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Search results for: isotope%20analysis
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Isotope-labeled substances in analysis of persistent organicpollutants in environmental samples
PublicationUltratrace analysis of persistent organic pollutants (POPs) in environmental samples requires very sophisticated methods for both sample preparation and instrumental analysis. The complex matrix requires a multi-stage procedure. Each stage is a potential source of error, as a consequence of which the final result of analysis could be a source of misinformation rather than information. The individual stages and the procedure as...
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Carbon isotope effect in superconductingMgCNi3
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Electronic and nuclear properties from the analysis of the isotope shifts in the spectral lines of lead
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Isotope shifts in the spectrum of Pb I
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Carbon isotope effect in superconducting MgCNi_3
PublicationPodstawienie izotopu węgla 13C w związku MgCNi_3 obniża temperaturę przejścia nadprzewodzącego o 300mK. Wyliczony na tej podstawie wspolczynnik izotopowy alfa(C) wynosi 0.54, co silnie potwierdza fononowy charakter nadprzewodnictwa.
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Electronic and nuclear properties from the analysis of the isotope shifts in the spectral lines of lead [online]
PublicationW pracy dokonano analizy 24 linii widmowych atomu i jonu ołowiu, przy użyciu metody diagramów Kinga. Połączenie danych pomiarowych otrzymanych z badań fizyki jądrowej z danymi spektroskopii optycznej pozwoliło na analizę przesunięć izotopowych linii widmowych niezależnie od modelu teoretycznego. W wyniku czego, rozdzielono efekt masy od efektu objętościowego i otrzymano szereg danych spektroskopowych stanowiących bogatą bazę doświadczalną...
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Atomic substitution and carbon isotope effect in superconducting MgCNi3
PublicationW pracy analizowany jest wpływ domieszkowania zarówno pozycji niklu, jak i węgla w nadprzewodzącym związku międzymetalicznym MgCNi3. Dodatkowo dyskutowany jest węglowy nadprzewodzący efekt izotopowy.
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Hyperfine structure and isotope shift study in singly ionized lead
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Isotope shifts of multipole lines of Pb I and Pb II
PublicationStudies of isotope shifts of three multipole lines between levels of the ground configuration 6s26p2 of Pb I, i.e.: 461.9 nm(1S0→3P1), 531.5 nm(1S0→3P2) and 733.2 nm(1D2→3P1), as well as 710.2 nm line (6s26p2P3∕2→6s26p2P1∕2) of Pb II are presented. We determined the isotope shifts between four stable isotopes: 204, 206, 207, 208. By the use of King plot analysis we were able to separate the mass and the field shifts. We found that...
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Problems of PAH quantification by GC–MS method using isotope-labelled standards
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Problems of PAH quantification by GC-MS method using isotope-labelled standards.
PublicationChromatografia gazowa w połączeniu ze spektromerią mas (GC-MS) jest obecnie rutynowo stosowaną metodą w analityce środowiskowej do oznaczania śladowych ilości zanieczyszczeń organicznych. Stosowanie detektora mas sprawia, że wygodnym wzorcem wewnętrznym są stabilne izotopowo analogi oznaczanych związków. Związki te są wykorzystywane do śledzenia i kompensacji strat analitów podczas wykonywania określonych operacji związanych z...
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ISOTOPES IN ENVIRONMENTAL AND HEALTH STUDIES
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Hyperfine structure and isotope shifts in 733.2 nm mixed forbidden line of Pb I
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Isotope shift study in two visible lines: 500.6 nm and 520.3 nm of Pb I
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ENGINEERING FAILURE ANALYSIS
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Comparison of different techniques for extracting Polychlorinated Biphenyls from bottom sediment samples using Isotope Dilution Mass Spectrometry
PublicationIn this work, problems that may occur during determination of trace levels of polychlorinated biphenyls in sediment samples are described. The main error sources are connected with extraction of analytes prior to final determination. During model studies, polychlorinated biphenyls have been extracted from sediment reference material (METRANAL 2) with the use of different solvents (dichloromethane, hexane, and toluene); the process...
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Determination of PCBs in marine sediment using pressurised liquid extraction-gas chromatography-isotope dilution mass spectrometry -method validation
PublicationOpracowano procedurę oznaczania wybranych analitów z grupy PCB w próbkach osadu dennego z wykorzystaniem techniki przyspieszonej ekstrakcji za pomocą rozpuszczalnika (PLE) w połączeniu z chromatografią gazową z detektorem spektrometrii mas. Opracowana procedura analityczna została wykorzystana do analizy próbek morskiego osadu dennego, które stanowiły przedmiot badań międzylaboratoryjnych organizowanych przez Comité Consultatif...
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Investigating the biochar effects on C‐mineralization and sequestration of carbon in soil compared with conventional amendments using the stable isotope (δ13C) approach
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A comprehensive review of biogeochemical distribution and fractionation of lead isotopes for source tracing in distinct interactive environmental compartments
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Quantification of key red blood cell folates from subjects with defined MTHFR 677C>T genotypes using stable isotope dilution liquid chromatography/mass spectrometry
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Determination of tributyltin (TBT) in marine sediment using pressurised liquid extraction–gas chromatography–isotope dilution mass spectrometry (PLE–GC–IDMS) with a hexane–tropolone mixture
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Determination of tributylotin (TBT) in marine sediment using pressurised liquid extraction-gas chromatography-isotope dilution mass spectrometry (PLE-GC-IDMS) with a hexane-tropolone mixture
PublicationOpracowano metodę oznaczania zawartości tributylocyny w próbkach osadu morskiego. Na etapie izolacji zastosowano technikę przyspieszonej ekstrakcji za pomocą roztworu tropolonu w heksanie.Na etapie oznaczeń końcowych wykorzystano technikę chromatografii gazowej, stosując metodę spektrometrii mas rozcieńczenia izotopowego. Wyznaczono parametry walidacyjne opracowanej metody: granicę wykrywalności, precyzję, poprawność i niepewność.
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Analysis
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APPLIED RADIATION AND ISOTOPES
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The Metal-Free Regioselective Deuteration of 2-Methylquinolin-8-ol and 2,5-Dimethylquinolin-8-ol, Spectroscopic and Computational Studies
PublicationAbstract: Aim and Background: Introducing deuterium to a molecule is of interest to a wide variety of research, including investigation of reaction mechanisms or kinetics, analysis of drug metabolism, structural elucidation of molecules, and syntheses of isotopically labeled materials used for NMR spectroscopy and medicinal research. Objective: The transition-metal-free regioselective deuteration of 2-methylquinolin-8-ol...
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PHYTOCHEMICAL ANALYSIS
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Identification of the featured-element in fine road dust of cities with coal contamination by geochemical investigation and isotopic monitoring
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15th Conference on Calorimetry and Thermal Analysis
EventsThe 15th Conference on Calorimetry and Thermal Analysis (CCTA 15) is the successive one in the cycle events coorganized by the Polish Society of Calorimetry and Thermal Analysis (PTKAT) this time Faculty of Chemistry of Gdańsk University of Technology and Stanislaw Staszic Research Association . The conference is devoted to application...
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Measurement report: Spatial variations in ionic chemistry and water-stable isotopes in the snowpack on glaciers across Svalbard during the 2015–2016 snow accumulation season
PublicationThe Svalbard archipelago, located at the Arctic sea-ice edge between 74 and 81∘ N, is ∼60 % covered by glaciers. The region experiences rapid variations in atmospheric flow during the snow season (from late September to May) and can be affected by air advected from both lower and higher latitudes, which likely impact the chemical composition of snowfall. While long-term changes in Svalbard snow chemistry have been documented in...
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Accurate, Direct, and High-Throughput Analyses of a Broad Spectrum of Endogenously Generated DNA Base Modifications with Isotope-Dilution Two-Dimensional Ultraperformance Liquid Chromatography with Tandem Mass Spectrometry: Possible Clinical Implication
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The effects of urban vehicle traffic on heavy metal contamination in road sweeping waste and bottom sediments of retention tanks
PublicationDiffuse pollution formed during a surface runoff on paved surfaces is a source of heavy metals (HMs) of various origin. This research study indicates the connection between bottom sediments of retention tanks located on urban streams and road sweeping wastes (RSW) that migrate during surface runoff to the stormwater drainage systems with discharge to the retention tanks. Moreover, we test the primary sources of HMs in RSW by analysing...
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Music Analysis
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Decision Analysis
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Landform Analysis
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ASYMPTOTIC ANALYSIS
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Linguistic Analysis
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Bayesian Analysis
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Analysis (Germany)
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Strategic Analysis
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GEOGRAPHICAL ANALYSIS
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Discrete Analysis
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Analysis and Metaphysics
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Tourism Analysis
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Analysis & PDE
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POLITICAL ANALYSIS
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RISK ANALYSIS
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Analysis and Applications
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Analysis Mathematica
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Journal of Analysis
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Carbon fractionation and stable carbon isotopic fingerprint of road dusts near coal power plant with emphases on coal-related source apportionment
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