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Search results for: high-intensity sweeteners
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Retention behaviour of some high-intensity sweeteners on different SPE sorbents
PublicationThe objective of this paper is to provide information about application of solid phase extraction (SPE) for isolation of nine high-intensity sweeteners (acesulfame-K, alitame, aspartame, cyclamate, dulcin, neotame, saccharin, sucralose and neohesperidin dihydrochalcone) from aqueous solutions. The influence of several types of LC-MS compatible buffers (different pH values and compositions) on their recovery has been studied and...
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The content of high-intensity sweeteners in different categories of foods available on the Polish market
PublicationThe objective of this study was to measure the concentrations of nine high-intensity sweeteners (acesulfame-K, aspartame, alitame, cyclamate, dulcin, neohesperidin DC, neotame, saccharin and sucralose) in different categories of food available on the Polish market. Over 170 samples of different brands of beverages, yoghurts, fruit preparations, vegetable preserves and fish products were analysed using an analytical procedure based...
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Determination of high-intensity sweeteners in beverages by high-performance liquid chromatography with mass spectrometry detection.
PublicationThe objective of the present study was to measure the concentration of nine high intensity sweeteners (acesulfame-K, aspartame, alitame, cyclamate, dulcin, neohesperidin dihydrochalcon, neotame, saccharin and sucralose) in different types of beverages available on the polish market. The proposed methodology reported here consists of a extraction with buffer composed of formic acid and N,N-diisopropylethylamine (pH 4.5) followed...
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Determination of nine high-intensity sweeteners in various foods by high-performance liquid chromatography with mass spectrometric detection
PublicationAn analytical procedure involving solid-phase extraction (SPE) and high-performance liquid chromatography-mass spectrometry has been developed for the determination of nine high-intensity sweeteners authorised in the EU; acesulfame-K (ACS-K), aspartame (ASP), alitame (ALI), cyclamate (CYC), dulcin (DUL), neohesperidin dihydrochalcone (NHDC), neotame (NEO), saccharin (SAC) and sucralose (SCL) in a variety of food samples (i.e. beverages,...
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Application of two-dimensional intensity maps in high-accuracy polarimetry
PublicationWe propose the analysis of 2D intensity contour maps which is based on the optical transmission function for the polarizer-specimen-analyzer system. A small modification of the high-accuracy universal polarimeter (HAUP) technique was used to measure the intensity maps (HAUP maps) and determine the phase retardation, linear dichroism (LD) parameters, and multiple light reflection contribution in uniaxial crystals. We have performed...
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RADIATION OF HIGH INTENSITY SOUND BY CIRCULAR DISC BY MEANS OF THE NUMERICAL METHOD
PublicationThe main goal of this paper is to find sound pressure distribution radiated by the circular piezoelectric disc that vibrates with the finite amplitude. There has been presented the pressure distribution close to the radiating surface. Also it is shown the sound pressure distribution in the 3D form. The mathematic modeling was carried out on the base of the nonlinear acoustic equation with the proper boundary condition. The axial...
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Determination of Nine Intense Sweeteners in Foodstuffs by High-Performance Liquid Chromatography and Evaporative Light-Scattering Detection: Interlaboratory Study
PublicationW pracy przedstawiono wyniki badań międzylaboratoryjnych, opracowanej wcześniej metody jednoczesnego oznaczania dziewięciu słodzików o wysokiej mocy w produktach żywnościowych. W badaniach wzięło udział siedem laboratoriów (Belgia, Niemcy, Portugalia). W rezultacie dowiedziono, iż opracowana metoda umożliwia uzyskanie dokładnych, powtarzalnych i odtwarzalnych wyników analiz dla wszystkich badanych słodzików i typów żywności.
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Contamination of runoff waters from roads with high traffic intensity in the urban region of Gdańsk, Poland
PublicationW ramach pracy prowadzone były badania zanieczyszczeń w próbkach wód spływnych z arterii komunikacyjnych. Próbki pobierano z sześciu stałych punktów zlokalizowanych wzdłuż szlaku komunikacyjnego prowadzącego z Redy do Gdańska (z miejsc o dużym natężeniu ruchu pojazdów) oraz z ulicy M. Buczka w Redzie (o mniejszym natężeniu ruchu). Próbki pobierane były przez okres dwóch miesięcy (okres deszczów jesiennych: 24.10 - 18.12.2000) oraz...
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Comparison of low-temperature cracks intensity on pavements with high modulus asphalt concrete and conventional asphalt concrete bases
PublicationHigh modulus asphalt concrete (HMAC) base courses provide very good resistance to rutting and fatigue but they can increase the risk of low-temperature cracking as compared with conventional asphalt concrete (AC). The article presents the comparison of these two road materials in terms of low-temperature cracking. The statistical method based on the ordered logistic regression model was used. The analysis was based on results of...
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Analytical methodologies for determination of artificial sweeteners in foodstuffs- a review
PublicationArtificial high-intensity sweeteners are more and more frequently used for food production. Food industry tends to highlight beneficial aspects of their use, such as tooth-friendliness, rising-up quality of life of those suffering from different forms of diabetes and possibility of weight control without sacrificing favorite unhealthy drinks or snacks. On the other hand some of the consumers are deeply concerned about safety of...