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Wyniki wyszukiwania dla: b(a)p
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Determination of tributyltin in marine sediment: Comit� Consultatif pour la Quantit� de Mati�re (CCQM) pilot study P-18 international intercomparison
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A new B-D-galactosidase with a low temperature optimum isolated from the Antarctic Arthrobacter sp. 20B: gene cloning, purification and characterization.
PublikacjaA psychrotrophic bacterium producing a coldadaptedB-galactosidase upon growth at low temperatureswas classiWed as Arthrobacter sp. 20B. A genomic DNAlibrary of strain 20B introduced into Escherichia coliTOP10F' and screening on X-Gal (5-bromo-4-chloro-3-indolyl-B-D-galactopyranoside)-containing agar plates ledto the isolation of B-galactosidase gene. The B-galactosidasegene (bgaS) encoding a protein of 1,053 amino acids,with a...
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Effect of chemical structure and deposition method on optical properties of polyazomethines with alkyloxy side groups
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Optical properties of phenylene–thiophene-based polyazomethine thin films
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Phosphinoborenium cations stabilized by N-heterocyclic carbenes: synthesis, structure, and reactivity
PublikacjaPhosphinoborenium cations stabilized by N-heterocyclic carbenes (NHCs) were synthesized via the reaction of bromo(phosphino)boranes with NHCs. Their structures were investigated by heteronuclear magnetic resonance spectroscopy, X-ray diffraction, and density functional theory calculations. They possess a planar trigonal boron center directly bonded with the pyramidal phosphanyl group (PR2) and can be treated as cationic phosphinoboranes....
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Crystal structure and physical properties of AePd1-xP1+x (Ae = Ca, Sr)
PublikacjaWe report the discovery of two new compounds AePd1-xP1+x (Ae = Ca, Sr) crystallized in different hexagonal structures. Single crystals of AePd1-xP1+x (Ae = Ca, Sr) are obtained using the Bi-flux method. Crystallographic analysis by both powder and single crystal X-ray diffraction shows that CaPd1-xP1+x crystallizes in a non-centrosymmetric hexagonal structure with the space group P-6m2 (No.187) and lattice parameters a = b = 4.0391(9)...
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Effect of Cyclodextrins on Coupling of o-Ethoxybenzenediazonium Salt with Pyrrole, Imidazole and 2-Methylimidazole
PublikacjaThe effect of b-cyclodextrin on o-ethoxybenzenediazonium salt coupling with pyrrole, imidazole and 2-methylimidazole has been studied. The differences in the reaction course, the overall yield and products distribution have been analyzed. Experiments without cyclodextrins and selected reactions with a- and c-cyclodextrins have been performed for comparison. The results are discussed in terms of co-conformation of azole molecules...
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Parseval Wavelet Frames on Riemannian Manifold
PublikacjaWe construct Parseval wavelet frames in L 2 (M) for a general Riemannian manifold M and we show the existence of wavelet unconditional frames in L p (M) for 1 < p < ∞. This is made possible thanks to smooth orthogonal projection decomposition of the identity operator on L 2 (M), which was recently proven by Bownik et al. (Potential Anal 54:41–94, 2021). We also show a characterization of Triebel–Lizorkin F sp,q (M) and Besov B...
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Late Aortic Remodeling after Endovascular Repair of Complicated Type B Aortic Dissection—TEVAR Protects Only the Covered Segment of Thoracic Aorta
PublikacjaIntroduction: TEVAR is the preferred way of treatment of complicated type B aortic dissection. The purpose of the study was to assess the impact of TEVAR on aortic remodelling in the thoracic and abdominal segment in long-term follow-up. Methods: 23 patients with complicated type B aortic dissection were treated by TEVAR in years 2004-2012 in our Department. Aortic remodelling was rated based on preoperative and final follow-up...
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Estimation of a smoothness parameter by spline wavelets
PublikacjaWe consider the smoothness parameter s*(f) of a function f∈L2(R) in terms of Besov spaces. The existing results on estimation of smoothness [K. Dziedziul, M. Kucharska and B. Wolnik, J. Nonparametric Statist. 23 (2011)] employ the Haar basis and are limited to the case 0
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Phase diagram of P3HT:PC70BM thin films based on variable-temperature spectroscopic ellipsometry
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New approach in determination of urinary diagnostic markers for prostate cancer by MALDI-TOF/MS
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Reactivity of bulky aminophosphanes towards small molecules: Activation of dihydrogen and carbon dioxide by aminophosphane/borane frustrated Lewis pairs
PublikacjaA series of mono- and bisaminophosphanes with formulas R2NPR’R’’ and (R2N)2PR’ (R = iPr, Cy; R’ = Ph, Cy; R’’ = iPr) were characterized by X-ray analysis, NMR spectroscopy and computational methods. The common structural futures of these species are short and polarized PAN bonds, a pyramidal geometry at the P atom and an almost planar geometry at the N atoms. According to DFT calculations, these...
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Diamond-Phase (Sp3-C) Rich Boron-Doped Carbon Nanowalls (Sp2-C): A Physico-Chemical And Electrochemical Properties
PublikacjaThe growth of B-CNW with different boron doping levels controlled by the [B]/[C] ratio in plasma, and the influence of boron on the obtained material’s structure, surface morphology, electrical properties and electrochemical parameters, such as -ΔE and k°, were investigated. The fabricated boron-doped carbon nanowalls exhibit activity towards ferricyanide redox couple, reaching the peak separation value of only 85 mV. The flatband...
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TL, OSL and RL emission spectra of RE-doped LiMgPO4 crystals
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Nonlinear Properties of Seawater as a Factor Determining Nonlinear Wave Propagation
PublikacjaTaking practical advantage of nonlinear acoustical interactions occurring in seawater [1, 2] requires knowledge of the parameter of nonlinearity B=A of this medium. The literature does not offer much reports on B=A parameter value for seawater. In the few papers concerning that address the issue, results concerning ocean waters with high salinity and at large depths are given [3], while studies concerning seawater with low salinity...
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Comparison of Fluoride Ion-Selective Electrode Based Potentiometric Methods of Fluoride Determination in Human Urine
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A study of concentration depolarization and quenching of photoluminescence of solutions
PublikacjaThe concentration-dependence of emission anisotropy r/r0 and quantum yield eta/eta0 of the photoluminescence of glycerol-water solutions of rhodamine B in two systems of viscosities 7.4 P and 0.72 P is investigated. The experimental data are compared with the new theory of concentraticn depolarization (J. Lumin., 5, 413 (1972)) and concentration quenching of photoluminescence (Acta Phys. Hungar., 30, 145 (1972)), which takes...
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Aging and rejuvenation effects in bismuth ferrite micro-cubes
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An MTA-phosphorylase gene discovered in the metagenomic library derived from Antarctic top soil during screening for lipolytic active clones confers strong pink fluorescence in the presence of rhodamine B.
PublikacjaIn this work, we present the construction of a metagenomic library in Escherichiacoli using the pUC19 vector and environmental DNA directly isolated fromAntarctic topsoil and screened for lipolytic enzymes. Unexpectedly, the screeningon agar supplemented with olive oil and rhodamine B revealed one unusual pinkfluorescent clone (PINKuv) out of 85 000 clones. This clone harbored a plasmid,pPINKuv, which has an insert of 8317 bp that...
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Synthesis of 3-D Graphene via Combustion Synthesis of Magnesium and Calcium/Magnesium Oxalates
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One-Step Combustion Synthesis of Novel Nanocarbons via Magnesiothermic Reduction of Carbon-Containing Oxidants
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Magnetic Relaxation in Bismuth Ferrite Micro-Cubes
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In vitro substance P-dependent induction of bone marrow cells in common (CD10) acute lymphoblastic leukaemia
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OSL and RL of LiMgPO4 crystals doped with rare earth elements
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Immunocytochemical Study on Endothelial Integrity of Saphenous Vein Grafts Harvested by Minimally Invasive Surgery with the Use of Vascular Mayo Stripers. A Randomized Controlled Trial
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Management and protection system for superconducting tokamak
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Stimulated by cyclodextrins high yield synthesis of azocrown analogues comprising pyrrole or imidazole residues
PublikacjaThe influence of cyclodextrins (CDs) on the formation of azocrown ethers comprising pyrrole, imidazole and substituted imidazole has been studied. Pyrrole, imidazole, 2-methyl-, 4-methyl- and 4-phenylimidazole were coupled with bisdiazonium salts derived from bis-1,5-(2-aminophenoxy)-3-oxapentane or bis-1,8-(2-aminophenoxy)-3,6-dioxaoctane to form macrocyclic compounds with two azo units. The syntheses were performed under standard...
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Galerkin formulations of isogeometric shell analysis: Alleviating locking with Greville quadratures and higher-order elements
PublikacjaWe propose new quadrature schemes that asymptotically require only four in-plane points for Reissner–Mindlin shell elements and nine in-plane points for Kirchhoff–Love shell elements in B-spline and NURBS-based isogeometric shell analysis, independent of the polynomial degree p of the elements. The quadrature points are Greville abscissae associated with pth-order B-spline basis functions whose continuities depend on the specific...
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Tensile and flexural moduli for human orbital wall bones – comparative study
PublikacjaThe main aims of the current research were: (1) to analyze in detail the tensile modulus and ultimate tensile strength (UTS) of orbital wall bones separately for the left and right orbit of the same cadaver and (2) to compare the obtained results with a flexural modulus of the left and right orbit reported earlier by A. C. van Leeuwen et al. [14]. A set of 54 specimens of orbital superior and/or medial walls harvested from 16 human...
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Photocatalytic decomposition of benzo-[a]-pyrene on the surface of acrylic, latex and mineral paints. Influence of paint composition
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Improvement of photocatalytic activity of silicate paints by removal of K2SO4
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INFLUENCE OF SINGLE-STAGE AND DUPLEX SHOT PEENING ON SURFACE ROUGHNESS AND RESIDUAL STRESSES IN Al Mg5 Mn1 Sc0,8 Zr0,4 ALLOY
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Comparison of commercial thermoluminescent readers regarding high-dose high-temperature measurements
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Two-dimensional thermoluminescence method for checking LiF crystals homogeneity
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The Investigation of Thermal and Optical Properties of Semiconducting Nanostructural Hybrid Films
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Parasitological and molecular identification of cestode Bothriocephalus scorpii sensu stricto in the new host Chelidonichthys lucerna (L. 1758) (Triglidae, Scorpaenoidei) from the North Sea
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Two-step synthesis of niobium doped Na–Ca–(Mg)–P–Si–O glasses
PublikacjaNiobium doped biosolubility glasses in the Na–Ca–(Mg)–P–Si–O system were prepared by using an untypical two-step synthesis route. The parent glass was melted in air atmosphere at 1350 °C followed by re-melting the glass in Nb crucible with the addition of metallic Mg/Ca powder in the nitrogen atmosphere. The second melting step was carried out at 1450–1650 °C, using an induction furnace. The topography and structure of the obtained...
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Laser stimulated second and third harmonic optical effects in F: SnO2 nanostructures grown via chemical synthetic route
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Carbon catalysts from pine cones – Synthesis and testing of their activities
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Hydrogen evolution on the reduced TiO2 under simulated solar lamp
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Studying of polyoxadiazole with Si atom in the backbone
PublikacjaPurpose: The aim of this paper is to show properties of spin-coated thin films of new polymer having siliconatom in the backbone. This amorphous polymer has appeared to be applied as active films in organic devices (asOLED).Design/methodology/approach: Thin films of 4-(diphenyl(4-(4-(5-(p-tolyoxy)phenyl)-1,3,4-oxadiazol-2-yl)phenyloamino)methyl)-phenyl)silyl)-1-methylbenzamide (Oxad–Si-B) were obtained by spin-coating method.The...
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OSL properties of lithium aluminate crystals grown with Micro-Pulling-Down technique
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Mo-P5:335 Influence of life style knowledge on the occurrence of cardiovascular risk factors in adults living in Krakow - South Poland
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29 Metabolic Syndrome and Selected Coronary Heart Disease Risk Factors in the Group of Krakow Adult Residents
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An inherited NBN mutation is associated with poor prognosis prostate cancer
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Phonon Mechanism of the Magnetostructural Phase Transition in MnAs
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Selected molecular and microfluidic aspects of mammalian oocyte maturation-perspectives: a review
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The structure and role of mammalian sperm RNA: a review
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Updated 24-year trend of Type 1 diabetes incidence in children in Poland reveals a sinusoidal pattern and sustained increase
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