Miniaturized, green salting-out liquid–liquid microextraction coupled with GC–MS used to evaluate biogenic amines in wine samples - Publication - Bridge of Knowledge

Your account

login

Search

Miniaturized, green salting-out liquid–liquid microextraction coupled with GC–MS used to evaluate biogenic amines in wine samples

Abstract

Monitoring of the biogenic amines (BAs) content in food products, including wine, is important due to the health and safety of consumers and from the quality control point of view. In a given study, simultaneous derivatization and salting-out liquid–liquid microextraction (SALLME) coupled with GC–MS for BAs determination from wine samples was developed. For the optimization the Box-Behnken design was applied, where three independent factors were evaluated: the amount of NaCl, amount of EtAc and vortexing time. The proposed approach is characterized by good sensitivity expressed in the detection limit between 1.5 and 8.1 µg/L, good recovery on the level 84 – 106% and good reproducibility, it is fast (20 min) and easy to perform. Moreover, the BAs index (BAI) was applied in order to assess the quality of examined wines. BAI value for most of wine samples were below 2 mg/L what indicates that selected wines were of high quality.

Citations

  • 9

    CrossRef

  • 0

    Web of Science

  • 9

    Scopus

Authors (4)

Cite as

Full text

download paper
downloaded 24 times
Publication version
Accepted or Published Version
DOI:
Digital Object Identifier (open in new tab) 10.1016/j.microc.2022.107616
License
Creative Commons: CC-BY open in new tab

Keywords

Details

Category:
Articles
Type:
artykuły w czasopismach
Published in:
MICROCHEMICAL JOURNAL no. 180,
ISSN: 0026-265X
Language:
English
Publication year:
2022
Bibliographic description:
Fabjanowicz M., Różańska A., Kalinowska K., Płotka-Wasylka J.: Miniaturized, green salting-out liquid–liquid microextraction coupled with GC–MS used to evaluate biogenic amines in wine samples// MICROCHEMICAL JOURNAL -Vol. 180, (2022), s.107616-
DOI:
Digital Object Identifier (open in new tab) 10.1016/j.microc.2022.107616
Sources of funding:
  • COST_FREE
Verified by:
Gdańsk University of Technology

seen 70 times

Recommended for you

Green, simple analytical method for biogenic amines determination in fruit juice samples using salting-out assisted liquid-liquid microextraction and gas chromatography-mass spectrometry

2022

The content of biogenic amines in Rondo and Zweigelt wines and correlations between selected wine parameters

2022

Novel analytical method for detection of orange juice adulteration based on ultra-fast gas chromatography

2018

Analytical methodologies for determination of artificial sweeteners in foodstuffs- a review

2009
Meta Tags