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prof. dr hab. inż. Juliusz Orlikowski
Employment
- Vice-Dean for Cooperation and Advancement at Faculty of Chemistry
- Professor at Department of Electrochemistry, Corrosion and Materials Engineering
- Head of Department at Department of Electrochemistry, Corrosion and Materials Engineering
Publications
Filters
total: 92
Catalog Publications
Year 2024
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Badanie skuteczności ochrony katodowej Ostrogi Pilotowej w Porcie Gdynia
PublicationPrzedmiotem ekspertyzy jest ocena skuteczności ochrony katodowej palościanki Ostrogi Pilotowej w Porcie Wojennym w Gdyni Oksywiu, po pogłębieniu Kanału Portowego i zamontowaniu dodatkowych anod galwanicznych.
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Corrosion Monitoring in Petroleum Installations—Practical Analysis of the Methods
PublicationThis paper presents the most typical corrosion mechanisms occurring in the petroleum industry. The methods of corrosion monitoring are described for particular corrosion mechanisms. The field and scope of the application of given corrosion-monitoring methods are provided in detail. The main advantages and disadvantages of particular methods are highlighted. Measurement difficulties and obstacles are identified and widely discussed...
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Underwater Electrochemical Offshore Tests of a Paint Coating Applied in Water on the Legs of an Oil Production Platform
PublicationThis paper presents the methodology developed for underwater measurements using electrochemical impedance spectroscopy (EIS) technique, aimed at determining the resistance of an epoxy coating applied in seawater to the legs of an oil production platform. Performing such underwater tests in an offshore environment was technically challenging. The results of measurements obtained on the platform were confronted with comparative results...
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Wet H2S corrosion and degradation of pipeline in amine regeneration system
PublicationThe paper presents the results of NDT examinations, metallographic tests and risk assessment of degradation related to corrosion of amine regeneration unit in a desulphurisation system. Intensive corrosion resulting from acid gases environment upon water condensation causes perforation of the pipeline. Detailed analysis reveals cracking related to the mechanism of wet H2S. Hydrogen penetration, resulting from the wet H2S process,...
Year 2023
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Application of galvanodynamic impedance spectroscopy for studying passive film cracking under mechanical strain
PublicationThe paper reports the results of simultaneous mechanical and electrochemical investigations on austenitic (18/8) stainless steel in a 2 % solution of sulphuric acid. The measurements were performed using Galvanodynamic Electrochemical Impedance Spectroscopy (GDEIS). Electrochemical analysis of mechanical passive layer cracking and repassivation conditions during a tensile test was carried out. Application of this methodology allowed...
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Corrosion mechanisms in columns for atmospheric distillation of crude oil
PublicationThe paper presents the most common corrosion processes occurring in the columns for atmospheric distillation of crude oil. It describes the mechanisms leading to formation of the chemical compounds, which contribute to corrosion phenomena. The main technological factors influencing corrosion processes have been indicated. The paper also presents the interactions between particular corrosion mechanisms resulting in acceleration...
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Effect of wet Hydrogen Sulfide on Carbon Steels Degradation in Refinery Based on Case Study
PublicationMaterial degradation caused by wet hydrogen sulfide (Wet H2S) is one of the major issues in refineries. Carbon steel is the main construction material used in refineries and is subjected not only to thickness loss but the hydrogen is the major concern. H2S leads to high atomic hydrogen penetration in steel which causes degradation in the form of blistering and/or cracking (HIC/SOHIC) and stress cracking in the area of welds and...
Year 2022
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Actual field corrosion rate of offshore structures in the Baltic Sea along depth profile from water surface to sea bed
PublicationThe paper presents the results of field electrochemical investigations on the corrosion rate of carbon steel in seawater of the Baltic Sea at the location of the Baltic Beta production rig. The measurements were conducted throughout the year in seawater at different depths from the sea surface to the sea bed (about 75 m). The results revealed corrosion aggressiveness of the seawater along the entire depth profile. There was...
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Corrosion monitoring as a factor increasing the safety of hydrotechnical infrastructure
PublicationWater distribution systems at KGHM S.A. are of great importance for the efficient production of copper and environmental protection. For failures leading to perforation and leakage, the corrosion processes are responsible. This paper aims to assess corrosion on the basis of the analysis of the exposure of the Hydrotechnical Plant pipelines. To this end, the system of transfer and deposition of post-flotation waste as well as the...
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Nowy system monitoringu korozji zastosowany w zakładzie produkcyjnym PKN Orlen SA
PublicationPrzedstawiono efekty projektu badawczo-rozwojowego związanego z opracowaniem, budową oraz wdrożeniem monitoringu korozji pracującego w trybie online. Opracowana przez PKN Orlen i Politechnikę Gdańską nowa technologia łączy funkcje monitoringu intensywności korozji ogólnej oraz kruchości wodorowej. Jednoczesny pomiar online kluczowych parametrów pozwala uzyskać zdolność szybkiej oceny postępowania procesu korozji oraz reakcji na...
Year 2021
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Badania skuteczności ochrony katodowej Nabrzeża Zachodniego odcinek nr 1 (południowy) oraz Pomostu A w Porcie Gdynia
PublicationZbadano skuteczność ochrony katodowej południowego odcinka nabrzeża zachodniego oraz pomostu A w Porcie Wojennym w Gdyni. Ochrona realizowana jest za pomocą aluminiowych anod galwanicznych spawanych do ścianki szczelnej oraz pali.
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Badania skuteczności ochrony katodowej Nabrzeża Zachodniego odcinek nr 2 (północny) oraz Pirsu C w Porcie Gdynia
PublicationZbadano skuteczność ochrony katodowej północnego odcinka nabrzeża zachodniego oraz pomostu C w Porcie Wojennym w Gdyni. Ochrona realizowana jest za pomocą aluminiowych anod galwanicznych spawanych do ścianki szczelnej oraz pali.
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Investigation of the 0.4C-35Cr-45Ni-Nb Alloy after Service in High-Temperature Steam and Hydrocarbons Environment
PublicationThe paper presents the results of investigation of the 0.4C-35Cr-45Ni-Nb alloy, which operated in the cracked hydrocarbon feeds and dilution steam at 1125 C. The material originated from the pyrolytic furnace coil tubes, of which internal walls were in contact with the aforementioned medium, whereas the external walls were in contact with the flue gases. The examination included metallographic and mechanical tests on the material...
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The Effect of Increasing the Amount of Indium Alloying Material on the Efficiency of Sacrificial Aluminium Anodes
PublicationAl-Zn-In alloys having 4.2% zinc content and various indium content in the range of 0.02–0.2% were tested with respect to the most important electrochemical properties of sacrificial anodes in a cathodic protection, i.e., the current capacity and potential of the operating anode. The distribution of In and Zn in the tested alloys was mapped by means of the EDX technique, which demonstrated that these elements dissolve well in the...
Year 2020
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Corrosion hazards and inhibitor protection in the seawater injection system on the Baltic sea rig
PublicationOil extraction efficiency in LOTOS Petrobaltic Company is increased by means of injection of seawater into an oilfield aquifer, which is implemented on the Baltic Beta rig, operating on the Baltic Sea. Operational experience has shown a significant degree of corrosion aggressiveness in the injected water, which necessitates frequent repairs of the seawater injection installation. Evaluation of the corrosion phenomena is crucial...
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DETERMINATION OF THE EFFECT OF ENVIRONMENTAL FACTORS ON THE CORROSION OF WATER DISTRIBUTION SYSTEM BASED ON ANALYSIS OF ON-LINE CORROSION MONITORING RESULTS
PublicationCorrosion of water distribution system is a significant issue causing problems with quality, safety and continuity of distribution. The changes of corrosion rates of the water distribution systems in Cracow made of carbon steel were investigated by analysis of online corrosion monitoring system results. Corrosion rates were determined using the linear polarization method. The impact of rain, temperatures, conductivity, dissolved...
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Modernized cathodic protection system for legs of the production rig – Evaluation during ten years of service
PublicationThe modernization of cathodic protection system of the Baltic Beta platform legs is described. It was that the sacrificial anodes cone-shaped groups were to be placed on the seabed at a depth of 80 m. The measurements results of cathodic protection effectiveness during its ten-years operation are presented. The effectiveness was assessed based on the potential value along the entire length of the legs from the sea surface to the...
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RESEARCH ON ORGANIC COATINGS DESIGNED FOR UNDERWATER APPLICATIONS
PublicationUnderwater steel structures require periodic maintenance. In the case of vessels, anti-corrosion works are carried out in the shipyard, where very good conditions for applying organic protective coatings can be provided. Very good surface preparation can be obtained by the use of abrasive blasting. The well-prepared metal surface is free from impurities (particularly inorganic salts). Suitable conditions for the application and...
Year 2019
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Derecho Evolving from a Mesocyclone—A Study of 11 August 2017 Severe Weather Outbreak in Poland: Event Analysis and High-Resolution Simulation
PublicationThis study documents atmospheric conditions, development, and evolution of a severe weather outbreak that occurred on 11 August 2017 in Poland. The emphasis is on analyzing system morphology and highlighting the importance of a mesovortex in producing the most significant wind damages. A derecho-producing mesoscale convective system (MCS) had a remarkable intensity and was one of the most impactful convective storms in the history...
Year 2018
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Complex Corrosion Monitoring System for Crude Distillation Unit in Form of Neutral Network
PublicationComplex and successful corrosion monitoring of refinery processes can significantly reduce material losses and failure risk. The developed corrosion monitoring system is based on online ultrasonic sensors, ER (electrical resistance) probes, gravimetric method and multipoint analytical analysis of chemical composition of the fluids. Additional online LPR (linear polarization resistance) sensors controlling corrosiveness of sour...
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Development of dynamic method for evaluation of inhibition efficiency on the example of 8-hydroxyquinolin
PublicationSelection of a proper inhibitor should be based on the evaluation of its mechanism and effective concentrations. Mechanism of inhibition usually has dynamic character due to changing physicochemical conditions of the environment and corroding metal surface. Most of actually used methods are stationary or contain assumptions which highly influences obtained values. Development of new dynamic method, based on modified EIS, allows...
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Metal dusting phenomena of 501 AISI furnace tubes in refinery fractional distillation unit
PublicationThe purpose of this investigation was to conduct the failure analysis of 501 AISI furnace tubes places before distillation column in fractional distillation unit. The investigated furnace tubes were planned to work for ten years however after just two years of exploitation <30% of the material left. The observed corrosion process had the intense and complex character. The well-adhered shiny black deposits and deep, round pits were...
Year 2017
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Badania korozyjne zbiornika magazynowego kwasu chlorooctowego
PublicationWykonano ekspertyzę zbiornika magazynowego na kwas chlorooctowy. Stwierdzono, że zbiornik znajduje się w stanie pasywnym (autopasywacja zachodzi w wyniku obecności powietrza po otwarciu zbiornika). Występuje korozja ogólna zbiornika w wyniku bardzo wysokiej agresywności korozyjnej środowiska (kwasu). Procesy korozyjne występują w trakcie napełnienia zbiornika kwasem.
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Badania skuteczności ochrony katodowej nóg platformy wydobywczej
PublicationWykonano badania potencjałowe parametrów ochrony platformy wydobywczej Baltic Beta. Stwierdzono występowanie pełnej ochrony katodowej w rejonie dna. Stan techniczny anod wykazuje znaczne zużycie, jednakże w dalszym ciągu realizują proces ochorny
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Determination of pitting corrosion stage of stainless steel by galvanodynamic impedance spectroscopy
PublicationThis paper investigates the methodology for differentiation of multistep process of pitting corrosion of AISI 304 stainless steel in the environment of iron (III) chloride. Measurements were performed using Galvanodynamic Electrochemical Impedance Spectroscopy (GDEIS). Application of this methodology allowed monitoring of natural corrosion process without external current (IDC = 0A) nor potential perturbation of the system. Applied...
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Monitorowanie szybkości korozji oraz dobór materiałów konstrukcyjnych w instalacji wody morskiej platformy Baltic Beta
PublicationWykonano analizę szybkości korozji systemu monitorowania korozji z okresu od 25.11.2016 do 12.07.2017. Zdemontowano czujnik korozyjny w instalacji wody morskiej, Zainstalowani nowy czujnik z opcją pomiaru szybkości korozji metodą kuponową. Monitoringiem poddano następujące materiały: 1.7362, 1.5415, 1.0038
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Wyjaśnienie przyczyn korozji rur kotła, wytwornicy pary technologicznej instalacji Olefiny
PublicationWykonano badania przyczyn korozji rurek wytwornicy pary instalacji Olefiny. Przeprowadzono badania metalograficzne oraz SEM i EDX produktów korozji
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Wykonanie czujnika LPR oraz dobór materiałów konstrukcyjnych w instalacji wody morskiej
PublicationWykonano analizę pracy systemu monitorowania korozji, dokonano wymiany czujnika. Zamontowano nowy czujnik z opcją pomiaru kuponowego w celu doboru materiałów konstrukcyjnych do instalacji wody morskiej.
Year 2016
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Critical analysis of laboratory measurements and monitoring system of water-pipe network corrosion-case study.
PublicationCase study of corrosion failure of urban water supply system caused by environmental factors was presented. Nowadays corrosion monitoring of water distribution systems is an object of major concern. There is possibility of application broad range of techniques like gravimetric and electrochemical. Both kinds of techniques can be applied in laboratory and field conditions. In many cases researches limit the case analysis to measurements...
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Development Of Dynamic Method For Evaluation Of Corrosion Rate On The Example Of Organic Corrosion İnhibitor
PublicationMeasurements of the corrosion rate belong to the most important aspects of materials science. In order to reduce material loss corrosion inhibitors are used. However selection of proper inhibitor should be based on evaluation of its mechanism and effective concentrations. Mechanism of inhibition usually has dynamic character so physicochemical parameters are changing in time. Most of actually used methods...
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Effect of Thermal Shock During Legionella Bacteria Removal on the Corrosion Properties of Zinc-Coated Steel Pipes
PublicationThe purpose of this investigation was to conduct the failure analysis of a water-supply system made from zinc-coated steel. The observed corrosion process had an intense and complex character. The brownish deposits and perforations were present after 2-3 years of exploitation. The electrochemical study based on the Tafel polarization, corrosion potential monitoring, and electrochemical impedance spectroscopy together with microscopic...
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Electrolytic corrosion of water pipeline system in the remote distance from stray currents– case study
PublicationCase study of corrosion failure of urban water supply system caused by the harmful effects of stray currents was presented. The failure occurred at a site distant from the sources of these currents namely the tramway and railway traction systems. Diagnosis revealed the stray currents flow to pipeline over a remote distance of 800 ÷ 1,000 meters from the point of failure. At the point of failure stray currents flowed from the pipeline...
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Opracowanie systemu monitorowania korozji instalacji podstawowej Alkilacji HF w celu bieżącej oceny zagrożenia korozyjnego instalacji
PublicationWykonano analizę stanu zagrożenia korozyjnego instalacji alkilacji HF w PKN Orlen S.A. Wytypowano miejsca które powinny zostać objęte systemem monitorowania korozji. Zaprojektowano śluzę korozyjną. Dokonano oceny merytorycznej oraz finansowej różnych rozwiązań systemów monitorowania korozji
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Research on causes of corrosion in the municipal water supply system
PublicationThis paper presents results of failure analysis study to characterize the corrosion damage that occurred in the water supply system in Krakow. This analysis includes: electrochemical noise, linear polarization and resistometric measurements. Water aggressiveness of four water intakes was defined using Langelier and Ryznar indices. Results from this indices did not reveal the causes of considerable corrosion losses in water systems....
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System pomiaru szybkości korozji metodą polaryzacji liniowej w zbiorniku zatłaczającym wodę złożową oraz systemu wody morskiej na platformie wydobywczej Baltic Beta
PublicationWykonano analizę sprawności systemu monitorowania szybkości korozji na Platformie wydobywczej Baltic Beta. Dokonano niezbędnych czynności, które umożliwiły ponowne uruchomienie systemu. Przedstawiono rejestry szybkości korozji w okresie od 01.01.2015 do 24.11.2016
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Wyjaśnienie przyczyn pocienienia rur w piecu technologicznym PC-1 na instalacji DRW II
PublicationWykonano analizę przyczyn korozji rur pieca instalacji DRW w oparciu o badania wizualne, SEM, EDX oraz literaturowe. W ciągu 5 lat eksploatacji nastąpiły znaczne ubytki korozyjne rur w wyniku procesów korozyjnych. Z uwagi na zbyt wysoką temperaturę rurek pieca nastąpił proces wysokotemperaturowego pylenia metalu.
Year 2015
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Assessment of protective properties of rubber lining in absorbers of flue gas desulphurization systems.
PublicationResults of research on degradation of rubber lining which is the main protection of absorbers in flue gas desulphurization (FGD) systems were presented. The power plant where the system operated is lignite-fired. Owing to measurements using electrochemical impedance spectroscopy and gravimetric determination of water content in the lining, the areas of the system which are most exposed to degradation were shown. The results obtained...
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Instantaneous impedance monitoring of AA 7075 aluminum alloy corrosion in borate buffer with admixed chloride ions
PublicationThe study presents a research capabilities of Dynamic Electrochemical Impedance Spectroscopy (DEIS) as a tool used for instantaneous on-line monitoring of corrosion processes on the example of AA 7075 aluminum alloy. A borate buffer with admixed chloride ions in a quantity ranging from 0.05 to 25 mM was used to represent different types of corrosion attack. The surface of samples specimens was evaluated before and after the tests...
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The protection and monitoring of a distribution piping network for potable water supply
PublicationPurpose – The purpose of this paper is to implement the corrosion protection method for steel pipes used in a municipal water-pipe network. Results of an inhibitor protection system installed on the system are presented. Inhibitor protection was required due to the high corrosivity of the water collected by a surface intake, which had resulted in a large number of failures and low water quality, due to the presence of corrosion...
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Zagrożenia korozyjne stali nierdzewnych w przemyśle spozywczym
PublicationPrzedstawiono przyczyny występowania zagrożeń korozyjnych stali nierdzewnych w przemyśle spożywczym. Szczegółowo omówiono mechanizm oraz sposób zapobiegania korozji wżerowej, szczelinowej oraz pękania korozyjnego. Zaprezentowano dokumentację fotograficzną omówionych typów korozji. Wskazano podstawowe problemy związane z doborem materiałów konstrukcyjnych do budowy instalacji w przemyśle spożywczym.
Year 2014
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Analiza weryfikująca poprawność istniejącego układu ochrony przed korozją i osadami instalacji DRW4 w kontekście obecnych warunków pracy instalacji
PublicationCelem pracy były pomiary korozyjności kondensatów pochodzących z kolumny destylacyjnej z dodatkiem neutralizatora oraz inhibitora korozji, ponadto przeprowadzono badania SEM i EDX produktów korozji pochodzących z rurek chłodnicy powietrznej. Wykazano, że znacznie większą agresywnością charakteryzują się kondensaty które pochodzą z przerobu ropy naftowej zawierającą slopy.
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Effect of native air-formed oxidation on the corrosion behavior of AA7075 aluminum alloys
PublicationThe microstructure of aluminum alloys plays a key role in their corrosion resistance. In particular, the presence of intermetallic precipitates differing in the potential from the alloy matrix induces local corrosion. The study presents the effect of native air-formed oxidation on the corrosion behavior of AA 7075 aluminum alloy. Various microscopic and spectroscopic techniques were used to examine the changes occurring in the...
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Simultaneous impedance and volumetric studies and additionally potentiodynamic polarization measurements of molasses as a carbon steel corrosion inhibitor in 1M hydrochloric acid solution
PublicationThe inhibition effect of molasses on the corrosion of low carbon steel in 1M hydrochloric acid solution was investigated by volumetric and electrochemical measurements. Potentiodynamic polarization and dynamic electrochemical impedance spectroscopy (DEIS) results were obtained and compared with to those, obtained with the hydrogen evolution technique. All results indicate that molasses functioned as a good inhibitor in 1M hydrochloric...
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Zbadanie środowiska korozyjnego oraz jego wpływu na rozkład, wielkość i głębokość wżerów korozyjnych rur.
PublicationPrzedstawiono wyniki oceny wizualnej rurociągów składowanych w okolicy Warszawy. Stwierdzono występowanie korozji galwanicznej w wyniku tworzenia się ogniw zmiennego napowietrzenia. Obserwacje poparto badaniami laboratoryjnymi.
Year 2013
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ANALIZA STANU TECHNICZNEGO RUROCIĄGÓW: WODY PRZeMYSŁOWEJ I SOLANKI
PublicationPracę wykonano na zlecenie Przedsiębiorstwa Badawczo-Wdrożeniowego "HYDRO-POMP" Sp. z o.o. ul. Wróblewskiego 19, 93-578 Łódź. Wykonawcą zlecenia jest Politechnika Gdańska, Wydział Chemiczny, Katedra Elektrochemii, Korozji i Inżynierii Materiałowej, 80-233 Gdańsk, ul. G. Narutowicza 11/12. Celem pracy była analiza stanu technicznego i badania dwóch rurociągów: solanki oraz wody przemysłowej. Badania wykonywano w warunkach terenowych...
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Badanie przyczyn korozji zbiorników magazynowych na paliwa na terenie stacji benzynowej grupy Lotos w Pruszkowie
PublicationPrzedstawiono wyniki oględzin zbiornika na olej napędowy eksploatowany na stacji benzynowej w Pruszkowie. Przedstawiono możliwe przyczyny powstania zniszczeń korozyjnych w dolnej części zbiornika.
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Corrosion monitoring by harmonic analysis in aqueous environments
PublicationThis paper presents tests concerning the rate of corrosion in non-alloy steel (type S235JR) in an aqueous environment, with an additive of sodium chloride by means of polarization resistance measurements and harmonic analysis. The tests have been carried out for steel samples exposed to the testing environment for six weeks, in order to obtain a constant rate of corrosion in the function of time. The measurements have aimed at...
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Multi-sensor monitoring of the corrosion rate and the assessment of the efficiency of a corrosion inhibitor in utility water installations
PublicationThis paper presents an implementation of the monitoring of the corrosion rate and the assessment of the efficiency of a corrosion inhibitor in a utility water installation using an automated corrosion monitoring system. Due to the fact that the corrosion inhibitor was added to water intended for human consumption, it was necessary to build a multi-sensor monitoring system. In order to implement corrosion monitoring using a linear...
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Opinia dotycząca zagrożenia korozyjnego zbiorników wody ciepłej na terenie warzelni browaru w Białymstoku
PublicationStwierdzono występowanie pęknięć w zbiorniku wody ciepłej procesowej w browarze w Białymstoku. Propagacja pęknięć ma miejsce w obrębie spawu. Wykonano niezbędne badania, oraz zaproponowano metodę ochrony zbiornika przed dalszym rozwojem korozji naprężeniowej.
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Pitting corrosion and stress-corrosion cracking of buffer tanks in a brewery
PublicationW pracy przedstawiono wyniki ekspertyzy zbiornika magazynowego na ciepłą wodę do produkcji piwa w browarze. Zbiornik uległ przyśpieszonym procesom korozyjnym, które doprowadziły do jego perforacji. Podczas eksploatacji zbiornika wystąpił proces korozji wżerowej oraz pękania korozyjnego. Przyśpieszone procesy korozyjne zbiornika związane były z wysoką zawartością jonów chlorkowych w wodzie oraz statycznymi naprężeniami mechanicznymi....
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