Method for the determination of carboxylic acids in industrial effluents using dispersive liquid-liquid microextraction with injection port derivatization gas chromatography–mass spectrometry - Publikacja - MOST Wiedzy

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Method for the determination of carboxylic acids in industrial effluents using dispersive liquid-liquid microextraction with injection port derivatization gas chromatography–mass spectrometry

Abstrakt

The paper presents a new method for the determination of 15 carboxylic acids in samples of postoxidative effluents from the production of petroleum bitumens using ion-pair dispersive liquid-liquid microextraction and gas chromatography coupled to mass spectrometry with injection port derivatization. Several parameters related to the extraction and derivatization efficiency were optimized. Under optimized experimental conditions,the obtained limit of detection and quantification ranged from 0.0069 to 1.12 ug/mL and 0.014 to 2.24 ug/mL, respectively. The precision (RSD ranged 1.29–6.42%) and recovery (69.43–125.79%) were satisfactory. Nine carboxylic acids at concentrations ranging from 0.10 ug/mL to 15.06 ug/mL were determined in the raw wastewater and in samples of effluents treated by various oxidation methods. The studies revealed a substantial increase of concentration of benzoic acids, in samples of wastewater after treatment, which confirms the need of carboxylic acids monitoring during industrial effluent treatment processes.

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Kategoria:
Publikacja w czasopiśmie
Typ:
artykuł w czasopiśmie wyróżnionym w JCR
Opublikowano w:
JOURNAL OF CHROMATOGRAPHY A nr 1517, strony 26 - 34,
ISSN: 0021-9673
Język:
angielski
Rok wydania:
2017
Opis bibliograficzny:
Makoś P., Fernandes A., Boczkaj G.: Method for the determination of carboxylic acids in industrial effluents using dispersive liquid-liquid microextraction with injection port derivatization gas chromatography–mass spectrometry// JOURNAL OF CHROMATOGRAPHY A. -Vol. 1517, (2017), s.26-34
DOI:
Cyfrowy identyfikator dokumentu elektronicznego (otwiera się w nowej karcie) 10.1016/j.chroma.2017.08.045
Bibliografia: test
  1. A. Latorre, A. Rigol, S. Lacorte, D. Barcelo, Comparison of gas chromatography-mass spectrometry and liquid chromatography-mass spectrometry for the determination of fatty and resin acids in paper mill process waters, J. Chromatogr. A 991 (2003) 205-215. otwiera się w nowej karcie
  2. A. Behvandi, A.A. Safekordi, F. Khorasheh, Removal of benzoic acid from industrial wastewater using metal organic frameworks: equilibrium, kinetic and thermodynamic study, J. Porous Mater. 24 (2017) 165-178. otwiera się w nowej karcie
  3. J. Wu, H.K. Lee, Ion-pair dynamic liquid-phase microextraction combined with injection-port derivatization for the determination of long-chain fatty acids in water samples, J. Chromatogr. A 1133 (2006) 13-20. otwiera się w nowej karcie
  4. M. Abalos, J.M. Bayona, J. Pawliszyn, Development of a headspace solid-phase microextraction procedure for the determination of free volatile fatty acids in waste waters, J. Chromatogr. A 873 (2000) 107-115. otwiera się w nowej karcie
  5. A. Banel, M. Wasielewska, B. Zygmunt, Application of headspace solid-phase microextraction followed by gas chromatography-mass spectrometry to determine short-chain alkane monocarboxylic acids in aqueous samples, Anal. Bioanal. Chem. 399 (2011) 3299-3303. otwiera się w nowej karcie
  6. P.S.C. Schulze, C.F.M. Carvalho, H. Pereira, K.N. Gangadhar, L.M. Schüler, T.F. Santos, J.C.S. Varela, L. Barreira, Urban wastewater treatment by Tetraselmis sp. CTP4 (Chlorophyta), Bioresour. Technol. 223 (2017) 175-183. otwiera się w nowej karcie
  7. K. Chai, H. Ji, Dual functional adsorption of benzoic acid from wastewater by biological-based chitosan grafted b-cyclodextrin, Chem. Eng. J. 203 (2012) 309-318. otwiera się w nowej karcie
  8. R. Thiruvenkatachari, T.O. Kwon, I.S. Moon, Degradation of phthalic acids and benzoic acid from terephthalic acid wastewater by advanced oxidation processes, J. Environ. Sci. Health A Toxic Hazard. Subst. Environ. Eng. 41 (2006) 1685-1697. otwiera się w nowej karcie
  9. G. Boczkaj, A. Fernandes, Wastewater treatment by means of advanced oxidation processes at basic pH conditions: a review, Chem. Eng. J. 320 (2017) 608-633. otwiera się w nowej karcie
  10. N.T. Mkhize, T.A.M. Msagati, B.B. Mamba, M. Momba, Determination of volatile fatty acids in wastewater by solvent extraction and gas chromatography, Phys. Chem. Earth 67-69 (2014) 86-92. otwiera się w nowej karcie
  11. A.C. Moura de Sena Aquino, M.S. Azevedo, D.H.B. Ribeiro, A.C.O. Costa, E.R. Amante, Validation of HPLC and CE methods for determination of organic acids in sour cassava starch wastewater, Food Chem. 172 (2015) 725-730. otwiera się w nowej karcie
  12. A.T. James, A.J.P. Martin, Gas-liquid partition chromatography: the separation and micro-estimation of volatile fatty acids from formic acid to dodecanoic acid, Biochem. J. 50 (1952) 679-690. otwiera się w nowej karcie
  13. W. Ziemer, M. Wortberg, C. Eichberger, J. Gerstel, W. Kerl, Direct aqueous injection with backflush thermal desorption for wastewater monitoring by online GC-MS, Anal. Bioanal. Chem. 397 (2010) 1315-1324. otwiera się w nowej karcie
  14. M.A. Ullah, K.-H. Kim, J.E. Szulejko, J. Cho, The gas chromatographic determination of volatile fatty acids in wastewater samples: evaluation of experimental biases in direct injection method against thermal desorption method, Anal. Chim. Acta 820 (2014) 159-167. otwiera się w nowej karcie
  15. A. Latorre, A. Rigol, S. Lacorte, D. Barcelo, Comparison of gas chromatography-mass spectrometry and liquid chromatography-mass spectrometry for the determination of fatty and resin acids in paper mill process waters, J. Chromatogr. A 991 (2003) 205-215. otwiera się w nowej karcie
  16. N. Li, C. Deng, X. Zhang, Determination of methylmalonic acid and glutaric acid in urine by aqueous-phase derivatization followed by headspace solid-phase microextraction and gas chromatography-mass spectrometry, J. Sep. Sci. 30 (2007) 266-271. otwiera się w nowej karcie
  17. F. Ngan, T. Ikesaki, Determination of nine acidic herbicides in water and soil by gas chromatograpy using an electron-capture detector, J. Chromatogr. A 537 (1991) 385-395. otwiera się w nowej karcie
  18. A.M.C. Ferreira, M.E.F. Laespada, J.L.P. Pavón, B.M. Cordero, In situ aqueous derivatization as sample preparation technique for gas chromatographic determinations, J. Chromatogr. A 1296 (2013) 70-83. otwiera się w nowej karcie
  19. P. Husek, P. Simek, Alkyl chloroformates in sample derivatization strategies for GC analysis. Review on a decade use of the reagents as esterifying agents, Curr. Pharm. Anal. 2 (2006) 23-43. otwiera się w nowej karcie
  20. Y. Sun, X. Wang, Y. Huang, Z. Pan, L. Wang, Derivatization following hollow-fiber microextraction with tetramethylammonium acetate as a dual-function reagent for the determination of benzoic acid and sorbic acid by GC, J. Sep. Sci. 36 (2013) 2268-2276. otwiera się w nowej karcie
  21. A. Banel, B. Zygmunt, Application of gas chromatography-mass spectrometry preceded by solvent extraction to determine volatile fatty acids in wastewater of municipal, animal farm and landfill origin, Water Sci. Technol. 63 (2011) 590-597. otwiera się w nowej karcie
  22. Á. Sebok, A. Vasanits-Zsigrai, A. Helenkár, Gy. Záray, I. Molnár-Perl, Multiresidue analysis of pollutants as their trimethylsilyl derivatives, by gas chromatography-mass spectrometry, J. Chromatogr. A 1216 (2009) 2288-2301. otwiera się w nowej karcie
  23. L. Feng, Y. Huang, H. Wang, Solid-phase microextraction in combination with GC-FID for quantification of the volatile free fatty acids in wastewater from constructed wetlands, J. Chromatogr. Sci. 46 (2008) 577-584. otwiera się w nowej karcie
  24. M. Rezaee, Y. Assadi, M.-R.M. Hosseini, E. Aghaee, F. Ahmadi, S. Berijani, Determination of organic compounds in water using dispersive liquid-liquid microextraction, J. Chromatogr. A 1116 (2006) 1-9. otwiera się w nowej karcie
  25. G. Boczkaj, M. Kamiński, A. Przyjazny, Process control and investigation of oxidation kinetics of postoxidative effluents using gas chromatography with pulsed flame photometric detector (GC-PFPD), Ind. Eng. Chem. Res. 49 (2010) 12654-12662. otwiera się w nowej karcie
  26. G. Boczkaj, A. Przyjazny, M. Kamiński, New procedures for control of industrial effluents treatment processes, Ind. Eng. Chem. Res. 53 (2014) 1503-1514. otwiera się w nowej karcie
  27. G. Boczkaj, A. Przyjazny, M. Kamiński, Characteristics of volatile organic compounds emission profiles from hot road bitumens, Chemosphere 107 (2014) 23-30. otwiera się w nowej karcie
  28. J. Wisniak, A. Polishuk, Analysis of residuals-a useful tool for phase equilibrium data analysis, Fluid Phase Equilibr. 164 (1999) 61-82. otwiera się w nowej karcie
  29. F.R. Mansour, N.D. Danielson, Solidification of floating organic droplet in dispersive liquid-liquid microextraction as a green analytical tool, Talanta 170 (2017) 22-35. otwiera się w nowej karcie
  30. W.-L. Liu, Y.-C. Ko, B.-H. Hwang, Z.-G. Li, T.C.-C. Yang, M.-R. Lee, Determination of perfluorocarboxylic acids in water by ion-pair dispersive liquid-liquid microextraction and gas chromatography-tandem mass spectrometry with injection port derivatization, Anal. Chim. Acta 726 (2012) 28-34. otwiera się w nowej karcie
  31. G. Boczkaj, P. Makoś, A. Przyjazny, Application of dispersive liquid-liquid microextraction and gas chromatography-mass spectrometry for the determination of oxygenated volatile organic compounds in effluents from the production of petroleum bitumen, J. Sep. Sci. 39 (2016) 2604-2615. otwiera się w nowej karcie
  32. G. Boczkaj, P. Makoś, A. Fernandes, A. Przyjazny, A new procedure for control of treatment of industrial effluents to remove volatile organosulfur compounds, J. Sep. Sci. 39 (2016) 3946-3956. otwiera się w nowej karcie
  33. G. Boczkaj, P. Makoś, A. Fernandes, A. Przyjazny, New procedure for examination of degradation of volatile organonitrogen compounds during treatment of industrial effluents, J. Sep. Sci. 40 (2017) 1301-1309. otwiera się w nowej karcie
  34. C.-L. Hsu, W.-H. Ding, Determination of low-molecular-weight dicarboxylic acids in atmospheric aerosols by injection-port derivatization and gas chromatography?mass spectrometry, Talanta 80 (2009) 1025-1028. otwiera się w nowej karcie
  35. J. Wu, H.K. Lee, Injection port derivatization following ion-pair hollow fiber-protected liquid-phase microextraction for determining acidic herbicides by gas chromatography/mass spectrometry, Anal. Chem. 78 (2006) 7292-7301. otwiera się w nowej karcie
  36. F.F. Cantwell, H. Freiser, Kinetics of ion pair extraction, Anal. Chem. 60 (1988) 226-230. otwiera się w nowej karcie
  37. E.W. Robb, J.J. Westbrook, Preparation of methyl esters for gas liquid chromatography of acids by pyrolysis of tetramethylammonium salts, Anal. Chem. 35 (1963) 1644-1647. otwiera się w nowej karcie
  38. L. Xu, M. Jiang, G. Li, Injection port derivatization following sonication-assisted ion-pair liquid-liquid extraction of nonsteroidal anti-inflammatory drugs, Anal. Chim. Acta 666 (2010) 45-50. otwiera się w nowej karcie
  39. Q. Wang, L. Ma, C. Yin, L. Xu, Developments in injection port derivatization, J. Chromatogr. A 1296 (2013) 25-35. otwiera się w nowej karcie
  40. A. Fallon, R.F.G. Booth, L.D. Bell, Laboratory Techniques in Biochemistry and Molecular Biology, Elsevier, 2009. otwiera się w nowej karcie
  41. G. Boczkaj, P. Makoś, A. Przyjazny, Application of dynamic headspace and gas chromatography coupled to mass spectrometry (DHS-GC-MS) for the determination of oxygenated volatile organic compounds in refinery effluents, Anal. Methods 8 (2016) 3570-3577. otwiera się w nowej karcie
  42. T.S.S. Rao, S. Awasthi, Oxidation of alkylaromatics, Eur. J. Chem. 4 (2007) 1-13. otwiera się w nowej karcie
Weryfikacja:
Politechnika Gdańska

wyświetlono 62 razy

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