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Wyniki wyszukiwania dla: Oxygen electrode
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Fe local structure in Pt-free nitrogen-modified carbon based electrocatalysts: XAFS study
PublikacjaThe paper presents a new results on the bonding environment (coordination number and geometry) and on oxidation states of Fe in nitrogen-modified Fe/C composites used as Pt-free catalysts for oxygen reduction in Direct Hydrogen Fuel Cells. Starting from glucose or fructose, two catalysts displaying different electrochemical performance were prepared and studied in the form of pristine powder and thin catalytic layer of electrode...
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Nanokrystaliczne warstwy ceramiczne otrzymywane metodą pirolizy aerozolowej w tlenkowych ogniwach paliwowych
PublikacjaNiniejsza rozprawa doktorska dotyczy badań materiałów wytwarzanych w postaci cienkich, nanokrystalicznych warstw ceramicznych metodą pirolizy aerozolowej dla zastosowań w tlenkowych ogniwach paliwowych (SOFC). Badane są trzy możliwe obszary zastosowań wytwarzanych warstw tj. osadzanie powłok ochronnych na stalowych interkonektorach dostarczających gazy do elektrody tlenowej, wytwarzanie bariery ochronnej zapobiegającej dyfuzji...
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Ceria Based Protective Coatings for Steel Interconnects Prepared by Spray Pyrolysis
PublikacjaStainless steels can be used in solid oxide fuel/electrolysis stacks as interconnects. For successful long term operation they require protective coatings, that lower the corrosion rate and block chemical reactions between the interconnect and adjacent layers of the oxygen or the hydrogen electrode. One of the promising coating materials for the hydrogen side is ceria. Using standard sintering techniques, ceria sinters at around...
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Electrochemical synthesis and characterization of nanocomposites based on poly(3,4-ethylenedioxythiophene) and functionalized carbon nanotubes
PublikacjaThis work is focused on new composite materials consisting of poly(3,4-ethylenedioxythiophene) (pEDOT) and functionalized multi-walled carbon nanotubes synthesized electrochemically. Three types of composites were synthesized: the first one containing carbon nanotubes with carboxyl groups (covalent functionalization), the second one containing oxidized carbon nanotubes ox-MWCNTs (with different oxygen-rich polar groups) (covalent...
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Electroactive polymer/graphene oxide nanostructured composites; evidence for direct chemical interactions between PEDOT and GOx
PublikacjaThis work concerns electrochemical synthesis of nanocomposites consisting of conducting polymer and reduced graphene oxide (rGOx) as electrode materials for supercapacitors. The electrosynthesis was performed in an aqueous solution of the 3,4-ethylenedioxytiophene (EDOT) monomer and graphene oxide (GOx) without supporting electrolyte. The amount of GOx was optimized to obtain the best electrochemical performance of the nanocomposite...
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Powering the Future by Iron Sulfide Type Material (FexSy) Based Electrochemical Materials for Water Splitting and Energy Storage Applications: A Review
PublikacjaWater electrolysis is among the recent alternatives for generating clean fuels (hydrogen). It is an efficient way to produce pure hydrogen at a rapid pace with no unwanted by-products. Effective and cheap water-splitting electrocatalysts with enhanced activity, specificity, and stability are currently widely studied. In this regard, noble metal-free transition metal-based catalysts are of high interest. Iron sulfide (FeS) is one...
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Review—Advances in Rechargeable Lithium-Ion Batteries Utilizing Polyoxometalate-Functionalized Nanocarbon Materials
PublikacjaPolyoxometalates (POMs) are inorganic nanoclusters that consist of oxygen and transition metals. These nanoclusters serve as excellent precursors for creating electrode materials that contain transition metals. Additionally, the interaction between POMs and carbon substrates produces positive synergistic effects. There has been considerable attention on employing POMs and carbon nanostructures (for example carbon nanotubes, graphene,...
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Water uptake kinetics and electrical transport in BaCe0.6Zr0.2Y0.1M0.1O3−δ (M = Tb, Pr, Fe) protonic conductors
PublikacjaBaCe0.6Zr0.2Y0.1M0.1O3−d (M = Fe, Pr, Tb) is a mixed conducting oxide in which three mobile charge carriers – oxygen ion, electron/hole, and protonic defects – are present. These types of materials have gained much interest as electrode materials for protonic ceramic fuel cells (PCFCs) and protonic ceramic electrolysis cells (PCECs). In this study, the water uptake and oxygen transport properties of different BaCe0.6Zr0.2Y0.1M0.1O3−d...
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Coupling between the photoactivity and CO2 adsorption on rapidly thermal hydrogenated vs. conventionally annealed copper oxides deposited on TiO2 nanotubes
PublikacjaHighly ordered spaced titanium dioxide nanotubes were fabricated via electrochemical anodization and modified with titania nanoparticles and copper oxides. Such materials were rapidly annealed in hydrogen atmosphere or conventionally in a tube furnace in air, in which the temperature slowly increases. Applied synthesis procedure can be considered as simple, cost-effective, and environmentally friendly as it allows for reduction...
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Induced-fit binding of laccase to gold and carbon electrodes for the biological fuel cell applications
PublikacjaAnalogues of laccase natural substrates (syringic, veratric, ferulic, vanillic, isovanillic, 3,5-dimethoxybenzoic aldehydes) were employed to bind and orient laccase molecules in a way which facilitates adsorption of the catalyst molecules and their electrical connection with the conductive support. Laccase was bound efficiently to these substrates both on gold and carbon electrodes forming, respectively, 2D and 3D films sensitive...
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High-temperature Co-electrolysis of CO2/H2O and direct methanation over Co-impregnated SOEC. Bimetallic synergy between Co and Ni
PublikacjaTo study the synergy between the transition metals for enhancing the electrochemical and chemical activity, a series of SOECs were modified with a small amount of Co ions, namely 1.8, 3.6, and 5.4 wt% in the reduced state. The addition of βCD into the precursor solution allowed for extremely fine dispersion of Co species across the Ni-YSZ cermet structure. The sample containing 3.6 wt% Co reached an outstanding over 2.5-times-higher...
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New ceramic materials derived from pyrolyzed poly(1,2-dimethylsilazane) and starch as a potential anode for Li-ion batteries
PublikacjaNewmaterialswere obtained by pyrolysis of starch (S) and poly(1,2-dimethylsilazane) (PSN) (weight ratio: PSN/S 30/70) at temperature a) 500 °C, b) 700 °C and c) 900 °C. Ceramic materials were characterized by infrared spectroscopy, TGA, Raman spectroscopy and SEM. New Si\O and shifted Si\C stretching vibration modes emerged confirming direct interaction between silicon originating fromsilazane and oxygen coming fromstarch. The...
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Tailoring Defects in B, N-Codoped Carbon Nanowalls for Direct Electrochemical Oxidation of Glyphosate and its Metabolites
PublikacjaTailoring the defects in graphene and its related carbon allotropes has great potential to exploit their enhanced electrochemical properties for energy applications, environmental remediation, and sensing. Vertical graphene, also known as carbon nanowalls (CNWs), exhibits a large surface area, enhanced charge transfer capability, and high defect density, making it suitable for a wide range of emerging applications. However, precise...
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Iron doped manganese cobaltite spinel coatings produced by electrophoretic co-deposition on interconnects for solid oxide cells: Microstructural and electrical characterization
PublikacjaWe report a systematic microstructural and electrical characterization of iron doped Mn–Co spinel coatings processed by electrophoretic co-deposition of Mn1.5Co1.5O4 and Fe2O3 powders on Crofer 22 APU and AISI 441 steel substrates. Iron addition to Mn–Co spinel coating leads to a reduction of the area specific resistance on both substrates, after 3200 h at 750 °C. The Fe doped Mn–Co coating both leads to a thinner oxide scale and...
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A set of data constituting the basis for the publication entitled "Mitochondria dysfunction is one of the causes of diclofenac toxicity in the green alga Chlamydomonas reinhardtii"
Dane BadawczeNon-steroidal anti-inflammatory drugs (NSAIDs), such as diclofenac (DCF), form a significant group of environmental contaminants. When the toxic effects of DCF on plants are analyzed, authors often focus on photosynthesis, whilemitochondrial respiration is usually overlooked. Therefore, an in vivo investigation of plant mitochondria functioning under...
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Materials for energy storage and conversion devices 2022/2023
Kursy OnlineElectrodes: Metals as electrodes in aqueous and non-aqueous systems, metal nanoparticles. Collectors current. 3D, 2D, 1 D carbons, carbon nanomaterials. Organic semiconductors "Synthetic metals" - p-type, n-type. Inorganic semiconductors: oxides, selenides, sulfides, others. Intercalated electrodes. Mixed conductors (MIEC). Photo-active semiconductor materials. Electrolytes. Water electrolytes in commercial products. Electroactive...
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Oznaczanie tlenu – od metody Winklera do czujników enzymatycznych (Determination of oxygen – from Winkler Method to enzymatic sensor)
PublikacjaMonitoring of dioxygen levels is of utmost importance from the view-point of life processes, medical diagnostics, nutrition and chemical industries. In all these measurements both low and high levels of this element are important. The common methods for the determination of dioxygen are the Winkler method, Clark electrode and pulsoxymeters. A new, already strong field of research can be now recognized – the development of miniaturized...
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Depth chemical profile in a CeIr3 sample
Dane BadawczeThe polycrystalline sample of CeIr3 used in the present studies was synthesized by arc-melting cerium (4N) and iridium (3N5) in an arc furnace on a water-cooled copper hearth using a tungsten electrode under a high purity argon atmosphere. A piece of zirconium was used as an oxygen getter. First, a button of Ir was prepared by arc-melting the iridium...
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Influence of the boron doping level on the electrochemical oxidation of raw landfill leachates: advanced pre-treatment prior to the biological nitrogen removal
PublikacjaThe electrochemical oxidative treatment of landfill leachates (LLs) containing high amounts of ammonia nitrogen and organic matter was used as a promising method, prior to biological processes, to achieve the final effluent quality that would be acceptable by current regulations. The deposited boron-doped diamond electrodes (BDDs) with different boron doping concentrations (10000, 5000 and 500 ppm of B) were applied as anodes....
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Aleksander Mroziński dr inż.
OsobyAleksander Mroziński jest doktorantem na Wydziale Elektroniki, Telekomunikacji i Informatyki Politechniki Gdańskiej. Od czerwca 2019r. został zatrudniony na stanowisku redaktora metadanych w projekcie MOST DANYCH. Ponadto jest uczestnikiem trzech innych projektów realizowanych na Politechnice Gdańskiej: InterPhD II, OPUS 13 oraz PROM. Chęć poznawania świata sprawia, że stara się zdobywać multidyscyplinarną wiedzę oraz umiejętności...
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Electrical conductivity of the Sr0.86Ti0.65Fe0.35O3-d pellet at different oxygen partial pressures
Dane BadawczeThis dataset contains results electrical conductivity measurements of dense Sr0.86Ti0.65Fe0.35O3-d (STF35) pellet. DC electrical conductivity measurements of STF35 were performed by the Van der Pauw method. Studies were performed at different oxygen partial pressures (20%, 1% and 0.1%) under humidified (~4 vol%) gas flow rate of 50 ml min -1.
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SEM images of symmetrical cell interface with SrTi0.30Fe0.70O3-d electrode and CGO-20 substrate in function of sintering temperature
Dane BadawczeThis dataset contains images of polished cross section of symmetrical cell interface with SrTi0.30Fe0.70O3-d electrode and CGO-20 substrate in function of sintering temperature (800 °C, 900°C and 1000 °C) . Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope (SEM) with an accelerating voltage...
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SEM image and EDS map of SrTi0.50Fe0.50O3-d powder aglomerate
Dane BadawczeThis dataset contains image of the SrTi0.50Fe0.50O3-d powder aglomerate with EDS map analysis results. Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope (SEM) with an accelerating voltage of 10 kV in a high vacuum mode. The chemical compositions of the investigated powder were determined...
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SEM image and EDS map of SrTi0.65Fe0.35O3-d powder aglomerate
Dane BadawczeThis dataset contains image of the SrTi0.65Fe0.35O3-d powder aglomerate with EDS map analysis results. Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope (SEM) with an accelerating voltage of 10 kV in a high vacuum mode. The chemical compositions of the investigated powder were determined...
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SEM images of symmetrical cell interface with SrTi0.65Fe0.35O3-d electrode and CGO-20 substrate in function of sintering temperature
Dane BadawczeThis dataset contains images of polished cross section of symmetrical cell interface with SrTi0.65Fe0.35O3-d electrode and CGO-20 substrate in function of sintering temperature (800 °C, 900°C and 1000 °C) . Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope (SEM) with an accelerating voltage...
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SEM images of symmetrical cell interface with SrTi1-xFexO3-d electrodes and CGO-20 substrate sintered at 800 °C
Dane BadawczeThis dataset contains images of polished cross section of symmetrical cell interface with SrTi1-xFexO3-d (x=0.35; 0.50; 0..70) electrodes and CGO-20 substrate sintered at 800 °C. Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope (SEM) with an accelerating voltage of 12 kV in a high vacuum...
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SEM image and EDS map of SrTi0.50Fe0.50O3-d porous electrode sintered at 800 °C
Dane BadawczeThis dataset contains image of the SrTi0.50Fe0.50O3-d porous electrode sintered at 800 °C with EDS map analysis results. This study were performed for better understanding the chemical composition of flat like structures that occurs in electrode. Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope...
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Electrical conductivity of the SrTi1-xFexO3-d pellets at 20% pO2
Dane BadawczeThis dataset contains results electrical conductivity measurements of dense SrTi1-xFexO3-d (x=0.35, 0.50, 0.70) pellets. DC electrical conductivity measurements were performed by the Van der Pauw method between 900 °C and 200 °C. Studies were performed at 20% of oxygen partial pressure under humidified (~4 vol%) gas flow rate of 50 ml min -1.
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SEM images of symmetrical cell interface with SrTi0.50Fe0.50O3-d electrode and CGO-20 substrate in function of sintering temperature
Dane BadawczeThis dataset contains images of polished cross section of symmetrical cell interface with SrTi0.50Fe0.50O3-d electrode and CGO-20 substrate in function of sintering temperature (800 °C, 900°C and 1000 °C) . Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope (SEM) with an accelerating voltage...
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Electrical conductivity of the (Ce0.80Gd0.20)O1.90 pellet at different oxygen partial pressures
Dane BadawczeThis dataset contains results electrical conductivity measurements of dense (Ce0.80Gd0.20)O1.90 (CGO-20) pellet. DC electrical conductivity measurements of CGO-20 were performed by the Van der Pauw method between 900 °C and 450 °C with 50 °C step. Studies were performed at different oxygen partial pressures (100%, 20% and 1%) under humidified (~4...
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SEM image and EDS map of SrTi0.30Fe0.70O3-d powder aglomerate
Dane BadawczeThis dataset contains image of the SrTi0.30Fe0.70O3-d powder aglomerate with EDS map analysis results. Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope (SEM) with an accelerating voltage of 10 kV in a high vacuum mode. The chemical compositions of the investigated powder were determined...
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SEM image and line EDS of SrTi0.50Fe0.50O3-d porous electrode sintered at 800 °C
Dane BadawczeThis dataset contains image of the SrTi0.50Fe0.50O3-d porous electrode sintered at 800 °C with line EDS analysis results. Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope (SEM) with an accelerating voltage of 20 kV in a high vacuum mode. The chemical compositions of the investigated powder...
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SEM images of symmetrical cell interface with Sr1.05Ti0.30Fe0.70O3-d electrodes and CGO-20 substrate sintered at 800 °C, 900 °C and 1000 °C
Dane BadawczeThis dataset contains images of polished cross section of symmetrical cell interface with Sr1.05Ti0.30Fe0.70O3-d electrodes and CGO-20 substrate sintered at three different temperatures 800 °C, 900 °C and 1000 °C. Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope (SEM) with an accelerating...
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Thermogravimetric analysis (TGA) of the SrxTi0.30Fe0.70O3-d materials
Dane BadawczeThis dataset contains results of thermogravimetric analysis (TGA) fot SrxTi0.30Fe0.70O3-d materials (x=0.90, 0.95, 1.00 and 1.05). The TGA experiments were carried out using a microbalance (CI Precision MK5) in the temperature range between 900 °C and 200 °C. During the whole measurement procedure, air was fed to the furnace chamber at a flow rate of...
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Chemical diffusion coefficient of oxygen (D*) of the SrxTi0.30Fe0.70O3 (x=0.90, 0.95 and 1.00) at different temperatures
Dane BadawczeIn this dataset are presented D* values designated based on the electrical conductivity relaxation (ECR) mesurement of the SrxTi0.30Fe0.70O3 (x=0.90, 0.95, 1.00) materials. The applied temperatures were 800 °C, 750 °C, 700 °C, 650 °C, and 600 °C. Studies were performed in a small tube furnace (internal diameter ~20 mm) with 64 cm3 gas volume. During...
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Chemical oxygen surface exchange coefficient (k*) of the SrxTi0.30Fe0.70O3 (x=0.90, 0.95 and 1.00) at different temperatures
Dane BadawczeIn this dataset are presented k* values designated based on the analysis of the electrical conductivity relaxation (ECR) mesurement of the SrxTi0.30Fe0.70O3 (x=0.90, 0.95, 1.00) materials. The applied temperatures were 800 °C, 750 °C, 700 °C, 650 °C, and 600 °C. Studies were performed in a small tube furnace (internal diameter ~20 mm) with 64 cm3 gas...
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SEM images of symmetrical cell interface with Sr0.90Ti0.30Fe0.70O3-d electrodes and CGO-20 substrate sintered at 800 °C, 900 °C and 1000 °C
Dane BadawczeThis dataset contains images of polished cross section of symmetrical cell interface with Sr0.90Ti0.30Fe0.70O3-d electrodes and CGO-20 substrate sintered at three different temperatures 800 °C, 900 °C and 1000 °C. Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope (SEM) with an accelerating...
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Dilatometry results of SrxTi0.30Fe0.70O3-d materials
Dane BadawczeThis dataset contains results of dilatometry measurements of SrxTi0.30Fe0.70O3-d (x=0.90, 0.95, 1.00 and 1.05) materials. The investigation of the linear thermal expansion was carried out using a Netzsch DIL402 dilatometer. The SrxTi0.30Fe0.70O3-d powder was formed into cylinders and heat up to 1100 °C with a heating rate of 5 °C min−1, dwelled for...
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SEM images of symmetrical cell interface with Sr0.95Ti0.30Fe0.70O3-d electrodes and CGO-20 substrate sintered at 800 °C, 900 °C and 1000 °C
Dane BadawczeThis dataset contains images of polished cross section of symmetrical cell interface with Sr0.95Ti0.30Fe0.70O3-d electrodes and CGO-20 substrate sintered at three different temperatures 800 °C, 900 °C and 1000 °C. Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope (SEM) with an accelerating...
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Particle size distributions (PSD) and the specific surface area (BET) results for SrxTi0.30Fe0.70O3-d materials
Dane BadawczeThis dataset contains results of particle size distributions (PSD) and BET measuremnt fot SrxTi0.30Fe0.70O3-d materials (x=0.90, 0.95, 1.00 and 1.05). The PSD of the powders were obtained using a Zetasizer Nano dynamic light scattering analyser (Malvern Panalytica). Measurements of the STF70-x solution in ethanol using backscattering mode .
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SEM images of symmetrical cell interface with Sr1.00Ti0.30Fe0.70O3-d electrodes and CGO-20 substrate sintered at 800 °C, 900 °C and 1000 °C
Dane BadawczeThis dataset contains images of polished cross section of symmetrical cell interface with Sr1.00Ti0.30Fe0.70O3-d electrodes and CGO-20 substrate sintered at three different temperatures 800 °C, 900 °C and 1000 °C. Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope (SEM) with an accelerating...
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The electrical conductivity relaxation curve of the SrxTi0.30Fe0.70O3 (x=0.90 and 1.00) at 700 °C
Dane BadawczeIn this dataset are presented exemplary curves used for analysis of the electrical conductivity relaxation (ECR) mesurement of the SrxTi0.30Fe0.70O3 (x=0.90, 1.00) materials. The applied measuring temperature were 700 °C. Studies were performed in a small tube furnace (internal diameter ~20 mm) with 64 cm3 gas volume. During the four-point single frequency...
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Low temperature electrical conductivity of the SrFeO3-d pellet
Dane BadawczeThis dataset contains results of low temperature electrical conductivity measurements of dense SrFeO3-d (SFO) pellet. DC electrical conductivity measurements of SFO were performed by the Van der Pauw method between 400 °C and room temperature with 20 °C step. Studies were performed at Synthetic Air flow under humidified (~4 vol%) gas flow rate of 40...
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X-ray diffractometry results of the Sr1.05Ti0.30Fe0.70O3-d material before and after H2-TPR measurement
Dane BadawczeThis dataset contains results of X-ray diffractometry mesurement (XRD) of the Sr1.05Ti0.30Fe0.70O3-d material. The phase composition of the investigated powders was analyzed by XRD at room temperature. The X-ray diffractometry (XRD) technique was used to determine the phase composition of the fabricated powder and powder after H2-TPR (temperature programmed...
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Dilatometry results of SrTi0.50Fe0.50O3-d powder
Dane BadawczeThis dataset contains results of dilatometry measurements of SrTi0.50Fe0.50O3-d powder. The investigation of the linear thermal expansion was carried out using a Netzsch DIL402 dilatometer. The SrTi0.50Fe0.50O3-d powder was formed into cylinders and heat up to 1100 °C with a heating rate of 5 °C min−1, dwelled for 15 min, and then cooled at a rate of...
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X-ray diffractometry results of the SrTi0.50Fe0.50O3-d powder
Dane BadawczeThis dataset contains results of X-ray diffractometry mesurement (XRD) of the SrTi0.50Fe0.50O3-d (STF50) powder after ball milling. The phase composition of the investigated STF50 powder was analyzed by XRD at room temperature. The X-ray diffractometry (XRD) technique was used to determine the phase composition of the fabricated powder. Measurements...
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X-ray diffractometry results of the SrTi0.35Fe0.65O3-d powder
Dane BadawczeThis dataset contains results of X-ray diffractometry mesurement (XRD) of the SrTi0.35Fe0.65O3-d (STF35) powder after ball milling. The phase composition of the investigated STF35 powder was analyzed by XRD at room temperature. The X-ray diffractometry (XRD) technique was used to determine the phase composition of the fabricated powder. Measurements...
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Low temperature electrical conductivity of the SrTi0.65Fe0.35O3-d pellet
Dane BadawczeThis dataset contains results of low temperature electrical conductivity measurements of dense SrTi0.65Fe0.35O3-d (STF35) pellet. DC electrical conductivity measurements of STF35 were performed by the Van der Pauw method between 400 °C and room temperature with 20 °C step. Studies were performed at Synthetic Air flow under humidified (~4 vol%) gas...
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Low temperature electrical conductivity of the SrTi0.30Fe0.70O3-d pellet
Dane BadawczeThis dataset contains results of low temperature electrical conductivity measurements of dense SrTi0.30Fe0.70O3-d (STF70) pellet. DC electrical conductivity measurements of STF70 were performed by the Van der Pauw method between 400 °C and room temperature with 20 °C step. Studies were performed at Synthetic Air flow under humidified (~4 vol%) gas...
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Low temperature electrical conductivity of the SrTi0.50Fe0.50O3-d pellet
Dane BadawczeThis dataset contains results of low temperature electrical conductivity measurements of dense SrTi0.50Fe0.50O3-d (STF50) pellet. DC electrical conductivity measurements of STF50 were performed by the Van der Pauw method between 400 °C and room temperature with 20 °C step. Studies were performed at Synthetic Air flow under humidified (~4 vol%) gas...