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Search results for: ANALYTICAL NOTATION
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pH/Organic Solvent Double-Gradient Reversed-Phase HPLC
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Influence of pH on Retention in Linear Organic Modifier Gradient RP HPLC
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Comparison of High Performance Liquid Chromatography Methods with Different Detectors for Determination of Steroid Hormones in Aqueous Matrices
PublicationThis paper presents the development and comparison of procedures for the qualitative and quantitative determination of five estrogenic compounds (17-a-ethynylestradiol, estrone, estradiol, estriol, and progesterone) in drinking water and wastewater samples. Five extraction columns and two disks were tested for their efficiency. The C18 columns were superior on the basis of cost for solid phase extraction of drinking water or sewage....
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Determination of parent and methylated polycyclic aromatic hydrocarbons in water samples by dispersive liquid–liquid microextraction–two dimensional gas chromatography–time-of-flight mass spectrometry
PublicationPolycyclic aromatic hydrocarbons (PAHs) are contaminants frequently found in environmental waters. Owing to their toxic effects, it is important to develop analytical methodologies that allow their fast and reliable determination. Dispersive liquid–liquid microextraction (DLLME) allows a quick extraction of analytes with little organic solvent consumption. The best results regarding sample preparation are obtained when 40 mL of...
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Membrane Solid Phase Microextraction - a new concept of sorbent preparation
PublicationOpracowano nowy układ sorpcyjny do izolacji i/lub wzbogacania polarnych analitów organicznych z próbek wody z zastosowaniem techniki solid phase microextraction (SPME). Układ bazuje na oddzieleniu sorbentu polarnego od próbki za pomocą membrany hydrofobowej. Próbnik membrane-SPME (M-SPME) sporządzono z zastosowaniem polietylenoglikolu (PEG)o masie cząsteczkowej 20 kDa. Polimer ten jest rozpuszczalny w wodzie i w typowych warunkach...
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Nuclear Activation Methods in the Estimation of Environmental Pollution and the Assessment of the Industrial Plant Impact on the Citizens of Gdansk (Poland)
PublicationNeutronowa Analiza Aktywacyjna została wykorzystana do oceny stanu jakości powietrza atmosferycznego na podstawie badań analitycznych stopnia kumulacji zanieczyszczeń nieorganicznych w mchu torfowca, a także składu wód opadowych. Ponadto przedstawiono wyniki badań dotyczących szacowania ryzyka zawodowego pracowników zakładów przemysłowych na podstawie analizy próbek materiału biologicznego pobranego od osób narażonych.
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Comparison of different extraction techniques of polychlorinated biphenyls from sediments samples.
PublicationIn this work, problems that may occur during determination of trace levels of polychlorinated biphenyls in sediment samples are described. Main error sources are connected with extraction of analytes prior to final determination. During model studies, polychlorinated biphenyls have been extracted from sedimentreference material (METRANAL 2) with the use of different solvents (dichloromethane, hexsane, and toluene); the process...
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Ultrasensitive internally quenched substrates of human cathepsin L
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Design and synthesis of new substrates of HtrA2 protease
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Novel internally quenched substrate of the trypsin-like subunit of 20S eukaryotic proteasome
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Development of sensitive cathepsin G fluorogenic substrate using combinatorial chemistry methods
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Three Wavelength Substrate System of Neutrophil Serine Proteinases
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Highly Specific Substrates of Proteinase 3 Containing 3-(2-Benzoxazol-5-yl)-l-alanine and Their Application for Detection of This Enzyme in Human Serum
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Design of selective substrates of proteinase 3 using combinatorial chemistry methods
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Surface plasmon resonance imaging biosensor for cathepsin G based on a potent inhibitor: Development and applications
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The new fluorogenic substrates of neutrophil proteinase 3 optimized in prime site region
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A new proteinase 3 substrate with improved selectivity over human neutrophil elastase
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Do we need a catalyst in the determination of dissolved organic carbon in environmental samples?
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Quantitative structure–retention relationships of ionic liquid cations in characterization of stationary phases for HPLC
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Different detection and stacking techniques in capillary electrophoresis for metabolomics
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Chemically Bonded Silica Stationary Phases: Synthesis, Physicochemical Characterization, and Molecular Mechanism of Reversed-Phase HPLC Retention
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Picomolar analysis of flavins in biological samples by dynamic pH junction-sweeping capillary electrophoresis with laser-induced fluorescence detection
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Sample Concentration of Charged Small Molecules and Peptides in Capillary Electrophoresis by Micelle to Cyclodextrin Stacking
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Solid-Phase Microextraction for the Determination of Inorganic Ions: Applications and Possibilities
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The simultaneous detection of food dyes from different samples in a 96-well plate by spectrophotometry
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Application of an iron-based porphyrinic metal–organic framework for removal of warfarin from aqueous solutions
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Rapid and sensitive determination of acrylamide in potato crisps using reversed-phase direct immersion single drop microextraction-gas chromatography
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Recent developments in the determination of residual solvents in pharmaceutical products by microextraction methods
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Determination of nicotine in saliva, urine and wastewater samples using tantalum metal organic framework pipette tip micro-solid phase extraction
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Salt saturated single-drop microextraction of malondialdehyde from human plasma before its determination by gas chromatography
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Molecularly imprinted stir bar sorptive extraction coupled with atomic absorption spectrometry for trace analysis of copper in drinking water samples
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Developing a New Micro Cloud Point Extraction Method for Simultaneous Preconcentration and Spectrophotometric Determination of Uranium and Vanadium in Brine
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Simultaneous Removal of Heavy Metals from Wastewater Using Modified Sodium Montmorillonite Nanoclay
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Statistical theory of component overlap in multicomponent chromatograms
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Porous, High Capacity Coatings for Solid Phase Microextraction by Sputtering
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Room temperature ionic liquid-based dispersive liquid–liquid microextraction of uranium in water samples before spectrophotometric determination
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Headspace Solvent Microextraction
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Extraction of mass spectra free of background and neighboring component contributions from gas chromatography/mass spectrometry data
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Molecularly Imprinted Polymers for Stir Bar Sorptive Extraction: Synthesis, Characterization, and Application
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Miniaturization and Automation of an Internally Cooled Coated Fiber Device
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Headspace Liquid-Phase Microextraction of Chlorobenzenes in Soil with Gas Chromatography-Electron Capture Detection
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Determination of mefenamic acid in urine and pharmaceutical samples by HPLC after pipette-tip solid phase microextraction using zinc sulfide modified carbon nanotubes
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Determination of (S)-warfarin using an activated screen printed gold electrode modified with gold nanoparticles and an enantioselective molecularly imprinted polymer
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Application of Box–Behnken design in the optimization of a simple graphene oxide/zinc oxide nanocomposite-based pipette tip micro-solid phase extraction for the determination of Rhodamine B and Malachite green in seawater samples by spectrophotometry
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In-Tube Molecularly Imprinted Polymer Solid-Phase Microextraction for the Selective Determination of Propranolol
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Rapid and sensitive determination of fluoride in toothpaste and water samples using headspace single drop microextraction-gas chromatography
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Potential Aluminium(III)- and Gallium(III)-selective Optical Sensors Based on Porphyrazines
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Application of single drop extraxtion (SDE) gas chromatography method for the determination of carbonyl compounds in spirits and vodkas
PublicationW pracy przedstawiono metodę oznaczania związków karbonylowych w spirytusach i wódkach, wykorzystującą do izolacji i wzbogacania technikę mikroekstrakcji do pojedynczej kropli (SDE)po derywatyzacji analitów O-(2,3,4,5,6-pentafluorobenzylo)hydroksylaminą. Określono optymalne parametry izolacji i wzbogacania aldehydów z roztworów alkoholowych (objętość próbki, objętość kropli, zawartość alkoholu, temperaturę i czas ekstrakcji)....
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Critical factors for the performance of chip array-based electrical detection of DNA for analysis of pathogenic bacteria
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Detection of DNA Replication Intermediates after Two-Dimensional Agarose Gel Electrophoresis Using a Fluorescein-Labeled Probe
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