consist of a wide range of natural and synthetic compounds. Due to complex composition, the determination of their ingredients is a difficult task. Most of the perfume components are either volatile or semi-volatile; however, most of the attention has been paid to volatile ones, and thus, gas chromatography or electronic noses are generally used. Nevertheless, in this study, liquid chromatography coupled...
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Anticancer and antimicrobial properties of novel η6-p-cymene ruthenium(ii) complexes containing a N,S-type ligand, their structural and theoretical characterization
PublikacjaRuthenium(II) complexes are lately of great scientific interest due to their chemotherapeutic potential asanticancer and antimicrobial agents. Here we present the synthesis of new pyrazole carbothioamidederivatives and their four arene–ruthenium complexes. The title compounds were characterized with theapplication of IR, NMR, mass spectrometry, elemental analysis and X-ray diffraction. Additionally, for newcomplexes DFT calculations...
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In-tube extraction for the determination of the main volatile compounds in Physalis peruviana L
PublikacjaAn analytical procedure based on in-tube extraction followed by gas chromatography with mass spectrometry has been developed for the analysis of 24 main volatile components in cape gooseberry (Physalis peruviana L.) samples. According to their chemical structure, the compounds were organized into different groups: one hydrocarbon, one aldehyde, four alcohols, four esters, and 14 monoterpenes. By single-factor experiments, incubation...
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Elucidation of transformation pathway of ketoprofen, ibuprofen, and furosemide in surface water and their occurrence in the aqueous environment using UHPLC-QTOF-MS
PublikacjaThe identification and determination of transformation products (TPs) of pharmaceuticals is essential nowadays, in order to track their fate in the aqueous environment and, thus, to estimate the actual pollution. However, this is a challenging task due to the necessity to apply high-resolution instruments enable to detect known and unknown compounds. This work presents the use of liquid chromatography quadrupole time-of-flight...
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Chemiluminogenic acridinium salts: A comparison study. Detection of intermediate entities appearing upon light generation
PublikacjaThe nine derivatives of acridine-9-carboxylic acid (CMADs) capable for chemiluminescence (CL), representing various classes of compounds were isolated in a chemically pure state (assessed by RP-HPLC) and identified using high resolution mass spectrometry (ESI-QTOF) and magnetic resonance (1H NMR) techniques. Among them are aryl acridinium esters, containing certainly selected and located substituents in both aromatic systems, an...
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Analytical data on molecular umbrella: cispentacin and molecular umbrella: fluorescent probe conjugates
Dane BadawczeAnalytical data (NMR, MS, FTIR) for nine conjugates of molecular umbrella with cispentacin, Lys(Mca) or Nap-NH2. The conjugates have been rationally designed as potential antifungal agents. 1H NMR and 13C NMR spectra were obtained at 500 MHz Varian Unity Plus spectrometer and the deuterated solvents were used as internal locks. High-resolution mass...
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Temperature influence on tire/road noise evaluated by the drum method
PublikacjaAmbient air and road surface temperatures substantially affect the road vehicle noise emission. The temperature influence on tire/road noise depends mainly on tire-road combination. It is different for dense and porous pavements, for bituminous and cement ones. It differs also depending on tires. The correction procedures for temperature effect are still under consideration and preparation. Laboratory experiment was prepared to...
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Assessment of baby disposable diapers application for urine collection and determination of phthalate metabolites
PublikacjaThe baby disposable diapers were investigated as a sampling material for urine collection and validated for the evaluation of the exposure of children to xenobiotics. Phthalate metabolites detected in urine samples were chosen as proof-of-concept analytes. For the determination of phthalate metabolites in children’s urine samples, high performance liquid chromatography coupled with tandem mass spectrometry (HPLC-MS/MS) was used. Two...
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The Interaction of Heptakis (2,6-di-O-Methyl)-β-Cyclodextrin with Mianserin Hydrochloride and Its Influence on the Drug Toxicity
PublikacjaOne tetracyclic antidepressant, mianserin hydrochloride (MIA), has quite significant side effects on a patients’ health. Cyclodextrins, which are most commonly used to reduce the undesirable features of contained drugs within their hydrophobic interior, also have the potential to alter the toxic behavior of the drug. The present paper contains investigations and the characteristics of interaction mechanisms for MIA and the heptakis...