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Enhanced extraction of proteins using cholinium-based ionic liquids as phase-forming components of aqueous biphasic systems
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Chemically Bonded Silica Stationary Phases: Synthesis, Physicochemical Characterization, and Molecular Mechanism of Reversed-Phase HPLC Retention
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Examination of the influence of macro and microscopic parameters of limestone on the effectiveness of gas phase desulphurisation according to the method of wet limestone
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Determination of fluoride as fluorosilane derivative using reversed-phase HPLC with UV detection for determination of total organic fluorine
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Discrimination of Selected Cold-Pressed and Refined Oils by Untargeted Profiling of Phase Transition Curves of Differential Scanning Calorimetry
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Numerical Simulation and Experimental Analysis of Thermal Cycles and Phase Transformation Behavior of Laser-Welded Advanced Multiphase Steel
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Application of reversed-phase thin layer chromatography and QSRR modelling for prediction of protein binding of selected β-blockers
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Best State Estimate for the Phase Angles of Busbars in Power Systems via Circuit Modeled with DC Load Flow
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Physical properties of homogeneous TiO2films prepared by high power impulse magnetron sputtering as a function of crystallographic phase and nanostructure
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Venetoclax in relapsed or refractory chronic lymphocytic leukaemia with 17p deletion: a multicentre, open-label, phase 2 study
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Application of normal-phase high-performance liquid chromatography followed by gas chromatography for analytics of diesel fuel additives
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Phase IIa study of the CD19 antibody MOR208 in patients with relapsed or refractory B-cell non-Hodgkin’s lymphoma
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Modeling and experimental investigation of the hydraulic jump in liquid film formed by an impinging two-phase air-water jet
PublicationPrzedstawiono model analityczny układu hydraulicznego powstałego na skutek uderzenia strugi dwufazowej wody i powietrza. Obliczenia porównano z badaniami eksperymentalnymi przeprowadzonymi na własnym stanowisku badawczym. Uzyskano zadowalającą zgodność.
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On performance limits of switched-capacitor multi-phase charge pump circuits. Remarks on papers of Starzyk et al.
PublicationW pracy zweryfikowano hipotezę Starzyka nt. maksymalnego, osiągalnego wzmocnienia napięciowego w wielotaktowym konwerterze napięcia stałego typu C-przełączane (w tzw. pompie ładunkowej). W konwerterze zbudowanym z k kondensatorów maksymalne wzmocnienie określone jest przez odpowiednią potęgę liczby 2 tj. 2^(k-1) przy czym warunek podany przez Starzyka jest konieczny lecz nie jest dostateczny. Podano warunki konieczne i dostateczne...
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Investigating the Ischaemic Phase of Skin NADH Fluorescence Dynamics in Recently Diagnosed Primary Hypertension: A Time Series Analysis
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Application of deep eutectic solvents in analytical sample pretreatment (update 2017–2022). Part A: Liquid phase microextraction
PublicationSustainable development in all branches of human activity has become an unequivocal necessity in the last two decades, and green chemistry goes hand in hand with it. Various ways have been proposed in analytical chemistry to meet the current requirements of green chemistry. One such approach is the research of new reagents and solvents for analytical purposes. Deep eutectic solvents (DESs) began being investigated and used in analytical...
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High Dynamic Range Microwave Displacement and Rotation Sensors Based on the Phase of Transmission in Groove Gap Waveguide Technology
PublicationThis research is focused on the design and realization of displacement sensors in gap waveguide technology. It is shown that with a small but fundamental change in the structure of a conventional gap waveguide, a linear displacement can be sensed. To this end, a unique feature of gap waveguides, i.e. the fact that no electrical connection between the top and bottom parts of the gap waveguide is required, is used. It is further shown...
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Silicon polypodands: powerful metal cation complexing agents and solid–liquid phase-transfer catalysts of new generation
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Tattooed man: Could menstrual cycle phase and contraceptive use change female preferences towards bad boys?
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The research on properties of asphaltene stationary phase to separate mixtures of optically active compounds with the use of gas chromatography technique
PublicationW pracy przedstawiono wyniki badań nad możliwością zastosowania asfaltenów jako chiralnej fazy stacjonarnej do chromatografii gazowej. Wyniki uzyskane dla fazy asfaltenowej porównano z wynikami uzyskanymi poprzez zastosowanie komercyjnie dostępnej chiralnej fazy stacjonarnej. Badania wykazały, że frakcja asfaltenowa posiada właściwości umożliwiające uzyskanie rozdzielenia mieszanin związków optycznie czynnych.
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Study of Phase Transformation Processes Occurring in the Nanocrystalline Iron/Ammonia/Hydrogen System by the Magnetic Permeability Measurement Method
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Development of headspace solid-phase microextraction-gas chromatography method for the determination of solvent residues in edible oils and pharmaceuticals
PublicationW pracy przedstawiono wyniki opracowania procedury oznaczania pozostałości rozpuszczalników organicznych w olejach jadalnych z wykorzystaniem techniki HS-SPME na etapie izolacji i wzbogacania analitów. Przedstawiono proces optymalizacji etapu izolacji i rozdzielenia związków. Dla każdego z analitów wyznaczono parametry walidacyjne charakteryzujące procedurę tj. granice wykrywalności, granicę oznaczalności, liniowość, zakres pomiarowy,...
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Physical aspect of application and usefulness of semi-Markovian processes for modelling the processes occurring in operational phase of technical objects.
PublicationW artykule zasygnalizowano przydatność teorii procesów semimarkowskich do tworzenia modeli procesów rzeczywistych, zachodzących w fazie eksploatacji różnych obiektów technicznych. Przydatność tej teorii została wykazana w wyniku przedstawienia: specyfiki procesów semimarkowskich oraz fizykalnych aspektów stosowania procesów semimarkowskich jako modeli procesów zachodzących w fazie eksploatacji wspomnianych obiektów. Specyfika została...
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Competitive Adsorption of a Binary VOC Mixture from the Gas Phase onto Activated Carbon Modified with Malic Acid
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Effect of the ionic liquids on extraction of aromatic and sulfur compounds from the model petrochemical stream
PublicationSuitability of a imidazolium ionic liquids (ILs) as solvents in dearomatization and desulfurization in the ternary systems and in a model multicomponent systems has been analyzed. With this aim, ternary liquid-liquid phase equilibrium data (LLE) have been obtained for ternary mixtures of {IL + benzene, or toluene, or thiophene, or 2-butanethiol + hexane}, or {IL + benzene + 2-methylpentane} at T = 298.15 K and ambient pressure,...
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Zastosowanie chromatografii cieczowej w odwróconym układzie faz (RP-LC) w rozdzielanie i oznaczaniu polifenoli i naftochinonów w materiałach roslinnychreversed = Phase liquid chromatography (RP-LC) for separation and quantitative determination of polyphenols and naphtoquinones in plant materials
PublicationW pracy przedstawiono przegląd metod rozdzielania i oznaczania naftochinonów i polifenoli pochodzących z materiału roślinnego, z wykorzystaniem technik chromatograficznych w układzie faz odwróconych - RP-TLC (Reversed-Phase Thin Layer Chromatography) oraz RP-HPLC (Reversed-Phase High Performance Liquid Chromatography). Przeanalizowano procedury przygotowania próbki, etap rozdzielania, a także kontroli czystości zbieranych frakcji....
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Emergence of Aggregation Induced Emission (AIE), Room-Temperature Phosphorescence (RTP), and Multistimuli Response from a Single Organic Luminogen by Directed Structural Modification
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Effectiveness of either short-duration ischemic pre-conditioning, single-set high-resistance exercise, or their combination in potentiating bench press exercise performance
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Comparison of two infant chest compression techniques during simulated newborn cardiopulmonary resuscitation performed by a single rescuer: A randomized, crossover multicenter trial
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Comparison of heat transfer from single- and double-sided heated horizontal plate under free convection in air with constant heat flux condition
PublicationThis paper presents the results of an experimental and numerical study of convective heat transfer from a newly designed double-sided heated horizontal plate in air. To ensure equal heat transfer from both surfaces, the plate was equipped with two independently supplied electric heaters and resistance thermometers on each side. Minimizing the plate's thickness reduced lateral heat loss and improved measurement accuracy. The study...
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Development of a new green analytical methodology for the determination of phthalates in single-use babies diapers using ultrasound-assisted extraction and polypropylene porous membrane
PublicationA green extraction strategy was developed and utilized for the extraction and determination of phthalates. The extraction is based on ultrasound-assisted extraction and a polypropylene porous membrane. The Box-Behnken model was performed to optimize the extraction condition. The optimal extraction conditions are 5.5 mL of ethyl acetate, 10 min of extraction time and 55 C for extraction temperature. The developed green extraction...
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Diamond-Phase (Sp3-C) Rich Boron-Doped Carbon Nanowalls (Sp2-C): A Physico-Chemical And Electrochemical Properties
PublicationThe growth of B-CNW with different boron doping levels controlled by the [B]/[C] ratio in plasma, and the influence of boron on the obtained material’s structure, surface morphology, electrical properties and electrochemical parameters, such as -ΔE and k°, were investigated. The fabricated boron-doped carbon nanowalls exhibit activity towards ferricyanide redox couple, reaching the peak separation value of only 85 mV. The flatband...
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Influence of pH of sol-gel solution on phase composition and photocatalytic activity of TiO 2 under UV and visible light
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New Green Determination of Cu, Fe, Mn, and Zn in Beetroot Juices along with Their Chemical Fractionation by Solid-Phase Extraction
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Analysis of Fluorescence Lifetime of Protochlorophyllide and Chlorophyllide in Isolated Etioplast Membranes Measured from Multifrequency Cross-correlation Phase Fluorometry
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The quantification of bisphenols and their analogues in wastewaters and surface water by an improved solid-phase extraction gas chromatography/mass spectrometry method
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Recovery of Nonsteroidal Anti-Inflammatory Drugs from Wastes Using Ionic-Liquid-Based Three-Phase Partitioning Systems
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Thermophysical properties and phase equilibria study of the binary systems {N-hexylquinolinium bis(trifluoromethylsulfonyl)imide+aromatic hydrocarbons, or an alcohol}
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Preparation and evaluation of solid-phase microextraction fibres based on functionalized latex nanoparticle coatings for trace analysis of inorganic anions
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A simple graphene-based pipette tip solid-phase extraction of malondialdehyde from human plasma and its determination by spectrofluorometry
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Quantitative structure—retention relationship modeling of the retention behavior of selected antipsychotic drugs in normal-phase thin-layer chromatography
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DSC Phase Transition Profiles Analyzed by Control Charts to Determine Markers for the Authenticity and Deterioration of Flaxseed Oil during Storage
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Venetoclax for Patients With Chronic Lymphocytic Leukemia With 17p Deletion: Results From the Full Population of a Phase II Pivotal Trial
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New approach based on solid-phase extraction for the assessment of organic compound pollutions in so-called pharmaceutically pure water
PublicationOpisano mozliwość zastosowania nowej procedury analitycznej opartej na wykorzystaniu techniki ekstrakcji do fazy stałej (na etapie izolacji i wzbogacania analitów) do oznaczania śladowych ilości zanieczyszczeń organicznych w wodzie specjalnej czystości używanej do celów farmaceutycznych.Próbka badanej wody jest przepuszczana przez złoże sorbenta, które jest osuszane za pomocą strumienia oczyszczonego powietrza, przed etapem termicznej...
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Estimation of platinum in environmental water samples with solid phase extraction technique using inductively coupled plasma mass spectrometry
PublicationZoptymalizowano metodykę oznaczania śladowych poziomów stężeń platyny (IV) w oparciu o technikę ekstrakcji do fazy stałej w połączeniu ze spektrometrią mas z plazmą wzbudzoną indukcyjnie. Na etapie wzbogacania platyny wykorzystano żel krzemionkowy modyfikowany grupami aminopropylowymi. Ilościowy odzysk platyny uzyskano poprzez wykorzystanie 1.0 mol L-1 roztworu tiomocznika jako eluenta. Odchylenie standardowe wyników (RSD) było...
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TiO2 with Tunable Anatase-to-Rutile Nanoparticles Ratios: How Does the Photoactivity Depend on the Phase Composition and the Nature of Photocatalytic Reaction?
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Purification and recovery of laccase produced by submerged cultures of Trametes versicolor by three-phase partitioning as a simple and highly efficient technique
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Monitoring the gas turbine start-up phase on the platform using a hierarchical model based on Multi-Layer Perceptron networks
PublicationVery often, the operation of diagnostic systems is related to the evaluation of process functionality, where the diagnostics is carried out using reference models prepared on the basis of the process description in the nominal state. The main goal of the work is to develop a hierarchical gas turbine reference model for the estimation of start-up parameters based on multi-layer perceptron neural networks. A functional decomposition...
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Low-temperature synthesis of zeolite from perlite waste — Part I: review of methods and phase compositions of resulting products
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Image Processing of Mg-Al-Sn Alloy Microstructures for Determining Phase Ratios and Grain Size and Correction with Manual Measurement
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